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Evaluation of oxidation rates of heat resistant materials for re-entryspace vehicles

Research Project

Project/Area Number 22360283
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Physical properties
Research InstitutionJapan Aerospace Exploration Agency

Principal Investigator

HATTA Hiroshi  独立行政法人宇宙航空研究開発機構, 宇宙科学研究所, 教授 (90095638)

Co-Investigator(Kenkyū-buntansha) YOSHINAKA Toshinari  独立行政法人宇宙航空研究開発機構, 航空本部, 主任開発員 (40526266)
桃沢 愛  東京都市大学, 工学部, 講師 (70575597)
Co-Investigator(Renkei-kenkyūsha) MOMOZAWA Ai  東京都市大学, 工学部, 講師研究者番号:705755597 (70575597)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥18,590,000 (Direct Cost: ¥14,300,000、Indirect Cost: ¥4,290,000)
Fiscal Year 2012: ¥6,500,000 (Direct Cost: ¥5,000,000、Indirect Cost: ¥1,500,000)
Fiscal Year 2011: ¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2010: ¥7,150,000 (Direct Cost: ¥5,500,000、Indirect Cost: ¥1,650,000)
Keywordsマトリックス材 / SiC / 酸化 / Active-Passive転移 / ZrB2-SiC / 酸化数値計算 / SiO2膜成長 / 大気圏再突入 / 酸化抑制効果 / 宇宙往還機 / 再使用型 / 耐熱材料 / 参加試験 / 試験方法 / 酸化試験 / 試験手法
Research Abstract

In order to establish quantitative estimation technology to measure oxidation rates of high temperature materials, this study has clarified that it is required to determine partial pressure of oxygen on the surface of the materials PO2-s. To demonstrate this assertion, procedures to determine PO2-ss in thermo-balances have developed for the active and passive oxidation behaviors of SiC, which has been used in reusable spaces vehicles. Next, oxidation behaviors of ZrB2-SiC were examined.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (28 results)

All 2013 2012 2011 2010 2009 Other

All Journal Article (6 results) (of which Peer Reviewed: 3 results) Presentation (22 results)

  • [Journal Article] Use of Volume Element Methods to Understand Experimental Differences in Active/Passive Transitions and Active Oxidation Rates for SiC2013

    • Author(s)
      Y. Kubota, H. Hatta, T. Yoshinaka, Y. Kogo, T.Goto, and T. Rong
    • Journal Title

      J. Am. Ceram. Soc. WILEY

      Volume: Vol. 96 Pages: 1317-1323

    • Related Report
      2012 Final Research Report
  • [Journal Article] Use of volume element methods to understand experimental differences in active/passive transition and active oxidation rates for SiC2013

    • Author(s)
      Yuki.Kubota
    • Journal Title

      Journal of American Ceramic Society

      Volume: 96 Pages: 1317-1323

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative evaluation of the oxidation behavior of ZrB2-15 vol.%SiC at a low oxygen partial pressure2012

    • Author(s)
      A. Momozawa, T. Rong, T. Goto, Y. Kubota, H. Hatta and K. Komurasaki
    • Journal Title

      Vacuum, ELSEVIER

      Volume: Vol. 88 Pages: 98-102

    • Related Report
      2012 Final Research Report
  • [Journal Article] Quantitative evaluation of the oxidation behavior of ZrB2-15 vol.%SiC at a low oxygen partial pressure2012

    • Author(s)
      Ai.Momozawa
    • Journal Title

      Vacuum

      Volume: 88 Pages: 98-102

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Oxidation Behavior of ZrB2-15vol.%SiC at an Oxygen Partial Pressure of 57 Pa2011

    • Author(s)
      A. Momozawa, Y. Kubota, T. Rong, T. Goto, K. Takagi, K. Komurasaki and H. Hatta
    • Journal Title

      Key Engineering Materials, SCOPUS

      Volume: Vol. 484 Pages: 21-25

    • Related Report
      2012 Final Research Report
  • [Journal Article] Oxidation test of ZrB2-SiC composites using an arc-heater Ai Momozawa2011

    • Author(s)
      Ai Momozawa, Yuuki Kubota, Rong Tu, Takashi Goto, Ken-Ichi Takagi, Kimiya Komurasaki, Hiroshi Hatta
    • Journal Title

      Key Engineering Materials

      Volume: 484 Pages: 21-25

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] Evaluation of Passive and Active Oxidation Transition of CVD-SiC by Numerical Calculation2012

    • Author(s)
      Toshinari.Yoshinaka
    • Organizer
      The American Institute of Aeronautics and Astronautics
    • Place of Presentation
      New Oreleans
    • Related Report
      2012 Annual Research Report
  • [Presentation] Oxidation tests on ZrB2-SiC Composites Using an Arc-Heater2011

    • Author(s)
      A. Momozawa, Y. Kubota, H. Hatta, and K. Komurasaki
    • Organizer
      4th Inter. Workshop Plasma Appli. & Hybrid Functionally Materials
    • Place of Presentation
      Melbourne, Australia
    • Related Report
      2012 Final Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of SiC under Elevated Temperatures2011

    • Author(s)
      Y. Kubota, T. Yoshinaka, H. Hatta, T. Goto, Y. Kogo
    • Organizer
      Inter. Conf. Mater. Processing, 51093
    • Place of Presentation
      Oregon, USA
    • Related Report
      2012 Final Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of SiC under Elevated Temperatures2011

    • Author(s)
      Y. Kubota, T. Yoshinaka, H. Hatta, T. Goto, Y. Kogo;
    • Organizer
      18th Inter. Conf. Compos. Mate., F09-5
    • Place of Presentation
      Jeju, Korea
    • Related Report
      2012 Final Research Report
  • [Presentation] Oxidation tests on ZrB2-SiC Composites2011

    • Author(s)
      A. Momozawa, Y. Kubota, H. Hatta, and K. Komurasaki
    • Organizer
      5th Inter Symp Applied Plasma Science
    • Place of Presentation
      Hakone, Japan
    • Related Report
      2012 Final Research Report
  • [Presentation] Accurate quantitative evaluation of Active oxidation of SiC under elevated temperatures2011

    • Author(s)
      久保田勇希, 他
    • Organizer
      International conference on materials and processing
    • Place of Presentation
      済州島、韓国
    • Related Report
      2011 Annual Research Report
  • [Presentation] Accurate quantitative evaluation of Active oxidation of SiC under elevated temperatures2011

    • Author(s)
      久保田勇希, 他
    • Organizer
      International conference on composite materials
    • Place of Presentation
      オレゴン、アメリカ
    • Related Report
      2011 Annual Research Report
  • [Presentation] 宇宙往還機におけるSicコーティングの酸化挙動の定量的評価2010

    • Author(s)
      久保田有希, 他
    • Organizer
      日本機会学会
    • Place of Presentation
      東京
    • Year and Date
      2010-11-27
    • Related Report
      2010 Annual Research Report
  • [Presentation] Passive Oxidation and Oxidation Transition of CVD-SiC under High Temperature2010

    • Author(s)
      芳仲敏成, 他
    • Organizer
      International Congress oll Ceramic
    • Place of Presentation
      大阪
    • Year and Date
      2010-11-15
    • Related Report
      2010 Annual Research Report
  • [Presentation] Evaluation of the Oxidation Behavior of ZrB_2-SiC at Elevated Temperatures2010

    • Author(s)
      桃沢愛, 他
    • Organizer
      International Congress on Ceramics
    • Place of Presentation
      大阪
    • Year and Date
      2010-11-15
    • Related Report
      2010 Annual Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of sic under Elevated Temperatures2010

    • Author(s)
      久保田有希, 他
    • Organizer
      International Congress on Ceramics
    • Place of Presentation
      大阪
    • Year and Date
      2010-11-15
    • Related Report
      2010 Annual Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of SiC under Elevated Temperatures2010

    • Author(s)
      Y. Kubota, T. Yoshinaka, H. Hatta, T. Goto, and Y. Kogo
    • Organizer
      10th HTCMC, 052
    • Place of Presentation
      Bayreuth, Germany
    • Year and Date
      2010-05-02
    • Related Report
      2012 Final Research Report
  • [Presentation] Passive Oxidation and Oxidation Transition of CVD-SiC under High Temperatures2010

    • Author(s)
      T. Yoshinaka, Y. Kubota, T. Goto, H. Hatta
    • Organizer
      7th HTCMC, 045
    • Place of Presentation
      Bayreuth, Germany
    • Year and Date
      2010-04-05
    • Related Report
      2012 Final Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of SiC under Elevated Temperature2010

    • Author(s)
      Y. Kubota, T. Yoshinaka, H. Hatta, T. Goto, Y. Kogo
    • Organizer
      4th Inter. Symp. Adv. Ceram., S14-076
    • Place of Presentation
      Osaka, Japan
    • Related Report
      2012 Final Research Report
  • [Presentation] Oxidation behavior of ZrB2-15%SiC at an Oxygen Partial Pressure of 57 Pa2010

    • Author(s)
      A. Momozawa, Y. Kubota, Rong Tu, T. Goto, K Komurasaki, H. Hatta
    • Organizer
      4th Inter. Symp. Adv. Ceram., S14-075
    • Place of Presentation
      Osaka, Japan
    • Related Report
      2012 Final Research Report
  • [Presentation] Passive Oxidation and Oxidation Transition of CVD-SiC High Temp2010

    • Author(s)
      T. Yoshinaka, Y. Kubota, H. Hatta, T. Goto
    • Organizer
      4th Inter. Symp. Adv. Ceram., S14-077
    • Place of Presentation
      Osaka, Japan
    • Related Report
      2012 Final Research Report
  • [Presentation] 宇宙往還機におけるSiCコーティングの酸化挙動の定量的評価2010

    • Author(s)
      久保田勇希、芳仲敏成、八田博志、向後保雄、後藤孝、桃沢愛
    • Organizer
      日本機会学会第18回機会材料・材料加工技術講演会、106
    • Place of Presentation
      東京大学
    • Related Report
      2012 Final Research Report
  • [Presentation] Passive Oxidation and Oxidation Transition of CVD-SiC under High Temperature2010

    • Author(s)
      芳仲敏成, 他
    • Organizer
      High Temperature Ceramic Materials and Composites
    • Place of Presentation
      バイロイト、ドイツ
    • Related Report
      2010 Annual Research Report
  • [Presentation] Accurate Quantitative Evaluation of Active Oxidation Rate of SiC under Elevated Temperatures2010

    • Author(s)
      久保田有希, 他
    • Organizer
      High Temperature Ceramic Materials and Composites
    • Place of Presentation
      バイロイト、ドイツ
    • Related Report
      2010 Annual Research Report
  • [Presentation] 宇宙往還機におけるSiCコーティングの酸化挙動の定量的評価2009

    • Author(s)
      久保田勇希、芳仲敏成、八田博志、向後保雄,
    • Organizer
      第25回 宇宙構造材料シンポジウム, A2、
    • Place of Presentation
      宇宙科学研究所
    • Related Report
      2012 Final Research Report
  • [Presentation] Evaluation of Passive and Active Oxidation Transition of CVD-SiC by Numerical Calculation

    • Author(s)
      T. Yoshinaka, Y. Kubota, H. Hatta
    • Organizer
      AIAA-2012-3007
    • Related Report
      2012 Final Research Report
  • [Presentation] Oxidation test of ZrB2-SiC composites using an arc-heater Ai Momozawa

    • Author(s)
      A.Momozawa
    • Related Report
      2011 Annual Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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