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High spatial-resolution crystal structure analysis using annular dark-field imaging

Research Project

Project/Area Number 21510121
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Nanomaterials/Nanobioscience
Research InstitutionNational Institute for Materials Science

Principal Investigator

KIMOTO Koji  独立行政法人物質・材料研究機構, 表界面構造・物性ユニット, ユニット長 (90354399)

Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2011: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2010: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2009: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywordsナノ材料解析・評価 / 電子顕微鏡 / 結晶構造
Research Abstract

Annular dark-field(ADF) imaging in scanning transmission electron microscopy(STEM) is an effective tool for the characterization of local crystal structure, because ADF imaging has high compositional sensitivity and intuitive interpretability. In this study, we performed high sensitivity and high precision(10pm) analyses of crystal structures using STEM imaging. We revealed the validity of incoherent imaging approximation of ADF imaging. We also achieved so-called spatially-resolved diffractometry, in which the diffraction patterns are fully acquired as a function of probe coordination to investigate the mechanism of STEM imaging.

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (26 results)

All 2011 2010 2009 2007 Other

All Journal Article (4 results) (of which Peer Reviewed: 4 results) Presentation (13 results) Remarks (8 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Spatially resolved diffractometry with atomic-column resolution2011

    • Author(s)
      K. Kimoto and K. Ishizuka
    • Journal Title

      Ultramicroscopy

      Volume: vol.111 Pages: 1111-1116

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Spatially-resolved Diffractometry with atomic-column resolution2011

    • Author(s)
      Koji KIMOTO, Kazuo ISHIZUKA
    • Journal Title

      Ultramicroscopy

      Volume: 111 Issue: 8 Pages: 1111-1116

    • DOI

      10.1016/j.ultramic.2011.01.029

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Local crystal structure analysis with several picometer precision using scanning transmission electron microscopy2010

    • Author(s)
      K. Kimoto, T. Asaka, X. Yu, T. Nagai, Y. Matsui, and K. Ishizuka
    • Journal Title

      Ultramicroscopy

      Volume: vol.110 Pages: 778-782

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Local crystal structure analysis with several picometer precision using scanning transmission electron microscope2010

    • Author(s)
      K.Kimoto, T.Asaka, X.Yu, T.Nagai, Y.Matsui, K.Ishizuka
    • Journal Title

      Ultramicroscopy

      Volume: 110 Pages: 778-782

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] Spatially-resolved diffractometryによる原子コラムの観察2011

    • Author(s)
      木本浩司
    • Organizer
      超分解能電子顕微鏡分科会,日本顕微鏡学会
    • Place of Presentation
      名古屋
    • Year and Date
      2011-11-29
    • Related Report
      2011 Final Research Report
  • [Presentation] Spatially-resolved diffractometryによる原子コラムの観察2011

    • Author(s)
      木本浩司
    • Organizer
      超分解能電子顕微鏡分科会,日本顕微鏡学会
    • Place of Presentation
      名古屋(招待講演)
    • Year and Date
      2011-11-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] Status report of NIMS-Titan ; preliminary results at 80 kV TEM and STEM2011

    • Author(s)
      Koji KIMOTO
    • Organizer
      FEI "Acht 2011" Meeting
    • Place of Presentation
      オランダ・アイントホーヘン
    • Year and Date
      2011-07-22
    • Related Report
      2011 Final Research Report
  • [Presentation] Status report of NIMS-Titan ; preliminary results at 80kV TEM and STEM2011

    • Author(s)
      Koji KIMOTO
    • Organizer
      FEI "Acht 2011"Meeting
    • Place of Presentation
      オランダ・アイントホーヘン(招待講演)
    • Year and Date
      2011-07-22
    • Related Report
      2011 Annual Research Report
  • [Presentation] 透過電子顕微鏡による新材料の微細構造評価2010

    • Author(s)
      木本浩司
    • Organizer
      合同公開シンポジウムナノ・先端計測によるオープンイノベーション
    • Place of Presentation
      NIMS(茨城県つくば市)
    • Year and Date
      2010-09-07
    • Related Report
      2011 Final Research Report
  • [Presentation] 透過電子顕微鏡による新材料の微細構造評価2010

    • Author(s)
      木本浩司
    • Organizer
      合同公開シンポジウムナノ・先端計測によるオープンイノベーション
    • Place of Presentation
      (独)物質・材料研究機構(茨城県)
    • Year and Date
      2010-09-07
    • Related Report
      2010 Annual Research Report
  • [Presentation] 走査透過形電子顕微鏡による結晶構造解析の試み2010

    • Author(s)
      木本浩司
    • Organizer
      第10回日立ナノテクパーク21
    • Place of Presentation
      つくば国際会議場(茨城県つくば市)
    • Year and Date
      2010-07-16
    • Related Report
      2011 Final Research Report
  • [Presentation] 走査透過形電子顕微鏡による結晶構造解析の試み2010

    • Author(s)
      木本浩司
    • Organizer
      第10回日立ナノテクパーク21
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Year and Date
      2010-07-16
    • Related Report
      2010 Annual Research Report
  • [Presentation] High spatial-resolution analysis using scanning transmission electron microscopy ; limiting factors for realizing atomic resolution2010

    • Author(s)
      木本浩司
    • Organizer
      IBM-NIMS symposium on characterization and manipulation
    • Place of Presentation
      NIMS(茨城県つくば市)
    • Year and Date
      2010-06-14
    • Related Report
      2011 Final Research Report
  • [Presentation] High spatial-resolution analysis using scanning transmission electron microscopy ; limiting factors for realizing atomic resolution2010

    • Author(s)
      木本浩司
    • Organizer
      IBM-NIMS symposium on characterization and manipulation
    • Place of Presentation
      (独)物質・材料研究機構(茨城県)
    • Year and Date
      2010-06-14
    • Related Report
      2010 Annual Research Report
  • [Presentation] Material Characterization with High Spatial Resolution Using Transmission Electron Microscopy and Electron Energy-loss Spectroscopy2009

    • Author(s)
      K. Kimoto
    • Organizer
      Symposium on Creation of Functional Materials
    • Place of Presentation
      つくば国際会議場(つくば市)
    • Year and Date
      2009-12-05
    • Related Report
      2011 Final Research Report 2009 Annual Research Report
  • [Presentation] 透過電子顕微鏡による原子選択イメージング2009

    • Author(s)
      木本浩司
    • Organizer
      第50回真空に関する連合講演会
    • Place of Presentation
      学習院大学(東京都)
    • Year and Date
      2009-11-05
    • Related Report
      2011 Final Research Report 2009 Annual Research Report
  • [Presentation] High spatial-resolution analysis using STEM-ADF and EELS ; Limit of incoherent imaging approximation2009

    • Author(s)
      K. Kimoto
    • Organizer
      FEMMS 2009
    • Place of Presentation
      ハウステンボス(長崎市)
    • Year and Date
      2009-09-30
    • Related Report
      2011 Final Research Report 2009 Annual Research Report
  • [Remarks] 研究代表者のホームページ

    • URL

      http://www.nims.go.jp/AEMG/index-j.html

    • Related Report
      2011 Final Research Report
  • [Remarks] 特に以下のサイトに本研究に関わる成果をダイジェストとしてまとめている(英語のみ)

    • URL

      http://www.nims.go.jp/AEMG/recent/STEM-ADF/STEM-BFADF_E.html

    • Related Report
      2011 Final Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/index-j.html

    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/research_J.html

    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/recent/STEM-ADF/STEM-BFADF_E.html

    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/index-j.html

    • Related Report
      2010 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/research_J.html

    • Related Report
      2010 Annual Research Report
  • [Remarks]

    • URL

      http://www.nims.go.jp/AEMG/recent/STEM-ADF/STEM-BFADF_E.html

    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] 電子顕微鏡とその対物レンズ系収差特性の計測方法2007

    • Inventor(s)
      木本浩司, 石塚和夫, 松井良夫
    • Industrial Property Rights Holder
      NIMS
    • Filing Date
      2007-04-25
    • Acquisition Date
      2012-03-09
    • Related Report
      2011 Annual Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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