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Multi-scale characterization of functional composite materials

Research Project

Project/Area Number 21560706
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionNational Institute for Materials Science

Principal Investigator

OHKUBO Tadakatsu  独立行政法人物質・材料研究機構, 磁性材料ユニット, グループリーダー (00242462)

Co-Investigator(Renkei-kenkyūsha) HONO Kazuhiro  独立行政法人物質・材料研究機構, フェロー (60229151)
Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2011: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2010: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2009: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords構造・機能材料 / ナノ材料 / 解析・評価 / 電子顕微鏡 / 3次元アトムプローブ
Research Abstract

In order to understand the relationships between the property changes and the microstructural changes of functional composite materials due to additional element or annealing process, the structure was characterized by SEM, TEM and 3DAP with multi-scale. The origin of coercivity change by Dy diffusion process or low temperature annealing of Nd-Fe-B sintered magnet had been shown. And, the reason of ion conductivity deterioration of Gd doped CeO_2 was found to be related with grain boundary segregation and compositional fluctuation in the grain based on UV laser 3DAP analysis result.

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (40 results)

All 2012 2011 2010 2009

All Journal Article (13 results) (of which Peer Reviewed: 13 results) Presentation (27 results)

  • [Journal Article] Grain boundary and interface chemistry of a Nd-Fe-B sintered magnet2012

    • Author(s)
      H. Sepehri-Amin, T. Ohkubo, T. Shima and K. Hono
    • Journal Title

      Acta Mater

      Volume: 60 Pages: 819-830

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Grain boundary and interface chemistry of an Nd-Fe-B-based sintered magnet2012

    • Author(s)
      H.Sepehri-Amin, 他2名
    • Journal Title

      Acta Materialia

      Volume: 60 Issue: 3 Pages: 819-830

    • DOI

      10.1016/j.actamat.2011.10.043

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Laser assisted field evaporation of oxides in atom probe analysis2011

    • Author(s)
      Y. M. Chen, T. Ohkubo and K. Hono
    • Journal Title

      Ultramicroscopy

      Volume: 111 Pages: 562-566

    • Related Report
      2011 Annual Research Report 2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative atom probe analyses of rare-earth-doped ceria by femtosecond pulsed laser2011

    • Author(s)
      F. Li, T. Ohkubo, Y. M. Chen, M. Kodzuka and K. Hono
    • Journal Title

      Ultramicroscopy

      Volume: 111 Pages: 589-594

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Laser-assisted Atom Probe Analysis of Bulk Insulating Ceramics2011

    • Author(s)
      T. Ohkubo, Y. M. Chen, M. Kodzuka, F. Li, K. Oh-ishi and K. Hono
    • Journal Title

      MRS 2009 Fall Meeting Proc

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative atom probe analyses of rare-earth-doped ceria by femtosecond2011

    • Author(s)
      F.Li, 他4名
    • Journal Title

      Ultramicroscopy

      Volume: 111 Issue: 6 Pages: 589-594

    • DOI

      10.1016/j.ultramic.2010.12.011

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Grain boundary structure and chemistry of Dy-diffusion processed Nd-Fe-B sintered magnets2010

    • Author(s)
      H. Sepehri-Amin, T. Ohkubo and K. Hono
    • Journal Title

      J. Appl. Phys

      Volume: 107

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Laser-assisted three-dimensional atom probe analysis of dopant distribution in Gd-doped CeO22010

    • Author(s)
      F. Li, T. Ohkubo, Y. M. Chen, M. Kodzuka, F. Ye, D. R. Ou, T. Mori and K. Hono
    • Journal Title

      Scripta Mater

      Volume: 63 Pages: 332-335

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Grain boundary structure and chemistry of Dy-diffusion processed Nd-Fe-B sintered magnets2010

    • Author(s)
      H.Sepehri-Amin, 他2名
    • Journal Title

      J.Appl.Phys.

      Volume: 107

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Laser-assisted Atom Probe Analysis of Bulk Insulating Ceramics2010

    • Author(s)
      T.Ohkubo, 他5名
    • Journal Title

      Mater.Res.Soc.Symp.Proc.

      Volume: 1231

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Laser-assisted three-dimensional atom probe analysis of dopant distribution in Gd-doped CeO_22010

    • Author(s)
      F.Li, 他7名
    • Journal Title

      Scripta Mater.

      Volume: 63 Pages: 332-335

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Anisotropic Nd-Fe-B nanocrystalline magnets processed by spark plasma sintering and in-situ hot pressing of HDDR powder2009

    • Author(s)
      R. Gopalan, H. Sepehri-Amin, K. Suresh, T. Ohkubo, K. Hono, T. Nishiuchi, N. Nozawa and S. Hirosawa
    • Journal Title

      Scripta Mater

      Volume: 61 Pages: 978-981

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Anisotropic Nd-Fe-B nanocrystalline magnets processed by spark plasma sintering and in situ hot pressing of hydrogenation-decomposition-desorption-recombination powder2009

    • Author(s)
      R.Gopalan, 他7名
    • Journal Title

      Scripta Materialia 61

      Pages: 978-981

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Presentation] マルチスケール組織解析による保磁力発現機構の解明2011

    • Author(s)
      大久保忠勝
    • Organizer
      第35回日本磁気学会学術講演会
    • Place of Presentation
      新潟市朱鷺メッセ国際会議場(新潟県)
    • Year and Date
      2011-09-27
    • Related Report
      2011 Annual Research Report
  • [Presentation] Nd-Fe-B磁石における焼結後熱処理による磁気特性と組織変化2011

    • Author(s)
      大久保忠勝
    • Organizer
      日本顕微鏡学会第67回学術講演会
    • Place of Presentation
      福岡市福岡国際会議場(福岡県)(招待講演)
    • Year and Date
      2011-05-18
    • Related Report
      2011 Annual Research Report
  • [Presentation] Microstructure of fine grained high coercivity Nd-Fe-B sintered magnet2011

    • Author(s)
      大久保忠勝
    • Organizer
      InterMag 2011
    • Place of Presentation
      Taipei International Convention Center, Taipei,台湾(招待講演)
    • Year and Date
      2011-04-26
    • Related Report
      2011 Annual Research Report
  • [Presentation] FIB-SEM/TEM/3DAPによるNdFeB磁石のマルチスケール組織解析2011

    • Author(s)
      大久保忠勝
    • Organizer
      高性能磁石材料研究とナノ計測技術研究会
    • Place of Presentation
      新世代研究所,千代田区
    • Year and Date
      2011-01-12
    • Related Report
      2011 Final Research Report
  • [Presentation] FIB-SEM/TEM/3DAPによるNdFeB磁石のマルチスケール組織解析2011

    • Author(s)
      大久保忠勝
    • Organizer
      「高性能磁石材料研究とナノ計測技術」研究会
    • Place of Presentation
      (財)新世代研究所(東京都)
    • Year and Date
      2011-01-12
    • Related Report
      2010 Annual Research Report
  • [Presentation] マイクロマグネティクスシミュレーションによるNd-Fe-B焼結磁石磁化過程の検討2011

    • Author(s)
      大久保忠勝, H. Sepehri-Amin,宝野和博, T. Schrefl
    • Organizer
      日本金属学会2011年秋期(第149回)講演大会
    • Place of Presentation
      沖縄コンベンションセンター,那覇市
    • Related Report
      2011 Final Research Report
  • [Presentation] マルチスケール組織解析による保磁力発現機構の解明2011

    • Author(s)
      大久保忠勝, H. Sepehri-Amin,宝野和博
    • Organizer
      第35回日本磁気学会学術講演会
    • Place of Presentation
      朱鷺メッセ国際会議場,新潟市
    • Related Report
      2011 Final Research Report
  • [Presentation] Grain boundary and interface chemistry of a Dy-free Nd-Fe-B sintered magnet2011

    • Author(s)
      H. Sepehri-Amin, T. Ohkubo, T. Shima, K. Hono
    • Organizer
      The Magnetics Society of Japan(MSJ)
    • Place of Presentation
      朱鷺メッセ国際会議場,新潟市
    • Related Report
      2011 Final Research Report
  • [Presentation] Nd-Fe-B磁石における焼結後熱処理による磁気特性と組織変化2011

    • Author(s)
      大久保忠勝, H. Xiu, H. Sepehri-Amin,西内武司,広沢哲,宝野和博
    • Organizer
      日本顕微鏡学会第67回学術講演会
    • Place of Presentation
      福岡国際会議場,福岡市
    • Related Report
      2011 Final Research Report
  • [Presentation] Microstructure of fine grained high coercivity Nd-Fe-B sintered magnet2011

    • Author(s)
      T. Ohkubo, S. Hossein, Y. Une, K. Hono, M. Sagawa
    • Organizer
      InterMag 2011
    • Place of Presentation
      Taipei International Convention Center,台湾
    • Related Report
      2011 Final Research Report
  • [Presentation] FIB-SEM/TEM/3DAPによるマルチスケール組織解析2010

    • Author(s)
      大久保忠勝,宝野和博
    • Organizer
      日本顕微鏡学会マテリアル電子線トモグラフィ研究部会講演会
    • Place of Presentation
      工学院大学,新宿区
    • Year and Date
      2010-11-27
    • Related Report
      2011 Final Research Report
  • [Presentation] FIB-SEM/TEM/3DAPによるマルチスケール組織解析2010

    • Author(s)
      大久保忠勝
    • Organizer
      日本顕微鏡学会マテリアル電子線トモグラフィ研究部会講演会
    • Place of Presentation
      工学院大学(東京都)
    • Year and Date
      2010-11-27
    • Related Report
      2010 Annual Research Report
  • [Presentation] Dy拡散処理したNd-Fe-B焼結磁石のマルチスケール組織解析2010

    • Author(s)
      大久保忠勝
    • Organizer
      第34回日本磁気学会学術講演会
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Year and Date
      2010-09-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] Grain boundary structure and chemistry of Dy-containing and Dy-diffused Nd-Fe-B sintered magnets2010

    • Author(s)
      大久保忠勝
    • Organizer
      21st Workshop on Rare-Earth Permanent Magnets and their Applications (REPM'10)
    • Place of Presentation
      Bled(スロベニア)
    • Year and Date
      2010-08-31
    • Related Report
      2010 Annual Research Report
  • [Presentation] Mg-2.4at% Zn合金の時効硬化性に及ぼす微量添加元素の効果2010

    • Author(s)
      大石敬一郎, C. Mendis,大久保忠勝,宝野和博
    • Organizer
      2010日本金属学会秋期大会
    • Place of Presentation
      北海道大学,札幌市
    • Related Report
      2011 Final Research Report
  • [Presentation] Dy拡散処理したNd-Fe-B焼結磁石のマルチスケール組織解析2010

    • Author(s)
      大久保忠勝, H. Sepehri-Amin,宝野和博
    • Organizer
      第34回日本磁気学会学術講演会
    • Place of Presentation
      つくば国際会議場,つくば市
    • Related Report
      2011 Final Research Report
  • [Presentation] Grain boundary structure and chemistry of Dy-containing and Dy-diffused Nd-Fe-B sintered magnets2010

    • Author(s)
      T. Ohkubo, H. Sepehri-Amin, W. F. Li, K. Hono
    • Organizer
      REPM' 10
    • Place of Presentation
      Grand Hotel Toplice, Bled, Slovenia
    • Related Report
      2011 Final Research Report
  • [Presentation] 3D atom probe investigation of the microstructure evelution during the HDDR process of Nd_<12.5> Fe_<72.8> Co_<8.0> B_<6.5> Ga_<0.2> powder2010

    • Author(s)
      H. Sepehri-Amin, T. Ohkubo, T. Nishiuchi, S. Hirosawa, K. Hono
    • Organizer
      REPM' 10
    • Place of Presentation
      Grand Hotel Toplice, Bled, Slovenia
    • Related Report
      2011 Final Research Report
  • [Presentation] 短波長レーザーアトムプローブの開発と応用2010

    • Author(s)
      大久保忠勝,陳一萌,小塚雅也, F. Li,大石敬一郎,宝野和博
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋国際会議場,名古屋市
    • Related Report
      2011 Final Research Report
  • [Presentation] レーザーアトムプローブによる水素不均化Nd-Fe-B磁石合金中軽元素の定量解析2010

    • Author(s)
      大久保忠勝, H. Sepehri-Amin,西内武司,広沢哲,宝野和博
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋国際会議場,名古屋市
    • Related Report
      2011 Final Research Report
  • [Presentation] レーザー補助アトムプローブによるNd-Fe-B磁石粒界の組成解析2010

    • Author(s)
      大久保忠勝, H. Sepehri-Amin, W. F. Li,宝野和博,西内武司,広沢哲
    • Organizer
      日本金属学会2010年春期(第146回)大会
    • Place of Presentation
      筑波大学,つくば市
    • Related Report
      2011 Final Research Report
  • [Presentation] Multi-scale characterization of Nd-Fe-B permanent magnets2009

    • Author(s)
      大久保忠勝
    • Organizer
      2009 MRS Fall Meeting
    • Place of Presentation
      John B.Hynes Convention Center (Boston, USA)
    • Year and Date
      2009-11-30
    • Related Report
      2009 Annual Research Report
  • [Presentation] HDDR Nd-Fe-B系磁石のナノ組織形成過程2009

    • Author(s)
      大久保忠勝
    • Organizer
      日本金属学会2009年秋期(第145回)大会
    • Place of Presentation
      京都大学吉田キャンパス(京都府)
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] Multi-scale characterization of Nd-Fe-B permanent magnets2009

    • Author(s)
      T. Ohkubo, W. F. Li, H. Sepehri-Amin, K. Hono
    • Organizer
      2009 MRS Fall Meeting
    • Place of Presentation
      John B. Hynes Convention Center, Boston, USA
    • Related Report
      2011 Final Research Report
  • [Presentation] HDDR Nd-Fe-B系磁石のナノ組織形成過程2009

    • Author(s)
      大久保忠勝, H. Sepehri-Amin,宝野和博,西内武司,広沢哲
    • Organizer
      日本金属学会2009年秋期(第145回)大会
    • Place of Presentation
      京都大学吉田キャンパス,京都市
    • Related Report
      2011 Final Research Report
  • [Presentation] 短波長レーザー3DAPによるセラミックス材料の原子レベル組織解析2009

    • Author(s)
      大久保忠勝,陳一萌,小塚雅也,森田孝治,宝野和博
    • Organizer
      日本金属学会2009年秋期(第145回)大会
    • Place of Presentation
      京都大学吉田キャンパス,京都市
    • Related Report
      2011 Final Research Report
  • [Presentation] Grain orientation and magnetic properties of HDDR Nd-Fe-B magnets in-situ deformed during spark plasma sintering2009

    • Author(s)
      R. Gopalan, H. Sepehri-Amin, S. Koppoju, T. Ohkubo, K. Hono, T. Nishiuchi, S. Hirosawa
    • Organizer
      EUROMAT 2009
    • Place of Presentation
      The Scottish Exhibition and Conference Centre, Glasgow, UK
    • Related Report
      2011 Final Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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