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Fretting behaviors and mechanism of biomedical materials in artificial body fluid

Research Project

Project/Area Number 21791944
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Dental engineering/Regenerative dentistry
Research InstitutionUniversity of Hyogo (2011)
Nagoya Institute of Technology (2009-2010)

Principal Investigator

MIURA Eri  兵庫県立大学, 大学院・工学研究科, 准教授 (70315258)

Co-Investigator(Renkei-kenkyūsha) SATO Hisashi  名古屋工業大学, 大学院・工学研究科, 准教授 (50402649)
Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2011: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2010: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2009: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Keywords生体材料学 / 生体材料 / 摩擦磨耗 / フレッティング / 歯科理工学 / 材料変形 / 摩擦摩耗
Research Abstract

Fretting wear behaviors of biomedical Ti alloys in artificial body fluid were investigated. We made special equipment with a micro-amplitude reciprocating heat stage for the measurement, α,β, and α+β type Ti alloys were tested. Counterface was ZrO_2 ball, and frictional test was carried out in Hank's solution, artificial saliva, and pure water at 37℃. Frictional coefficient. duration time curves were qualitatively similar among them. As compared with a sliding frictional behavior, frictional coefficient by fretting wear was seems to be constant and did not change very much during entire fretting cycle. According to wear surface observation by a scanning electron microscopy, adhesive wear was dominant throughout the applied fretting condition. Wear and tear was not observed on ZrO_2 ball, and Zr was not detected on the wear surface.
As the results of fretting test on CP Ti and Ti-Mo-Zr-Al alloy(TMZA) which has αphase and βphase, respectively, both frictional coefficient and specific wear rate in TMZA were higher than CP Ti. Wear surface morphology observed by SEM indicated that surface fatigue occurred by fretting wear in either Hank's solution or pure water, and an asperity generated by exfoliation was observed. In addition, the surface exfoliation in TMZA was more obvious than that in CP Ti. Therefore, it is suggested that increasing asperity due to surface fatigue increased frictional coefficient and specific wear rate of the alloys. Chemical composition analysis by AES and EPMA suggested that surface damage including exfoliation was related to strength and saturation of oxygen of materials.

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (10 results)

All 2011 2010 2009

All Journal Article (2 results) (of which Peer Reviewed: 1 results) Presentation (5 results) Patent(Industrial Property Rights) (3 results)

  • [Journal Article] 摩擦摩耗による特異ナノ構造層の形成挙動2011

    • Author(s)
      佐藤尚, 三浦永理, 渡辺義見
    • Journal Title

      まてりあ

      Volume: 50(8) Pages: 331-338

    • NAID

      10029298072

    • Related Report
      2011 Final Research Report
  • [Journal Article] Fabrication of Ti-based Biodegradable Material Composites Prepared by Spark Plasma Sintering Method2010

    • Author(s)
      E.Miura-Fujiwara, T.Teramoto, H.Sato, E.Kobayashi, Y.Watanabe
    • Journal Title

      Materials Science Forum

      Volume: 654-656 Pages: 2158-2161

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] Fabrication of Ti-based Biodegradable Material Composites Prepared by Spark Plasma Sintering Method2010

    • Author(s)
      E.Miura-Fujiwara, T.Teramoto, H.Sato, E.Kobayashi, Y.Watanabe
    • Organizer
      7th Pacific Rim Int.Conf.on Advanced Materials and Processing
    • Place of Presentation
      Cairns Convention Centre, Cairns, Queensland, AUS
    • Year and Date
      2010-08-04
    • Related Report
      2010 Annual Research Report
  • [Presentation] Wear Properties of Single Phase Ti Alloys and Surface Damage Characterization by X-Ray Diffraction2010

    • Author(s)
      Eri Mirua-Fujiwara, G.Ice, H.Sato, Y.Watanabe
    • Organizer
      2010 TMS Annual Meeting & Exhibition
    • Place of Presentation
      Washington State Convention Center, Seattle, WA, USA
    • Year and Date
      2010-02-17
    • Related Report
      2009 Annual Research Report
  • [Presentation] Wear Properties of Single Phase Ti Alloys and Surface Damage Characterization by X-Ray Diffraction2010

    • Author(s)
      Eri Miura-Fujiwara, G. E. Ice, H. Sato, Y. Watanabe
    • Organizer
      TMS Annual Meeting & Exhibition, Symposium
    • Place of Presentation
      Seattle, WA, USA
    • Related Report
      2011 Final Research Report
  • [Presentation] β型Ti合金疑似体液中でのスライディング摩耗特性2009

    • Author(s)
      三浦永理Wenjun.Liu, Gene E.Ice, 佐藤尚, 渡辺義見
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      京都大学吉田キャンパス
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] β型Ti合金の疑似体液中でのスライディング摩耗特性2009

    • Author(s)
      三浦永理, Wenjun. Liu, Gene E. Ice, 佐藤尚, 渡辺義見
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      京都大学吉田キャンパス
    • Related Report
      2011 Final Research Report
  • [Patent(Industrial Property Rights)] 摩耗量の評価方法2011

    • Inventor(s)
      三浦永理,寺本武司,渡辺義見,佐藤尚
    • Industrial Property Rights Holder
      国立大学法人名古屋工業大学
    • Filing Date
      2011-03-31
    • Related Report
      2011 Final Research Report
  • [Patent(Industrial Property Rights)] 摩耗量の評価方法2011

    • Inventor(s)
      三浦永理, 寺本武司, 渡辺義見, 佐藤尚
    • Industrial Property Rights Holder
      名古屋工業大学
    • Industrial Property Number
      2011-079980
    • Filing Date
      2011-03-31
    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] 複合材料の製造方法および医療用複合材料2010

    • Inventor(s)
      三浦永理, 寺本武司, 渡辺義見, 佐藤尚
    • Industrial Property Rights Holder
      名古屋工業大学
    • Industrial Property Number
      2010-149283
    • Filing Date
      2010-06-30
    • Related Report
      2010 Annual Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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