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Electrochemical formation of self-organized porousstructures on metallic substrates in organic solvents and their application

Research Project

Project/Area Number 22360307
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionOsaka University

Principal Investigator

TSUCHIYA Hiroaki  大阪大学, 大学院・工学研究科, 准教授 (50432513)

Co-Investigator(Kenkyū-buntansha) FUJIMOTO Shinji  大阪大学, 大学院・工学研究科, 教授 (70199371)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥19,240,000 (Direct Cost: ¥14,800,000、Indirect Cost: ¥4,440,000)
Fiscal Year 2012: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Fiscal Year 2011: ¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2010: ¥11,570,000 (Direct Cost: ¥8,900,000、Indirect Cost: ¥2,670,000)
Keywords電気化学プロセス / ナノポーラス / ステンレス鋼 / コバルト・クロム合金 / チタン / バナジウム / 有機溶媒 / 生体適合性 / インコネル合金
Research Abstract

In the present work we have examined the electrochemical formation of porous surface on various metallic substrates in organic solvents and achieved the porosification of stainless steel, nickel-based alloys, cobalt chromium alloy and titanium surfaces in perchlorate ion containing organic solvents and vanadium in organic solvents containing sulfuric acid and hydrochloric acid. SEM observations and AFM analyses indicated that the morphology of porous structure depended on electrochemical conditions such as applied voltage and duration. Wealso found that the porosification of stainless steel surface can improve cell activity as well as corrosion resistance in a simulated body fluid

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (34 results)

All 2013 2012 2011 2010

All Journal Article (5 results) (of which Peer Reviewed: 4 results) Presentation (28 results) Book (1 results)

  • [Journal Article] Selective pore growth on lamellar Ti-41at.%Al alloy2013

    • Author(s)
      Hiroaki Tsuchiya, Toshifumi Akaki, Yuichiro Koizumi, Yoritoshi Minamino, Shinji Fujimoto
    • Journal Title

      Electrochemistry Communications

      Volume: Vol. 26 Pages: 117-120

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Selective pore growth on lamellar Ti-41at.Al alloy2013

    • Author(s)
      Hiroaki Tsuciya
    • Journal Title

      Electrochemistry Communicaitons

      Volume: 26 Pages: 117-120

    • DOI

      10.1016/j.elecom.2012.08.025

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of self-organized pores on type 316 stainless steel in organic solvents2012

    • Author(s)
      Hiroaki Tsuchiya, Takahiro Suzumura, Yoshiyuki Terada, Shinji Fujimoto
    • Journal Title

      Electrochica Acta

      Volume: Vol. 82 Pages: 333-338

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Formation of self-organized pores on type 316 stainless steel in organic solvents2012

    • Author(s)
      Hiroaki Tsuchiya
    • Journal Title

      Electrochimica Acta

      Volume: 82 Pages: 333-338

    • DOI

      10.1016/j.electacta.2012.06.048

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] バルブ金属・合金の陽極酸化によるポーラス酸化物層の創製2010

    • Author(s)
      土谷博昭、藤本慎司
    • Journal Title

      金属

      Volume: 80巻 Pages: 743-750

    • Related Report
      2012 Final Research Report 2010 Annual Research Report
  • [Presentation] 有機溶媒を用いた電解処理による金属・合金表面ポーラス化2012

    • Author(s)
      土谷博昭, 寺田圭徹, 鈴村貴大, 藤本慎司
    • Organizer
      電気化学会第79回大会
    • Place of Presentation
      アクトシティ浜松
    • Year and Date
      2012-03-31
    • Related Report
      2011 Annual Research Report
  • [Presentation] TiAlおよびTiFe合金のアノード分極挙動と酸化皮膜形態2012

    • Author(s)
      土谷博昭、黒住健太、中田淳二、藤本慎司
    • Organizer
      日本金属学会春季(第150回)講演大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] 有機溶媒電気化学プロセスによる金属・合金表面のナノポーラス化2012

    • Author(s)
      土谷博昭, 鈴村貴大, 寺田圭徹, 藤本慎司
    • Organizer
      表面技術協会第152回講演大会
    • Place of Presentation
      東京都市大学
    • Year and Date
      2012-03-13
    • Related Report
      2011 Annual Research Report
  • [Presentation] Electrochemical Formation of Ordered Pore Arrays on Metallic Substrates2012

    • Author(s)
      Hiroaki Tsuchiya, Min-Su Kim,Yoshiyuki Terada, Shinji Fujimoto
    • Organizer
      The 222nd Meeting of the Electrochemical Society
    • Place of Presentation
      Hawaii Honolulu
    • Related Report
      2012 Final Research Report
  • [Presentation] 電解処理によるバナジウムのナノホールアレイ形成2012

    • Author(s)
      寺田圭徹、土谷博昭、藤本慎司
    • Organizer
      日本金属学会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Final Research Report
  • [Presentation] Electrochemical Formation of Ordered Pore Arrays2012

    • Author(s)
      Hiroaki Tsuchiya, Takahiro Suzumura, Yoshiyuki Terada, Shinji Fujimoto
    • Organizer
      The 63rd Annual Meeting of the International Society of Electrochemistry
    • Place of Presentation
      Prague, Czech Republic.
    • Related Report
      2012 Final Research Report
  • [Presentation] Electrochemical Formation of Ordered Pore Arrays2012

    • Author(s)
      Hiroaki Tsuchiya
    • Organizer
      The 63rd Annual Meeting of the International Society of Electrochemisty
    • Place of Presentation
      Prague, Czech Republic
    • Related Report
      2012 Annual Research Report
  • [Presentation] アノード分極による生体用金属材料表面のナノポーラス化2012

    • Author(s)
      土谷博昭
    • Organizer
      日本金属学会秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 電解処理によるバナジウムのナノホールアレイ形成2012

    • Author(s)
      土谷博昭
    • Organizer
      日本金属学会秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 陽極酸化TiO2ナノチューブ層形成に及ぼす基板熱処理および加工の影響2012

    • Author(s)
      土谷博昭
    • Organizer
      日本金属学会秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 陽極酸化によるTi表面ポーラス化2012

    • Author(s)
      土谷博昭
    • Organizer
      日本金属学会秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 陽極酸化による生体用金属材料の表面改質と 生体適合性評価2012

    • Author(s)
      土谷博昭
    • Organizer
      表面技術協会
    • Place of Presentation
      室蘭工業大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Electrochemical Formation of Ordered Pore Arrays on Metallic Substrates2012

    • Author(s)
      Hiroaki Tsuchiya
    • Organizer
      222nd Meeting of the Electrochemical Society
    • Place of Presentation
      Hawaii, Honolulu
    • Related Report
      2012 Annual Research Report
  • [Presentation] Formation of ordered pore arrays by self-organizing electrochemical treatments2011

    • Author(s)
      H.Tsuchiya, T.Suzumura, Y.Terada, S.Fujimoto
    • Organizer
      ECO-MATES2011
    • Place of Presentation
      Hotel Hankyu Expo Park, Osaka
    • Year and Date
      2011-11-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] 電気化学プロセスによる金属・合金表面のナノポーラス化2011

    • Author(s)
      土谷博昭, 鈴村貴大, 寺田圭徹, 藤本慎司
    • Organizer
      日本金属学会秋季(第149回)講演大会
    • Place of Presentation
      沖縄コンベンションセンター
    • Year and Date
      2011-11-07
    • Related Report
      2011 Annual Research Report
  • [Presentation] Formation of Ordered Pore Arrays on Stainless Steels2011

    • Author(s)
      H.Tsuchiya, T.Suzumura, S.Fujimoto
    • Organizer
      220^<th> Meeting of The Electrochemical Society
    • Place of Presentation
      The Boston Convention and Exhibition Center
    • Year and Date
      2011-10-10
    • Related Report
      2011 Annual Research Report
  • [Presentation] Biocompatibility of nano-structured TiO2 surfaces2011

    • Author(s)
      H.Tsuchiya, K.Tamura, S.Miyabe, P.Schmuki, S.Fujimoto
    • Organizer
      220^<th> Meeting of The Electrochemical Society
    • Place of Presentation
      The Boston Convention and Exhibition Center
    • Year and Date
      2011-10-10
    • Related Report
      2011 Annual Research Report
  • [Presentation] 有機溶媒電気化学プロセスによるステンレス鋼のポーラス化2011

    • Author(s)
      土谷博昭, 鈴村貴大, 藤本慎司
    • Organizer
      日本鉄鋼協会第162回秋季講演大会
    • Place of Presentation
      大阪大学
    • Year and Date
      2011-09-20
    • Related Report
      2011 Annual Research Report
  • [Presentation] バルブ金属・合金上へのポーラス酸化物皮膜の形成-基板組織・組成に着目して-2011

    • Author(s)
      土谷博昭
    • Organizer
      金属のアノード酸化皮膜の機能化部会(ARS)例会
    • Place of Presentation
      工学院大学
    • Year and Date
      2011-09-16
    • Related Report
      2012 Final Research Report
  • [Presentation] バルブ金属・合金上へのポーラス酸化物皮膜の形成-基板組織・組成に着目して-2011

    • Author(s)
      土谷博昭
    • Organizer
      金属のアノード酸化皮膜の機能化部会(ARS)例会
    • Place of Presentation
      工学院大学(招待講演)
    • Year and Date
      2011-09-16
    • Related Report
      2011 Annual Research Report
  • [Presentation] チタン表面へのポーラス酸化皮膜の形成2011

    • Author(s)
      土谷博昭
    • Organizer
      軽金属学会関西支部「関西軽金属サマースクール」
    • Place of Presentation
      京都大学
    • Year and Date
      2011-09-15
    • Related Report
      2012 Final Research Report
  • [Presentation] チタン表面へのナノポーラス酸化皮膜の形成2011

    • Author(s)
      土谷博昭
    • Organizer
      軽金属学会関西支部「関西軽金属サマースクール」
    • Place of Presentation
      京都大学(招待講演)
    • Year and Date
      2011-09-15
    • Related Report
      2011 Annual Research Report
  • [Presentation] Formation of Ordered Pore Arrays on Stainless Steels2011

    • Author(s)
      Hiroaki Tsuchiya, Takahiro Suzumura, Shinji Fujimoto
    • Organizer
      The 220th Meeting of The Electrochemical Society
    • Place of Presentation
      Boston, MA.
    • Related Report
      2012 Final Research Report
  • [Presentation] Formation of Self-organized Pores on Fe-Cr Alloys2010

    • Author(s)
      H.Tsuchiya, T.Suzumura, S.Fujimoto
    • Organizer
      218^<th> Meeting of The Electrochemical Society
    • Place of Presentation
      Riviera Hotel(LasVegas)
    • Year and Date
      2010-10-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] 電気化学プロセスによるFe-Cr合金表面へのナノサイズ孔の形成2010

    • Author(s)
      土谷博昭、鈴村貴大、藤本慎司
    • Organizer
      日本金属学会
    • Place of Presentation
      北海道大学(札幌)
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] 有機溶媒中での電解プロセスによる金属・合金表面のナノポーラス化2010

    • Author(s)
      鈴村貴大、土谷博昭、藤本慎司
    • Organizer
      日本金属学会
    • Place of Presentation
      北海道大学(札幌)
    • Year and Date
      2010-09-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] 電気化学プロセスによるポーラス・ステンレス鋼表面の創製2010

    • Author(s)
      土谷博昭、鈴村貴大、藤本慎司
    • Organizer
      表面技術協会
    • Place of Presentation
      東北大学(仙台)
    • Year and Date
      2010-09-07
    • Related Report
      2010 Annual Research Report
  • [Presentation] 有機溶媒中での電解処理によるSUS316ステンレス鋼表面のナノポーラス化2010

    • Author(s)
      鈴村貴大、土谷博昭、藤本慎司
    • Organizer
      電気化学会
    • Place of Presentation
      神奈川工科大学(厚木)
    • Year and Date
      2010-09-03
    • Related Report
      2010 Annual Research Report
  • [Book] Advanced Materials Design by Electrochemical Approach :Self-Organizing Anodization, Progress in Advanced Structural and Functional Materials Design2013

    • Author(s)
      Hiroaki Tsuchiya
    • Publisher
      Springer
    • Related Report
      2012 Final Research Report

URL: 

Published: 2010-08-23   Modified: 2019-07-29  

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