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Simultaneous control of surface microstructure and residual stress using solid solution of tool elements during friction stir processing

Research Project

Project/Area Number 21K14438
Research Category

Grant-in-Aid for Early-Career Scientists

Allocation TypeMulti-year Fund
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionOsaka University

Principal Investigator

Yamamoto Hajime  大阪大学, 接合科学研究所, 助教 (00842577)

Project Period (FY) 2021-04-01 – 2024-03-31
Project Status Completed (Fiscal Year 2023)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2023: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2022: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2021: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords摩擦攪拌プロセス / 残留応力 / 表面合金化 / 残留オーステナイト / 超硬合金 / 摩耗 / マルテンサイト / ツール摩耗 / マルテンサイト変態 / 固溶強化 / メカニカルアロイング
Outline of Research at the Start

摩擦攪拌プロセス(FSP)は,高速回転させたツールを金属板に押し付けることで生じる摩擦熱と塑性変形を利用した表面改質手法である.鉄鋼材料のような高強度金属のFSPではツールの摩耗をしばしば伴うが,このときに施工部内へ分散されるツール構成元素は,その後の組織形成と材料特性に悪影響を及ぼすとされてきた.本研究では,そのツール摩耗を逆活用した鋼中への元素供給・強制固溶によって,施工面のマルテンサイト変態制御とそれに起因する圧縮残留応力付与を実現し,両機構の解明を通じて鉄鋼材料の高疲労強度化に資する新技術の確立を目指す.

Outline of Final Research Achievements

Friction stir processing (FSP) with the WC tool wear was conducted on the low-carbon steel plate to elucidate the mechanism of compressive residual stress applied to the FSPed steel surface, alloyed with the tool constituent elements. The alloyed topmost layers in the stir zone consisted of martensite structures with small amount of retained austenite grains. The residual stresses applied to the stir zone surface depended on the alloying contents and the related martensite start temperature (Ms). The compressive residual stresses can be maximized at the Ms of about 150°C due to the martensitic transformation expansion near room temperature. Further decreasing Ms below about 150°C resulted in applying tensile residual stresses and increasing volume fraction of retained austenite. This suggests that martensitic transformation expansion near room temperature is insufficient for applying compressive residual stress.

Academic Significance and Societal Importance of the Research Achievements

FSPによる疲労強度改善の事例として,き裂発生起点となる欠陥や粗大析出物の除去を目的とした鋳造合金や積層造形部材への適用は多数みられるが,ツール摩耗による元素供給を利用した改善は本研究が初である.当該プロセスでは基板表面への元素添加と焼入れが同時に施されるため,炭素量や合金元素の少ない加工性を重視した軟鋼に対しても,部分的に疲労特性を強化でき,構造設計上の材料選択における自由度の大幅な向上に貢献できると考えている.

Report

(4 results)
  • 2023 Annual Research Report   Final Research Report ( PDF )
  • 2022 Research-status Report
  • 2021 Research-status Report
  • Research Products

    (10 results)

All 2023 2022 2021

All Presentation (10 results) (of which Int'l Joint Research: 4 results)

  • [Presentation] Adapted to generate compressive residual stress and retained austenite in a steel surface layer by friction stir processing with the WC tool2023

    • Author(s)
      Hajime Yamamoto, Yuji Yamamoto, Kazuhiro Ito, Yoshiki Mikami
    • Organizer
      The 76th IIW Annual Assembly and International Conference on Welding and Joining
    • Related Report
      2023 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Alloying of low-carbon steel surface due to friction stir processing with WC tool wear2023

    • Author(s)
      Hajime Yamamoto, Yuji Yamamoto, Yudai Imagawa, Kazuhiro Ito, Yoshiki Mikami
    • Organizer
      The 3rd Materials Research Meeting (MRM2023) / The 24th IUMRS-International Conference in Asia (IUMRS-ICA2023)
    • Related Report
      2023 Annual Research Report
    • Int'l Joint Research
  • [Presentation] WCツール摩擦攪拌プロセスにより生成された残留γの疲労き裂進展抵抗への寄与2023

    • Author(s)
      山本 啓, 山元優士, 伊藤和博
    • Organizer
      一般社団法人 溶接学会 2023年度春季全国大会
    • Related Report
      2023 Annual Research Report
  • [Presentation] 摩擦攪拌プロセス中の荷重低減とそのWCツール元素固溶量への影響2023

    • Author(s)
      柳 悠輔, 山本 啓, 伊藤和博
    • Organizer
      一般社団法人 溶接学会 2023年度秋季全国大会
    • Related Report
      2023 Annual Research Report
  • [Presentation] 摩擦攪拌プロセス中の荷重低減とそのWCツール元素固溶量への影響2023

    • Author(s)
      山本 啓, 柳 悠輔, 伊藤和博
    • Organizer
      公益社団法人 日本金属学会 2023年秋期(第173回)講演大会
    • Related Report
      2023 Annual Research Report
  • [Presentation] Surface alloying due to WC tool wear during FSP and its effects on the microstructure and mechanical properties of topmost steel layer2023

    • Author(s)
      Hajime Yamamoto, Yudai Imagawa, Yuji Yamamoto, Kazuhiro Ito
    • Organizer
      TMS 2023 152nd Annual Meeting & Exhibition
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research
  • [Presentation] Addition of compressive residual stress and retained austenite in steel surface layers by friction stir processing with the WC tool2022

    • Author(s)
      Hajime Yamamoto, Yuji Yamamoto, Kazuhiro Ito, Yoshiki Mikami
    • Organizer
      The 6th International Symposium on Visualization in Joining & Welding Science through Advanced Measurements and Simulation (Visual-JW 2022)
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research
  • [Presentation] WCツール摩擦攪拌プロセスによる鋼表層への圧縮残留応力と残留オーステナイトの付与2022

    • Author(s)
      柳 悠輔, 山元優士, 山本 啓, 伊藤和博, 三上欣希
    • Organizer
      一般社団法人 溶接学会 2022年度秋季全国大会
    • Related Report
      2022 Research-status Report
  • [Presentation] WCツール摩擦攪拌プロセスにより鋼表層に生じる圧縮残留応力と残留オーステナイト2022

    • Author(s)
      山本 啓*, 山元優士, 伊藤和博, 三上欣希
    • Organizer
      公益社団法人 日本金属学会 2022年秋期(第171回)講演大会
    • Related Report
      2022 Research-status Report
  • [Presentation] 摩擦攪拌プロセス施工鋼表層の残留応力とWCツール構成元素固溶量との関係2021

    • Author(s)
      山元優士, 山本 啓, 伊藤和博, 三上欣希
    • Organizer
      一般社団法人 溶接学会 2021年度秋季全国大会
    • Related Report
      2021 Research-status Report

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Published: 2021-04-28   Modified: 2025-01-30  

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