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Small-angle scattering for characterizing nano-scale heterogeneities of light elements in steels

Research Project

Project/Area Number 21246103
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionNational Institute for Materials Science

Principal Investigator

OHNUMA Masato  独立行政法人物質・材料研究機構, 量子ビームユニット, 主席研究員 (90354208)

Co-Investigator(Kenkyū-buntansha) SUZUKI Jun-ichi  原子力研究機構, J-PARCセンター, 主任研究員 (40354899)
TSUZAKI Kaneaki  物質・材料研究機構, 元素戦略センター, センター長 (40179990)
AKIYAMA Eiji  物質・材料研究機構, 元素戦略センター, 主幹研究員 (70231834)
FURUSAKA Michihiro  北海道大学, 工学研究院, 教授 (60156966)
Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥40,300,000 (Direct Cost: ¥31,000,000、Indirect Cost: ¥9,300,000)
Fiscal Year 2011: ¥7,150,000 (Direct Cost: ¥5,500,000、Indirect Cost: ¥1,650,000)
Fiscal Year 2010: ¥7,930,000 (Direct Cost: ¥6,100,000、Indirect Cost: ¥1,830,000)
Fiscal Year 2009: ¥25,220,000 (Direct Cost: ¥19,400,000、Indirect Cost: ¥5,820,000)
Keywordsインテリジェント / 安全 / 安心材料 / 量子ビーム / 安全・安心 / 軽元素ナノスケール測定 / 安全・安心材料
Research Abstract

For suppressing hydrogen embrittlement, small-angle neutron scattering(SANS) measurements system has been optimized to get accurate and keep high reproducibility for relatively small samples for bolts. Furthermore, combined use of SANS and small-angle X-ray scattering(SAXS) has been established for getting compositional information of the embryo or clusters of carbide, oxide, nitride or other hetero-structure with light elements.

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (52 results)

All 2012 2011 2010 2009

All Journal Article (26 results) (of which Peer Reviewed: 26 results) Presentation (26 results)

  • [Journal Article] 小角散乱法によるナノサイズ不均質の評価2012

    • Author(s)
      大沼正人
    • Journal Title

      表面科学

      Volume: 33 Pages: 278-283

    • NAID

      10030756294

    • Related Report
      2011 Annual Research Report 2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen-induced cracking at grain and twin boundaries in an Fe. Mn. C austenitic steel2012

    • Author(s)
      M. Koyama, E. Akiyama, T. Sawaguchi, D. Raabe, K. Tsuzaki
    • Journal Title

      Scripta Mater

      Volume: 66 Pages: 459-462

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen Embrittlement of a 1500-MPa Tensile Strength Level Steel with an Ultrafine Elongated Grain Structure2012

    • Author(s)
      Y. Nie, Y. Kimura, T. Inoue, F. Yin, E. Akiyama, K. Tsuzaki
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 43A Pages: 1670-1687

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of delayed fracture property of high strength bolt steels2012

    • Author(s)
      E. Akiyama
    • Journal Title

      ISIJ International

      Volume: 52 Pages: 307-315

    • NAID

      10030747023

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Analysis of inclusions in low carbons steel using small-angle X-ray and neutron scattering2012

    • Author(s)
      Y. Oba, S. Koppoju, M. Ohnuma, Y. Kinjo, S. Morooka, Y. Tomota, J. Suzuki, D. Yamaguchi, S. Koizumi, M. Sato, T. Shiraga
    • Journal Title

      ISIJ International

      Volume: 52 Pages: 457-463

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Analysis of Inclusions in Low Carbon Free Cutting Steel Using Small-angle X-ray and Neutron Scattering2012

    • Author(s)
      Y.Oba, S.Koppoju, M Ohnuma, Y.Kinjo, S.Morooka, Y.Tomota J.Suzuki, D.Yamaguchi, S.Koizumi, M.Sato, T.Shiraga
    • Journal Title

      ISIJ International

      Volume: 52 Pages: 457-463

    • NAID

      10030974112

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 金属組織研究への小角散乱の利用2011

    • Author(s)
      大沼正人
    • Journal Title

      非破壊検査

      Volume: 60 Pages: 86-92

    • NAID

      10027903001

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Delayed Fracture of High Strength Steels under Atmospheric Corrosion2011

    • Author(s)
      E. Akiyama
    • Journal Title

      Zairyo-to-Kankyo

      Volume: 60 Pages: 184-189

    • NAID

      10028124875

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Delayed Fracture of High Strength Steels under Atmospheric Corrosion2011

    • Author(s)
      E. Akiyama
    • Journal Title

      Corrosion Engineering

      Volume: 60 Pages: 148-155

    • NAID

      10028124875

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Constant-load delayed fracture test of atmospherically corroded high strength steels2011

    • Author(s)
      E. Akiyama, K. Matsukado, S. Li, K. Tsuzaki
    • Journal Title

      Applied Surface Science

      Volume: 257 Pages: 8725-8281

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen entry into Fe and high strength steels under simulated atmospheric corrosion2011

    • Author(s)
      E. Akiyama, S. Li, T. Shinohara, Z. Zhang, K. Tsuzaki
    • Journal Title

      Electrochimica Acta

      Volume: 56 Pages: 1799-1805

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Analysis of Precipitates in Vanadium-microalloyed Medium Carbon Steels Using Small-angle X-ray and Neutron Scattering Methods2011

    • Author(s)
      Y. Oba, S. Koppoju, M. Ohnuma, T, Murakami, H. Hatano, K. Sasakawa, A. Kitahara, J. Suzuki
    • Journal Title

      ISIJ International

      Volume: 51 Pages: 1852-1858

    • NAID

      10030745657

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen behaviorin an Ultrafine-Grained Electrodeposited Pure Iron2011

    • Author(s)
      Y. Su, Y. Tomota, J. Suzuki, M. Ohnuma
    • Journal Title

      ISIJ international

      Volume: 51 Pages: 1534-1538

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Analysis of Precipitate in Vanadium-microalloyed Medium Carbon Steels Using Small-angle X-ray and Neutron Scattering2011

    • Author(s)
      Y.Oba, S.Koppoju, M.Ohnuma, T.Murakami, H.Hatano, K.Sasakawa, A.Kitahara, J.Suzuki
    • Journal Title

      ISIJ International

      Volume: 51 Pages: 1852-1858

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of hydrogen entry into high strength steel under atmospheric corrosion2010

    • Author(s)
      E. Akiyama, K. Matsukado, M. Wang, K. Tsuzaki
    • Journal Title

      Corros. Sci

      Volume: 52 Pages: 2758-2765

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrogen embrittlement property of a 1700 MPa class ultra-high strength tempered martensitic steel2010

    • Author(s)
      S. Li, E. Akiyama, Y. Kimura, K. Tsuzaki, N. Uno, B. Zhang
    • Journal Title

      Science and Technology of Advanced Materials

      Volume: 11 Pages: 25005-25005

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of delayed fracture property of outdoor-exposed high strength AISI 4135 steels2010

    • Author(s)
      S. Li, E. Akiyama, N. Uno, K. Hirai, K. Tsuzaki, B. Zhang
    • Journal Title

      Corros. Sci

      Volume: 52 Pages: 3198-3204

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of susceptibility of high strength steels to delayed fracture by using Cyclic Corrosion Test and SSRT2010

    • Author(s)
      S. Li, Z. Zhang, E. Akiyama, K. Tsuzaki, B. Zhang
    • Journal Title

      Corros. Sci

      Volume: 52 Pages: 1660-1667

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] 中性子小角散乱法による鉄鋼中ナノ析出物のサイズ評価2010

    • Author(s)
      安原久雄,佐藤馨,田路勇樹,大沼正人,鈴木淳市,友田陽
    • Journal Title

      鉄と鋼

      Volume: 96

    • NAID

      130000450151

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] ProbingAr ion induced nanocavties/bubbles in silicon by small-angle x-ray scattering2010

    • Author(s)
      K. Suresh, M. Ohnuma, Y. Oba, N. Kishimoto, P. Das, T. K. Chini
    • Journal Title

      J. Applied Physics

      Volume: 107 Pages: 73504-73504

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Size Analysis of Nanometer Titanium Carbide in Steel by Using Small-Angle Neutron Scattering2010

    • Author(s)
      H.Yasuhara, K.Sato, Y.Toji, M. Ohnuma, J.Suzuki, Y.Tomota
    • Journal Title

      TETSU TO HAGANE-J.ISIJ

      Volume: 96 Pages: 15-19

    • NAID

      130000450151

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Stress-induced magnetic and structural anisotropy of nanocry stalline Fe-based alloys2010

    • Author(s)
      M.Ohnuma, T.Yanai, K.Hono, M.Nakano, H.Fukunaga, Y.Yoshizawa, G.Herzer
    • Journal Title

      J.Appl.Phys

      Volume: 108

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 金属組織研究への小角散乱の利用(解説記事)2010

    • Author(s)
      大沼正人
    • Journal Title

      非破壊検査

      Volume: 60 Pages: 86-92

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Probing Ar ion induced nanocavities/bubbles in silicon by small-angle x-ray scattering2010

    • Author(s)
      K.Suresh, M.Ohnuma, Y.Oba, N.Kishimoto, P.Das, T.K.Chini
    • Journal Title

      JOURNAL OF APPLIED PHYSICS 107

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A new method for quantitative analysis of the scale and composition of nanosized oxide in 9C-ODS steel2009

    • Author(s)
      M. Ohnuma, J. Suzuki, S. Ohtsuka, S-W. Kim, T. Kaito, M. Inoue, H. Kitazawa
    • Journal Title

      Acta materialia

      Volume: 57 Pages: 5571-5581

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] New Method for the Quantitative Analysis of Scale and Composition of Nano-size oxide in 9Cr-ODS steel2009

    • Author(s)
      M.Ohnuma, J.Suzuki, S.Ohtsuka, S-W.Kim, T.Kaito, M.Inoue, H.Kitazawa
    • Journal Title

      ACTA MATERIALIA 57

      Pages: 5571-5581

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Presentation] Combined Use of Small-Angle X-Ray and Neutron Scattering : SAS in Color2012

    • Author(s)
      Ohnuma, Oba, Kozikowski, Koppoju
    • Organizer
      TMS2012(アメリカ材料系3学会141回年会)
    • Place of Presentation
      合衆国(オーランド)
    • Related Report
      2011 Final Research Report
  • [Presentation] Combined Use of Small-Angle X-ray and Neutron Scattering2012

    • Author(s)
      大沼正人
    • Organizer
      TMS(アメリカ材料系3学会合同会議)
    • Place of Presentation
      オーランド(米国)(招待講演)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Wetting process ofβ-FeOOH with Ti by Small-angle neutron and X-ray scattering2011

    • Author(s)
      Ohnuma, Oba, Kozikowski, Wakabayashi, Sasakawa, Nakayama, Ishikawa
    • Organizer
      21st Academic Symposium of MRS-Japan 2011
    • Place of Presentation
      横浜情報文化センター
    • Related Report
      2011 Final Research Report
  • [Presentation] Combined Use of Small-Angle X-ray and Neutron Scattering2011

    • Author(s)
      大沼正人
    • Organizer
      The 7th International Symposium on the Characterization of Metal(韓国金属学会中のセミナー)
    • Place of Presentation
      テジョン(韓国)(招待講演)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Wetting Process of beta-FeOOH with Ti by small-angle neutron and X-ray scattering2011

    • Author(s)
      大沼正人
    • Organizer
      日本鉄鋼協会第162回秋期講演大会
    • Place of Presentation
      大阪
    • Related Report
      2011 Annual Research Report
  • [Presentation] Microstructural Analysis of Metallic Materials using Small-Angle X-ray and Neutron Scattering2011

    • Author(s)
      大場、大沼、Koppoju
    • Organizer
      1st Asia-Oceania Conference on Neutron Scattering
    • Place of Presentation
      つくば
    • Related Report
      2011 Annual Research Report
  • [Presentation] 中性子・X線小角散乱による鉄鋼材料の微細組織の観察2010

    • Author(s)
      大沼正人
    • Organizer
      日本中性子科学会
    • Place of Presentation
      東北大学(宮城県)
    • Year and Date
      2010-12-10
    • Related Report
      2010 Annual Research Report
  • [Presentation] 鉄鋼材料研究への中性子小角散乱の利用2010

    • Author(s)
      大沼正人
    • Organizer
      日本鉄鋼協会 秋季講演大会
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] 大強度型パルス中性子小中角散乱装置「大観」の開発III2010

    • Author(s)
      鈴木,高田,篠原,奥,吉良,中谷,稲村,伊藤,鈴谷,相澤,新井,大友,杉山
    • Organizer
      日本物理学会2010年秋季大会
    • Place of Presentation
      大阪府立大学
    • Year and Date
      2010-09-24
    • Related Report
      2011 Final Research Report
  • [Presentation] X線および中性子小角散乱による材料中のヘテロ構造の定量評価2010

    • Author(s)
      大沼正人
    • Organizer
      日本分析化学会
    • Place of Presentation
      東北大学(宮城県)(招待講演)
    • Year and Date
      2010-09-16
    • Related Report
      2010 Annual Research Report
  • [Presentation] 中性子小角散乱による鉄鋼中水素のトラップ現象の検出/中性子小角散乱による鉄鋼中水素のトラップ現象の検出(招待講演)2010

    • Author(s)
      大沼正人
    • Organizer
      第46回X線材料強度に関する討論会
    • Place of Presentation
      島製作所 関西支社,大阪市
    • Year and Date
      2010-01-08
    • Related Report
      2009 Annual Research Report
  • [Presentation] 中性子・X線小角散乱による鉄鋼材料の微細組織の観察2010

    • Author(s)
      大沼
    • Organizer
      2010年日本中性子科学会
    • Place of Presentation
      東北大学
    • Related Report
      2011 Final Research Report
  • [Presentation] X線および中性子小角散乱による材料中のへテロ構造の定量評価2010

    • Author(s)
      大沼
    • Organizer
      日本分析化学会第59年会
    • Place of Presentation
      東北大学
    • Related Report
      2011 Final Research Report
  • [Presentation] 小角散乱によるゴムメタル組織のナノ不均質構造の解析/小角散乱によるゴムメタル組織のナノ不均質構造の解析2010

    • Author(s)
      大沼, Koppoju,大場,倉本,古田
    • Organizer
      日本金属学会秋期講演大会
    • Place of Presentation
      北海道大学
    • Related Report
      2011 Final Research Report
  • [Presentation] J-PARC中性子小中角散乱装置「大観」の開発と鉄鋼材料評価への応用2010

    • Author(s)
      鈴木,高田,篠原,奥,吉良,中谷,稲村,伊藤,鈴谷,相澤,新井,大友,杉山
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Place of Presentation
      北海道大学
    • Related Report
      2011 Final Research Report
  • [Presentation] Microstructure and deformation behavior of an ultrafine-grained electrodeposited iron2010

    • Author(s)
      Su,友田,鈴木,大沼
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Place of Presentation
      北海道大学
    • Related Report
      2011 Final Research Report
  • [Presentation] 鉄鋼材料研究への中性子小角散乱の利用2010

    • Author(s)
      大沼,大場, Koppoju,鈴木,友田
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Place of Presentation
      北海道大学
    • Related Report
      2011 Final Research Report
  • [Presentation] 小角散乱法による微細組織の定量評価/小角散乱法による微細組織の定量評価(招待講演)2009

    • Author(s)
      大沼正人
    • Organizer
      コマテリアルフォーラム 原子レベルの元素代替戦略のための計測技技術
    • Place of Presentation
      東京大学 生産技術研究所,東京都
    • Year and Date
      2009-10-28
    • Related Report
      2009 Annual Research Report
  • [Presentation] Small-angle scattering as a tool for quantitative microstructure analysis in steel research2009

    • Author(s)
      Ohnuma, Oba, Koppoju
    • Organizer
      The 5th International Symposium on the Characterization of Metal
    • Place of Presentation
      韓国金属学会(Deagu)
    • Year and Date
      2009-10-22
    • Related Report
      2011 Final Research Report
  • [Presentation] 大強度型パルス中性子小中角散乱装置「大観」の開発II2009

    • Author(s)
      鈴木,高田,篠原,奥,吉良,鈴谷,相澤,新井,大友,杉山
    • Organizer
      日本物理学会2009年秋季大会
    • Place of Presentation
      熊本大学
    • Year and Date
      2009-09-27
    • Related Report
      2011 Final Research Report
  • [Presentation] 小角散乱法による構造材料の微細組織解析/小角散乱法による構造材料の微細組織解2009

    • Author(s)
      大沼正人
    • Organizer
      東関東支部 若手会員の集う会 第3回勉強会
    • Place of Presentation
      テクノ交流館リコッティ,茨城県東海村
    • Year and Date
      2009-07-24
    • Related Report
      2009 Annual Research Report
  • [Presentation] Small-angle scattering as a tool for quantitative analysis of precipitates in steels2009

    • Author(s)
      Ohnuma, Suzuki, Oba, Koppoju
    • Organizer
      SAS2009
    • Place of Presentation
      オックスフォード大学(イギリス)
    • Related Report
      2011 Final Research Report
  • [Presentation] Characterization of Nano-oxide in ODS steels by alloy contrast variation method2009

    • Author(s)
      Ohnuma, Suzuki, Ohtsuka
    • Organizer
      SAS2009
    • Place of Presentation
      オックスフォード大学(イギリス)
    • Related Report
      2011 Final Research Report
  • [Presentation] Direct observation of Hydrogen trapped by nano-size carbide in steel2009

    • Author(s)
      Ohnuma, Suzuki, Tsuzaki, Wei
    • Organizer
      SAS2009
    • Place of Presentation
      オックスフォード大学(イギリス)
    • Related Report
      2011 Final Research Report
  • [Presentation] Direct observation of Hydrogen trapped by nano-size carbide in steel2009

    • Author(s)
      大沼正人、鈴木淳市、津崎兼彰、Fu-GaoWei
    • Organizer
      小角散乱国際会議(SAS2009)
    • Place of Presentation
      Oxford Univ, Oxford, England
    • Related Report
      2009 Annual Research Report
  • [Presentation] Characterization of Nano-oxide in ODS steels by alloy contrast variation method2009

    • Author(s)
      大沼正人、鈴木淳市、大塚智史
    • Organizer
      小角散乱国際会議(SAS2009)
    • Place of Presentation
      Oxford Univ, Oxford, England
    • Related Report
      2009 Annual Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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