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Development of Liquid-liquid Countercurrent Centrifuge Extractor for Nuclide Separation Application

Research Project

Project/Area Number 21360466
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Nuclear engineering
Research InstitutionTokyo Institute of Technology

Principal Investigator

TAKESHITA Kenji  東京工業大学, 原子炉工学研究所, 教授 (80282870)

Co-Investigator(Kenkyū-buntansha) KIKURA Hiroshige  東京工業大学, ソリューション研究機構, 准教授 (00302985)
Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥18,980,000 (Direct Cost: ¥14,600,000、Indirect Cost: ¥4,380,000)
Fiscal Year 2011: ¥6,240,000 (Direct Cost: ¥4,800,000、Indirect Cost: ¥1,440,000)
Fiscal Year 2010: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2009: ¥8,840,000 (Direct Cost: ¥6,800,000、Indirect Cost: ¥2,040,000)
Keywords遠心抽出 / 液々向流 / Taylor-Couette流 / 多段分離 / 分散 / 核種分離 / 流動可視化 / 流動解析 / 油水向流 / 連続抽出 / 軸混合効果 / 超音波パルスドップラー法 / 理論段数 / 微粒化 / セシウム / 発熱性核種
Research Abstract

A new liquid-liquid countercurrent extractor with Taylor-Couette flow was proposed and following three research subjects to improve the extraction performance were studied
(1) Increasing the stability of oil-water countercurrent flow
(2) Highly efficient extraction using oil-water emulsion
(3) Scale-up of extractor and feasibility of total extraction process
As a result, we made clear the chemico-physical properties of oil phase, water phase and inner rotor surface, which were required for the formation of suitable countercurrent flow with highly dispersed oil. By stabilizing the Taylor-Couette flow with oil-water emulsion by the addition of a small amount of PEG(poly-ethyleneglycol), the high-speed extraction with high theoretical stages more than 10 stages were attained. Finally the scale-up tests were carried out. By the use of larger extractor, the increase of theoretical stages was observed for the positive extraction and the high recovery rate for the back extraction

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (42 results)

All 2012 2011 2010 2009 Other

All Journal Article (16 results) (of which Peer Reviewed: 14 results) Presentation (24 results) Remarks (2 results)

  • [Journal Article] 軸流を伴うテーラークエッテ渦流れのUVP計測2011

    • Author(s)
      高橋秀治、木倉宏成、竹下健二、有冨正憲
    • Journal Title

      日本機械学会論文集(B編)

      Volume: 76 Pages: 1006-1010

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Characteristics of Taylor-Couette vortex flow with counter flow2011

    • Author(s)
      H. Takehashi, H. Kikura, K. Takeshita, M. Aritomi
    • Journal Title

      J. Japanese Society for Experimental Mechanics

      Volume: 11 Pages: 168-173

    • NAID

      10029700350

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Optimization of Centrifuge Extraction Operation by Visualization of Oil-water Countercurrent Flow2011

    • Author(s)
      M. Nakase, R. Makabe, K. Takeshita, H. Kikura
    • Journal Title

      17th International Conference on Separation Science and Technology for Energy Applications

      Volume: p-53

    • Related Report
      2011 Final Research Report
  • [Journal Article] Visualization of Oil-water Flow in Countercurrent Centrifuge Extractor by UVP Measurement and Numerical Calculation2011

    • Author(s)
      M. Nakase, R. Makabe, K. Takeshita
    • Journal Title

      1st China-Japan Academic Symposium on Nuclear Fuel Cycle

      Pages: 6-10

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Visualization of Dispersed Phase Flow in Centrifugal Extractor Using Taylor-Couette Vortex Flow2011

    • Author(s)
      H. Takahashi, H. Kikura, K. Takeshitaand M. Aritomi
    • Journal Title

      The 8th ASME-JSME Thermal Engineering Joint Conference

      Volume: AJTEC Pages: 2011-44403

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] 軸流を伴うテーラークェッテ渦流れのUVP計測2011

    • Author(s)
      高橋秀治、木倉宏成、竹下健二、有冨正憲
    • Journal Title

      日本機械学会論文集(B編)

      Volume: 77 Pages: 1006-1010

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Characteristics of Taylor-Couette vortex flow with counter flow2011

    • Author(s)
      H.Takehashi, H.Kikura, K.Takeshita, M.Aritomi
    • Journal Title

      J.Japanese Society for Experimental Mechanics

      Volume: 11 Pages: 168-173

    • NAID

      10029700350

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Optimization of Centrifuge Extraction Operation by Visualization of Oil-water Countercurrent Flow2011

    • Author(s)
      M.Nakase, R.Makabe, K.Takeshita, H.Kikura
    • Journal Title

      17^<th> International Conference on Separation Science and Technology for Energy Applications

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Visualization of Oil-water Flow in Countercurrent Centrifuge Extractor by UVP Measurement and Numerical Calculation (Best Presentation Award)2011

    • Author(s)
      M.Nakase, R.Makabe, K.Takeshita
    • Journal Title

      1st China-Japan Academic Symposium on Nuclear Fuel Cycle

      Pages: 6-10

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 軸流を伴うテイラークエット渦流れのUVP計測2011

    • Author(s)
      高橋秀治・木倉宏成・竹下健二・有冨正憲
    • Journal Title

      日本機械学会論文集(B編)

      Volume: 77 Pages: 1006-1006

    • NAID

      130000873860

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] aylor-Couette流を伴う液々向流型遠心抽出装置の開発2010

    • Author(s)
      竹下健二
    • Journal Title

      混相流学会誌

      Volume: 24(3) Pages: 267-274

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Characteristics of Taylor Vortex on Counter Flow2010

    • Author(s)
      H. Takahashi, H. Kikura, K. Takeshitaand M. Aritomi
    • Journal Title

      5thInternational Symposium on Advanced Science and Technology in Experimental Mechanics

      Volume: No.149

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Flow Characteristics of Taylor vortices in a new type liquid-liquid countercurrent centrifugal extractor2010

    • Author(s)
      H. Takahashi, H. Kikura, K. Takeshitaand M. Aritomi
    • Journal Title

      The 8thInternational Topical Meeting onNuclear Thermal-Hydraulicsq

      Volume: No.N8P0304

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Flow Field Measurement of Taylor-Couette Vortex Flow with Axial Flow using UVP2010

    • Author(s)
      H. Takahashi, H. Kikura, K. Takeshitaand M. Aritomi
    • Journal Title

      The14th International Symposium on Flow Visualization

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Taylor-Couette流を伴う液々向流型遠心抽出装置の開発Development of Liquid-liquid Countercurrent Centrifugal Extractor with Taylor-Couette Flo2010

    • Author(s)
      竹下健二
    • Journal Title

      混相流学会24巻3号

      Volume: 24 Pages: 267-274

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article]2009

    • Author(s)
      竹下健二
    • Journal Title

      分離プロセス工学の基礎4.4.3塔型抽出装置(朝倉書店)

    • Related Report
      2009 Annual Research Report
  • [Presentation] VOFモデルによる液々向流型遠心抽出器内の油水流動解析2012

    • Author(s)
      中瀬正彦、竹下健二
    • Organizer
      日本原子力学会2012春の年会
    • Place of Presentation
      福井大学
    • Year and Date
      2012-03-21
    • Related Report
      2011 Annual Research Report 2011 Final Research Report
  • [Presentation] 液々向流型遠心抽出器内の油水分散挙動解析2012

    • Author(s)
      中瀬正彦、竹下健二
    • Organizer
      化学工学会第77年会
    • Place of Presentation
      工学院大学
    • Year and Date
      2012-03-17
    • Related Report
      2011 Annual Research Report 2011 Final Research Report
  • [Presentation] 液々向流型遠心抽出器の流動場解析による油水分散性の評価2011

    • Author(s)
      中瀬正彦、竹下健二
    • Organizer
      日本原子力学会関東甲越支部若手発表会
    • Place of Presentation
      東京都市大学
    • Year and Date
      2011-11-17
    • Related Report
      2011 Final Research Report
  • [Presentation] 液々向流型遠心抽出器の流動場解析による油水分散性の評価2011

    • Author(s)
      中瀬正彦、竹下健二
    • Organizer
      日本原子力学会関東甲越支部若手発表会
    • Place of Presentation
      東京都市大学(奨励賞)
    • Year and Date
      2011-11-14
    • Related Report
      2011 Annual Research Report
  • [Presentation] 液々向流型遠心抽出装置の油水流動と抽出効率の関係2011

    • Author(s)
      中瀬正彦、竹下健二
    • Organizer
      日本原子力学会2011年秋の大会
    • Place of Presentation
      北九州国際会議場
    • Year and Date
      2011-09-21
    • Related Report
      2011 Annual Research Report 2011 Final Research Report
  • [Presentation] Visualization of Dispersed Phase Flow in Centrifugal Extractor Using Taylor-Couette Vortex Flow2011

    • Author(s)
      Hideharu TAKAHASHI, Hiroshige KIKURA, Kenji TAKESHITA, Masanori ARITOMI
    • Organizer
      The 8th ASME-JSME Thermal Engineering Joint Conference (AJTEC2011)
    • Place of Presentation
      Waikiki Beach Marriott Resort & Spa, Honolulu, Hawaii, USA
    • Year and Date
      2011-03-14
    • Related Report
      2010 Annual Research Report
  • [Presentation] Characteristics of Taylor Vortex on Counter Flow2010

    • Author(s)
      Hideharu TAKAHASHI, Hiroshige KIKURA, Kenji TAKESHITA, Masanori ARITOMI
    • Organizer
      The 5th International Symposium on Advanced Science and Technology in Experimental Mechanics (5th ISEM'10-Kyoto)
    • Place of Presentation
      龍谷大学(京都市下京区)
    • Year and Date
      2010-11-07
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development of Countercurrent Centrifugal Extractor with Taylor-Couette Flow for Nuclide Separation2010

    • Author(s)
      Kenji Takeshita, Hitoshi Rokkaku, Hiroshi Kinuhata
    • Organizer
      The Third International Symposium on Innovative Nuclear Energy Systems
    • Place of Presentation
      東京工業大学(東京都目黒区)
    • Year and Date
      2010-11-01
    • Related Report
      2010 Annual Research Report
  • [Presentation] Flow Characteristics of Taylor vortices in a new type liquid-liquid countercurrent centrifugal extractor2010

    • Author(s)
      Hideharu TAKAHASHI, Hiroshige KIKURA, Kenji TAKESHITA, Masanori ARITOMI
    • Organizer
      The 8th International Topical Meeting on Nuclear Thermal-Hydraulics, Operation and Safety (NUTHOS-8)
    • Place of Presentation
      Eton hotel, Shanghai, China
    • Year and Date
      2010-10-12
    • Related Report
      2010 Annual Research Report
  • [Presentation] セシウム連続抽出のための液々向流型遠心抽出装置の開発2010

    • Author(s)
      竹下健二、衣旗広志、眞壁亮司
    • Organizer
      化学工学会第42回秋季大会
    • Place of Presentation
      同志社大学(京都市上京区)
    • Year and Date
      2010-09-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] 遠心抽出装置内テイラークエット渦流れの可視化と超音波計測2010

    • Author(s)
      高橋秀治、木倉宏成、竹下健二、有冨正憲
    • Organizer
      日本実験力学会2010年度年次講演会講演論文集
    • Place of Presentation
      長崎大学
    • Year and Date
      2010-08-17
    • Related Report
      2011 Final Research Report
  • [Presentation] 遠心抽出装置内テイラークエット渦流れの可視化と超音波計測2010

    • Author(s)
      高橋秀治・木倉宏成・竹下健二・有冨正憲
    • Organizer
      日本実験力学会2010年度年次講演会
    • Place of Presentation
      長崎大学(長崎市)
    • Year and Date
      2010-08-17
    • Related Report
      2010 Annual Research Report
  • [Presentation] 遠心抽出装置内のテイラークエット渦流れの超音波流速分布計測2010

    • Author(s)
      高橋秀治、木倉宏成、竹下健二、有冨正憲
    • Organizer
      日本混相流学会年会講演会2010浜松講演論文集
    • Place of Presentation
      静岡大学
    • Year and Date
      2010-07-19
    • Related Report
      2011 Final Research Report
  • [Presentation] 遠心抽出装置内のテイラークエット渦流れの超音波流速分布計測2010

    • Author(s)
      高橋秀治・木倉宏成・竹下健二・有冨正憲
    • Organizer
      日本混相流学会年会講演会2010浜松
    • Place of Presentation
      静岡大学(浜松市)
    • Year and Date
      2010-07-19
    • Related Report
      2010 Annual Research Report
  • [Presentation] Flow Field Measurement of Taylor-Couette Vortex Flow with Axial Flow using UVP, The 14th International Symposium on Flow Visualization (ISFV14)2010

    • Author(s)
      Hideharu TAKAHASHI, Hiroshige KIKURA, Kenji TAKESHITA, Masanori ARITOMI
    • Organizer
      The 14th International Symposium on Flow Visualization (ISFV14)
    • Place of Presentation
      EXCO, Daegu, Republic of Korea
    • Year and Date
      2010-06-23
    • Related Report
      2010 Annual Research Report
  • [Presentation] 軸流を伴うテイラークエット渦流れのUVP計測2010

    • Author(s)
      高橋秀治・木倉宏成・竹下健二・有冨正憲
    • Organizer
      日本機械学会第15回動力・エネルギー技術シンポジウム
    • Place of Presentation
      早稲田大学(東京都新宿区)
    • Year and Date
      2010-06-21
    • Related Report
      2010 Annual Research Report
  • [Presentation] テイラークエット渦流れを利用した遠心抽出装置の開発2010

    • Author(s)
      高橋秀治、木倉宏成、竹下健二、有冨正憲
    • Organizer
      日本原子力学会関東・甲越支部第3回学生研究発表会
    • Place of Presentation
      東京大学
    • Year and Date
      2010-03-12
    • Related Report
      2011 Final Research Report
  • [Presentation] 高酸性溶液からのセシウム連続抽出のための液々向流型遠心抽出装置の開発2009

    • Author(s)
      衣旗広志、竹下健二
    • Organizer
      第28回 溶媒抽出討論会
    • Place of Presentation
      大阪大学
    • Year and Date
      2009-11-20
    • Related Report
      2009 Annual Research Report
  • [Presentation] Development of new countercurrent centrifugal extractor with Talor-Couette flow2009

    • Author(s)
      K. Takeshita
    • Organizer
      16th Symposium on Separation Science and Technology for Energy Applications
    • Place of Presentation
      Gatlinburg
    • Year and Date
      2009-10-21
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of new countercurrent centrifugal extractor with Taylor-Couette flow2009

    • Author(s)
      Kenji Takeshita
    • Organizer
      16th Symposium on Separation Science and Technology for Energy Applications
    • Place of Presentation
      米国、テネシー
    • Year and Date
      2009-10-19
    • Related Report
      2009 Annual Research Report
  • [Presentation] 高酸性溶液からのセシウム連続抽出のための液々向流型遠心抽出装置の開発2009

    • Author(s)
      衣旗広志、竹下健二
    • Organizer
      化学工学会第41回秋季大会
    • Place of Presentation
      広島大学
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] A New Strategy for Establishment of FBR Fuel Cycle2009

    • Author(s)
      Kenji Takeshita
    • Organizer
      第5回日中化工シンポジウム(キーノート、招待講演)
    • Place of Presentation
      中国、西安
    • Year and Date
      2009-07-22
    • Related Report
      2009 Annual Research Report
  • [Presentation] Development of countercurrent centrifugal extractor with Talor-Couette flow and its application to close-separation process2009

    • Author(s)
      K. Takeshita
    • Organizer
      6th International Conference on Stable Osotopes and Isotope Effects
    • Place of Presentation
      Isotopes
    • Year and Date
      2009-05-25
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of counter-current centrifugal extractor with Talor-Couette flow and its application to close-separation process2009

    • Author(s)
      Kenji Takeshita
    • Organizer
      6th International Conference on Stable Osotopes and Isotope Effects (Isotopes2009)招待講演
    • Place of Presentation
      ルーマニア
    • Year and Date
      2009-05-25
    • Related Report
      2009 Annual Research Report
  • [Remarks]

    • URL

      http://www.nr.titech.ac.jp/~takeshita/

    • Related Report
      2011 Final Research Report
  • [Remarks]

    • URL

      http://www.nr.titech.ac.jp/~takeshita/

    • Related Report
      2011 Annual Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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