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Development of ultrasonic atomic force microscopy for nondestructive evaluation of thin films

Research Project

Project/Area Number 21760577
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Material processing/treatments
Research InstitutionTohoku University

Principal Investigator

TSUJI Toshihiro  東北大学, 大学院・工学研究科, 助教 (70374965)

Project Period (FY) 2009 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2010: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2009: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Keywords超音波原子間力顕微鏡 / レーザー顕微鏡 / 剥離 / スパッタリング成膜 / スピンコート / ボールSAWセンサ / 感度 / 検出限界 / 燃料電池 / 水素ガス / 水蒸気 / 弾性表面波センサ / ZnO / Pt / マグネトロンスパッタリング / 原子間力顕微鏡
Research Abstract

Nondestructive evaluation of thin films with a thickness of sub-μm is required for development of high-performance devices. Since some sensitive films for surface acoustic wave gas sensor have a problem of delamination, I aimed to develop delamination-free sensitive films during sensor operation and verify the usefulness of the evaluation using ultrasonic atomic force microscopy and laser microscopy. As a result of the evaluation of the sensitivity of the sensors and the observation of the films, it was found that developed sensitive films were useful for highly sensitive sensor. Therefore, the purpose of this study was achieved.

Report

(3 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • Research Products

    (44 results)

All 2011 2010 2009 Other

All Journal Article (18 results) (of which Peer Reviewed: 10 results) Presentation (24 results) Remarks (2 results)

  • [Journal Article] Meandering collimated beam of surface acoustic waves on a trigonal crystal ball2011

    • Author(s)
      Takayuki Yanagisawa, Tsuneo Ohgi, Shingo Akao, Noritaka Nakaso, Yusuke Tsukahara, Yoshikazu Ohara, Toshihiro Tsuji, Kazushi Yamanaka
    • Journal Title

      Applied Physics Letters

      Volume: 98 Pages: 123508-123508

    • Related Report
      2010 Annual Research Report 2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] ボールSAWセンサによる極性ガスの高感度測定2011

    • Author(s)
      永井弘樹, 小峯和也, 吉野絢, 岩谷隆光, 坂本俊裕, 辻俊宏, 赤尾慎吾, 柳沢恭行, 大木恒郎, 中曽教尊, 山中一司
    • Journal Title

      圧電材料・デバイスシンポジウム2011講演論文集

      Pages: 121-126

    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Journal Article] 環境計測のためのボールSAWガスクロマトグラフシステム2011

    • Author(s)
      坂本俊裕, 吉野絢, 岩谷隆光, 永井弘樹, 小峯和也, 辻俊宏, 赤尾慎吾, 柳沢恭行, 大木恒郎, 中曽教尊, 山中一司
    • Journal Title

      圧電材料・デバイスシンポジウム2011講演論文集

      Pages: 127-128

    • Related Report
      2010 Annual Research Report
  • [Journal Article] 軸外スピンコート法で成膜した感応膜を用いる球状弾性表面波センサによる極性化合物の測定2010

    • Author(s)
      辻俊宏, 小峯和也, 永井弘樹, 坂本俊裕, 岩谷隆光, 赤尾慎吾, 柳沢恭行, 大木恒郎, 中曽教尊, 山中一司
    • Journal Title

      電子情報通信学会技術研究報告

      Volume: US2010-55 Pages: 39-44

    • NAID

      110008106814

    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Journal Article] Ball SAW gas chromatograph for detection of mixed VOC and FC gases2010

    • Author(s)
      Toshihiro Tsuji, Shohei Kawai, Hiroki Nagai, Toshihiro Sakamoto, Takamitsu Iwaya, Shingo Akao, Takayuki Yanagisawa, Tsuneo Ohgi, Noritaka Nakaso, Kazushi Yamanaka
    • Volume
      20
    • Related Report
      2010 Final Research Report
  • [Journal Article] Possibility for sub-ppm hydrogen detection with the ball SAW sensor2010

    • Author(s)
      Hiroki Nagai, Shohei Kawai, Osamu Ito, Toru Oizumi, Toshihiro Tsuji, Nobuo Takeda, Kazushi Yamanaka
    • Journal Title

      Proceedings of 20th International Congress on Acoustics

      Volume: 20

    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Journal Article] Development of Multiple-Gas Analysis Method Using the Ball Surface Acoustic Wave Sensor2010

    • Author(s)
      Yutaro Yamamoto, Shingo Akao, Hiroki Nagai, Toshihiro Sakamoto, Noritaka Nakaso, Toshihiro Tsuji , Kazushi Yamanaka
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 49(7)

    • NAID

      210000068876

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Development of Multiple-Gas Analysis Method Using the Ball Surface Acoustic Wave Sensor2010

    • Author(s)
      Yutaro Yamamoto, Shingo Akao, Hiroki Nagai, Toshihiro Sakamoto, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 49(7)

    • NAID

      210000068876

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ball SAW gas chromatograph for detection of mixed VOC and FC gases2010

    • Author(s)
      Toshihiro Tsuji, Shohei Kawai, Hiroki Nagai, Toshihiro Sakamoto, Takamitsu Iwaya, Shingo Akao, Takayuki Yanagisawa, Tsuneo Ohgi, Noritaka Nakaso, Kazushi Yamanaka
    • Journal Title

      Proceedings of 20th International Congress on Acoustics

      Volume: 20

    • Related Report
      2010 Annual Research Report
  • [Journal Article] ボールSAWセンサによるVOCおよび燃料電池関連ガスの計測2010

    • Author(s)
      辻俊宏, 河合祥平, 永井弘樹, 坂本俊裕, 岩谷隆光, 赤尾慎吾, 柳沢恭行, 大木恒郎, 中曽教尊, 山中一司
    • Journal Title

      日本音響学会2010年秋季研究発表会講演論文集

      Pages: 1437-1438

    • Related Report
      2010 Annual Research Report
  • [Journal Article] ボールSAWガスクロマトグラフのための金属カラムの開発2010

    • Author(s)
      岩谷隆光, 赤尾慎吾, 辻俊宏, 坂本俊裕, 中曽教尊, 山中一司
    • Journal Title

      日本音響学会2010年秋季研究発表会講演論文集

      Pages: 1439-1440

    • Related Report
      2010 Annual Research Report
  • [Journal Article] Development of ball SAW gas chromatograph with quantitative analysis of multiple hazard gases2010

    • Author(s)
      Toshihiro Sakamoto, Shingo Akao, Hiroki Nagai, Takamitsu Iwaya, Aya Yoshiho, Noritaka Naka Toshihiro Tsuji, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 31 Pages: 185-186

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Pressure Characteristics of Leaky Loss and Velocity on Ball SAW Device2010

    • Author(s)
      Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Toshiihro Tsuji, Omar Elmazria, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 31 Pages: 213-214

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development and Evaluation of Metal MEMS Column for the Ball SAW Gas Chromatograph2010

    • Author(s)
      Shingo Akao, Takamitsu Iwaya, Toshihiro Sakamoto, Hiroki Nagai, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 31 Pages: 453-454

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication of Thin Sensitive Film of Ball Surface Acoustic Wave Sensor by Off-Axis Spin-Coating Method2009

    • Author(s)
      Kentaro Kobari, Yutaro Yamamoto, Masanori Sakuma, Shingo Akao, Toshihiro Tsuji, Kazushi Yamanaka
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 48(7)

    • NAID

      210000067132

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Development of Packed Column for Surface Acoustic Wave Gas Chromatograph Using Anodically Bonded Silicon-Glass Structure with a Cmpression Jacket2009

    • Author(s)
      Y.Yamamoto, S.Akao, M.Samuka, K.Kobari, K.Noguchi, N.Nakaso, T.Tsuji, K.Yamanaka
    • Journal Title

      Japanese Journal of Applied Physics 48(7)

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication of Thin Sensitive Film of Ball Surface Acoustic Wave Sensor by Off-Axis Spin-Coating Method2009

    • Author(s)
      K.Kobari, Y.Yamamoto, M, Sakuma, S.Akao, T.Tsuji, K.Yamanaka
    • Journal Title

      Japanese Journal of Applied Physics 48(7)

    • NAID

      210000067132

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of Ball SAW Gas Chromatograph for Natural Gas Analysis2009

    • Author(s)
      S.Akao, Y.Yamamoto, H.Nagai, T.Ohgi, T.Yanagisawa, K.Okubata, H.Jige, T.Fukiura, N.Nakaso, T.Tsuji, K.Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics 30

      Pages: 79-80

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Presentation] ボールSAWガスクロマトグラフを用いた環境計測2011

    • Author(s)
      坂本俊裕, 吉野絢, 岩谷隆光, 永井弘樹, 小峯和也, 辻俊宏, 赤尾慎吾, 柳沢恭行, 大木恒郎, 中曽教尊, 山中一司
    • Organizer
      第58回応用物理学関係連合講演会
    • Place of Presentation
      厚木
    • Year and Date
      2011-03-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 可搬型ガスクロマトグラフのための金属MEMSカラムの開発2011

    • Author(s)
      岩谷隆光, 吉野絢, 赤尾慎吾, 坂本俊裕, 中曽教尊, 辻俊宏, 山中一司
    • Organizer
      第58回応用物理学関係連合講演会
    • Place of Presentation
      厚木
    • Year and Date
      2011-03-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] ボールSAWセンサによる極性ガスの高感度測定2011

    • Author(s)
      永井弘樹、小峯和也、吉野絢、岩谷隆光、坂本俊宏、辻俊宏、赤尾慎吾、柳沢恭行、大木恒郎、中曽教尊、山中一司
    • Organizer
      圧電材料・デバイスシンポジウム2011
    • Place of Presentation
      仙台
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] 環境計測のためのボールSAWガスクロマトグラフシステム2011

    • Author(s)
      坂本俊裕、吉野絢、岩谷隆光、永井弘樹、小峯和也、辻俊宏、赤尾慎吾、柳沢恭行、大木恒郎、中曽教尊、山中一司
    • Organizer
      圧電材料・デバイスシンポジウム2011
    • Place of Presentation
      仙台
    • Related Report
      2010 Annual Research Report
  • [Presentation] 多種類の危険・有害ガス分析のためのボールSAWガスクロマトグラフ2010

    • Author(s)
      坂本俊裕、赤尾慎吾、山本祐太郎、永井弘樹、岩谷隆光、中曽教尊、辻俊宏、山中一司
    • Organizer
      2010年春季 第57回応用物理学関係連合講演会
    • Place of Presentation
      神奈川・東海大学
    • Year and Date
      2010-03-17
    • Related Report
      2009 Annual Research Report
  • [Presentation] ボールSAWセンサを用いた多種類の危険・有害ガス分析法の開発2010

    • Author(s)
      山本祐太朗、赤尾慎吾、永井弘樹、坂本俊裕、岩谷隆光、中曽教尊、辻俊宏、山中一司
    • Organizer
      圧電材料・デバイスシンポジウム2010
    • Place of Presentation
      仙台・東北大学
    • Year and Date
      2010-02-02
    • Related Report
      2009 Annual Research Report
  • [Presentation] 軸外スピンコート法で成膜下感応膜を用いる球状弾性表面波センサによる極性化合物の測定2010

    • Author(s)
      辻俊宏、小峰和也、永井弘樹、坂本俊裕、岩谷隆光、赤尾慎吾、柳沢恭行、大木恒郎、中曽教尊、山中一司
    • Organizer
      電子情報通信学会超音波研究会
    • Place of Presentation
      仙台
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] ボールSAWセンサによるVOCおよび燃料電池関連ガスの計測2010

    • Author(s)
      辻俊宏、河合祥平、永井弘樹、坂本俊裕、岩谷隆光、赤尾慎吾、柳沢恭行、大木恒郎、中曽教尊、山中一司
    • Organizer
      日本音響学会2010年秋季研究発表会
    • Place of Presentation
      大阪
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] Ball SAW Gas Chromatograph for Detection of Mixed VOC and FC Gases2010

    • Author(s)
      Toshihiro Tsuji, Shohei Kawai, Hiroki Nagai, Toshihiro Sakamoto, Takamitsu Iwaya, Shingo Akao, Takayuki Yanagisawa, Tsuneo Ohgi, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      The 20th International Congress on Acoustics (ICA)
    • Place of Presentation
      オーストラリア シドニー
    • Related Report
      2010 Final Research Report
  • [Presentation] Possibility for Sub-ppm Hydrogen Detection with the Ball SAW Sensor2010

    • Author(s)
      Hiroki Nagai, Shohei Kawai, Osamu Ito, Toru Oizumi, Toshihiro Tsuji, Nobuo Takeda, Kazushi Yamanaka
    • Organizer
      The 20th International Congress on Acoustics (ICA)
    • Place of Presentation
      オーストラリア シドニー
    • Related Report
      2010 Final Research Report
  • [Presentation] Multiple Organic Gas Detection by the Ball Surface Acoustic Wave Sensor2010

    • Author(s)
      Kazushi Yamanaka, Toshihiro Sakamoto, Yutato Yamamoto, Kentaro Kobari, Toshihiro Tsuji, Shingo Akao, Noritaka Nakaso
    • Organizer
      International Academy, Research, and Industry Association(IARIA) The First International Conference on Sensor Device Technologies and Applications
    • Place of Presentation
      イタリア ヴェネツィア
    • Related Report
      2010 Final Research Report
  • [Presentation] Multiple Organic Gas Detection by the Ball Surface Acoustic Wave Sensor2010

    • Author(s)
      Kazushi Yamanaka, Toshihiro Sakamoto, Yutato Yamamoto, Kentaro Kobari, Toshihiro Tsuji, Shingo Akao, Noritaka Nakaso
    • Organizer
      International Academy, Research, and Industry Association (IARIA) The First International Conference on Sensor Device Technologies and Applications
    • Place of Presentation
      イタリアヴェネツィア
    • Related Report
      2010 Annual Research Report
  • [Presentation] Possibility for Sub-ppm Hydrogen Detection with the Ball SAW Sensor2010

    • Author(s)
      Hiroki Nagai, Shohei Kawai, Osamu Ito, Toru Oizumi, Toshihiro Tsuji, Nobuo Takeda, Kazushi Yamanaka
    • Organizer
      The 20th International Congress on Acoustics (ICA)
    • Place of Presentation
      オーストラリアシドニー
    • Related Report
      2010 Annual Research Report
  • [Presentation] Ball SAW Gas Chromato graph for Detection of Mixed VOC and FC Gases2010

    • Author(s)
      Toshihiro Tsuji, Shohei Kawai Hiroki Nagai, Toshihiro Sakamoto, Takamitsu Iwaya, Shingo Akao, Takayuki Yanagisawa, Tsuneo Ohgi, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      The 20th International Congress on Acoustics (ICA)
    • Place of Presentation
      オーストラリアシドニー
    • Related Report
      2010 Annual Research Report
  • [Presentation] ボールSAWガスクロマトグラフのための金属カラムの開発2010

    • Author(s)
      岩谷隆光、坂本俊裕、辻俊宏、赤尾慎吾、中曽教尊、山中一司
    • Organizer
      日本音響学会2010年秋季研究発表会
    • Place of Presentation
      大阪
    • Related Report
      2010 Annual Research Report
  • [Presentation] Ball SAW Gas Chromatograph for Automatic Analysis of Wide Variety of Gases2010

    • Author(s)
      Toshihiro Sakamoto, Shingo Akao, Hiroki Nagai, Takamitsu Iwaya, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      2010 IEEE International Ultrasonic Symposium (IUS)
    • Place of Presentation
      アメリカサンディエゴ
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development and Evaluate of Metal MEMS Column for the Ball SAW Gas Chromatograph2010

    • Author(s)
      Shingo Akao, Takamitsu Iwaya, Toshihiro Sakamoto, Hiroki Nagai, Toshihiro Tsuji, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      2010 IEEE International Ultrasonic Symposium (IUS)
    • Place of Presentation
      アメリカサンディエゴ
    • Related Report
      2010 Annual Research Report
  • [Presentation] Developenient of Ball SAW Gas Chromatograph with Quantitative Analysis of Multiple Hazard Gases2010

    • Author(s)
      Toshihiro Sakamoto, Shingo Akao, Hiroki Nagai, Takamitsu Iwaya, Aya Yoshino, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      第31回超音波エレクトロニクスの基礎と応用に関するシンポジウムUSE2010
    • Place of Presentation
      東京
    • Related Report
      2010 Annual Research Report
  • [Presentation] Pressure Characteristics of Leaky Loss and Velocity on Ball SAW Device2010

    • Author(s)
      Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Toshihiro Tsuji, Omar Elmazria, Kazushi Yamanaka
    • Organizer
      第31回超音波エレクトロニクスの基礎と応用に関するシンポジウムUSE2010
    • Place of Presentation
      東京
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development and Evaluation of Metal MEMS Column for the Ball SAW Gas Chromatograph2010

    • Author(s)
      Shingo Akao, Takamitsu Iwaya, Toshihiro Sakamoto, Hiroki Nagai, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      第31回超音波エレクトロニクスの基礎と応用に関するシンポジウムUSE2010
    • Place of Presentation
      東京
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development of Ball SAW Gas Chromatograph for Natural Gas Analysis2009

    • Author(s)
      S.Akao, Y.Yamamoto, H.Nagai, T.Ohgi, T.Yanagisawa, K.Okubata, H.Jige, T.Fukiura, N.Nakaso, T.Tsuji, K.Yamanaka
    • Organizer
      第30回超音波エレクトロニクスの基礎と応用に関するシンポジウム
    • Place of Presentation
      京都・同志社大学
    • Year and Date
      2009-11-19
    • Related Report
      2009 Annual Research Report
  • [Presentation] Development of Ball SAW Gas Chromatograph for Natural Gas Components2009

    • Author(s)
      山本祐太朗, 赤尾慎吾, 永井弘樹, 中曽教尊, 辻俊宏, 山中一司
    • Organizer
      IEEE International Ultrasonic Symposium
    • Place of Presentation
      イタリア・ローマ
    • Year and Date
      2009-09-23
    • Related Report
      2009 Annual Research Report
  • [Presentation] Separation and Measurement of Mixed Hazardous Gases by Ball SAW Gas Chromatograph with Sensitive Film Fabricated Using Off-Axis Spin-Coating2009

    • Author(s)
      T.Tsuji, Y.Kawai, K.Kobari, Y.Yamamoto, S.Akao, N.Nakaso, K.Yamanaka
    • Organizer
      IEEE International Ultrasonic Symposium
    • Place of Presentation
      イタリア・ローマ
    • Year and Date
      2009-09-23
    • Related Report
      2009 Annual Research Report
  • [Presentation] Separation and Measurement of Mixed Hazardous Gases by Ball SAW Gas Chromatograph with Sensitive Film Fabricated Using Off-Axis Spin-Coating2009

    • Author(s)
      Toshihiro Tsuji, Yuki Kawai, Kentaro Kobari, Yutaro Yamamoto, Shingo Akao, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      IEEE International Ultrasonic Symposium
    • Place of Presentation
      イタリアローマ
    • Related Report
      2010 Final Research Report
  • [Remarks]

    • URL

      http://www.material.tohoku.ac.jp/~hyoka/database_year_j.html

    • Related Report
      2010 Final Research Report
  • [Remarks]

    • URL

      http://www.material.tohoku.ac.jp/~hyoka/database_year_j.html

    • Related Report
      2010 Annual Research Report

URL: 

Published: 2009-04-01   Modified: 2016-04-21  

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