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Automatic separation technique of ultra-trace multi-elements to analyze the origin of trace environmental materials

Research Project

Project/Area Number 22550143
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Environmental chemistry
Research InstitutionJapan Atomic Energy Agency

Principal Investigator

MIYAMOTO Yutaka  独立行政法人日本原子力研究開発機構, 原子力基礎工学研究部門, 研究副主幹 (60219821)

Co-Investigator(Renkei-kenkyūsha) YASUDA Kenichiro  独立行政法人日本原子力研究開発機構, 原子力基礎工学研究部門, 研究副主幹 (20354871)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2012: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2011: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2010: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Keywordsミクロ化学手法 / イオン交換分離 / 環境試料 / ウラン / 鉛 / トリウム / イオン交換分離法 / 極微量分析 / ランタノイド
Research Abstract

The objective of this study is to develop an automatic separation technique of ultra-trace multi-elements. The experimental conditions of sequential separation with a single anion-exchange column were optimized. An automatic separation system was assembled. A reference environmental sample was separated and quantitatively analyzed with the optimized system, and the features of this system were evaluated. The elements of interest were sequentially and completely separated within 6 hours. The chemical recovery yield was more than 95%. This evaluation suggests that a sample in more than 500 micro grams (equivalent to several micro meters in diameter) of sample can be analyzed.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (9 results)

All 2012 2011 2010

All Journal Article (1 results) Presentation (8 results)

  • [Journal Article] 極微量元素イオン交換逐次分離法の自動化に向けた分離条件の検討2010

    • Author(s)
      宮本ユタカ、安田健一郎、間柄正明、木村貴海
    • Journal Title

      Journal of Nuclear and Radiochemical Sciences

      Volume: Vol.11 Pages: 151-151

    • Related Report
      2012 Final Research Report 2010 Annual Research Report
  • [Presentation] 環境試料極微量分析のための逐次化学分離法2012

    • Author(s)
      宮本、安田、間柄、木村
    • Organizer
      京都大学原子炉実験所専門研究会「放射化分析を用いた微量元素分析の現状」
    • Place of Presentation
      京都大学原子炉実験所(熊取)
    • Year and Date
      2012-02-01
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] Sequential separation of ultra-trace U, Th, Pb, and Lanthanides with a single anion-exchange column2012

    • Author(s)
      Y.Miyamoto, K.Yasuda, M.Magara, T.Kimura
    • Organizer
      EuCheMS 8th International Conference on Nuclear and Radiochemistry (NRC8)
    • Place of Presentation
      コモ(イタリア)
    • Related Report
      2012 Final Research Report
  • [Presentation] Sequential separation of ultra-trace U, Th, Pb, and Lanthanides with a single anion-exchange column2012

    • Author(s)
      宮本ユタカ、安田健一郎、間柄正明、木村貴海
    • Organizer
      EuCheMS 8th International Conference on Nuclear and Radiochemistry (NRC8)
    • Place of Presentation
      イタリア・コモ
    • Related Report
      2012 Annual Research Report
  • [Presentation] Optimization of Sequential Separation of U, Th, Pb, and Lanthanides for Ultra-trace Analysis2011

    • Author(s)
      Y.Miyamoto, K.Yasuda, M.Magara, T.Kimura
    • Organizer
      3rd International Nuclear Chemistry Congress (3rd INCC)
    • Place of Presentation
      パレルモ(イタリア)
    • Year and Date
      2011-09-22
    • Related Report
      2012 Final Research Report
  • [Presentation] Optimization of Sequential Separation of U, Th, Pb, and Lanthanides for Ultra-trace Analysis2011

    • Author(s)
      Y.Miyamoto, K.Yasuda, M.Magara, T.Kimura
    • Organizer
      3rd International Nuclear Chemistry Congress (3rd INCC)
    • Place of Presentation
      イタリア、パレルモ
    • Year and Date
      2011-09-22
    • Related Report
      2011 Annual Research Report
  • [Presentation] Sequential Separation for Ultratrace Analysis of U, Th, Pb, and Lanthanides in Environmental Samples2010

    • Author(s)
      T.Kimura, M.Magara, Y.Miyamoto, K.Yasuda
    • Organizer
      The 36th International Symposium on Environmental Analytical Chemistry (ISEAC)
    • Place of Presentation
      ローマ(イタリア)
    • Year and Date
      2010-10-06
    • Related Report
      2012 Final Research Report
  • [Presentation] Sequential Separation for Ultra-trace Analysis of U, Th, Pb, and Lanthanides in Environmental Samples2010

    • Author(s)
      T.Kimura, M.Magara, Y.Miyamoto, K.Yasuda
    • Organizer
      The 36th International Symposium on Environmental Analytical Chemistry (ISEAC)
    • Place of Presentation
      ローマ(イタリア)
    • Year and Date
      2010-10-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] 極微量元素イオン交換逐次分離法の自動化に向けた分離条件の検討2010

    • Author(s)
      宮本ユタカ、安田健一郎、間柄正明、木村貴海
    • Organizer
      第54回日本放射化学討論会
    • Place of Presentation
      大阪大学銀杏会館
    • Year and Date
      2010-09-29
    • Related Report
      2012 Final Research Report 2010 Annual Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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