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Evaluation of ceramics grain blandly using AFM-Raman spectroscopy

Research Project

Project/Area Number 22560679
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic materials/Physical properties
Research Institution防衛大学校

Principal Investigator

YAMAMOTO Takashi  防衛大学校, 電気情報学群, 教授 (70546043)

Co-Investigator(Kenkyū-buntansha) NISHIDA Ken  防衛大学校, 電気情報学群, 准教授 (40299384)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2012: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2011: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2010: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords機能性セラミックス / AFM ラマン分光法 / AFMラマン / 強誘電体 / 欠陥 / 高空間分解能測定 / 近接場光 / 酸素欠陥
Research Abstract

We applied AFM-Raman combined equipment for high sensitive and high spatial resolution measurement technique. The intensity of Raman spectra at TERS was 5 times as high as that of normal Raman measurement. The spatial resolution was about 300 nm. We established the evaluation method for perovskite oxides. The changes of phonon modes related to A- and B-site ions was indicated anti-site and appearance of additional mode was showed oxygen vacancy.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (18 results)

All 2012 2011 2010

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (13 results)

  • [Journal Article] Investigation of Sputtering Damage in SrRuO3 Films Prepared by Sputtering with Raman and X-ray Photoemission Spectroscopies2012

    • Author(s)
      T. Tai、M. Nishide、M. Matsuoka、T. Kamo、 H. Funakubo 、T. Katoda 、H. Shima 、 K. Nishida 、T. Yamamoto
    • Journal Title

      Jpn. J. Appl. Phys.

      Volume: 51 Issue: 9S1 Pages: 09LA19-09LA19

    • DOI

      10.1143/jjap.51.09la19

    • NAID

      210000141237

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Thermooptic Property of Polycrystalline BiFeO_3 Film2011

    • Author(s)
      H.Shima, K.Tsutsumi, M.Suzuki, T.Tadokoro, H.Naganuma, T.Iijima, K.Nishida, T.Yamamoto, T.Nakajima, S.Okamura
    • Journal Title

      Jpn.J.Appl.Phys

      Volume: 50 Issue: 9S2 Pages: 09NB02-09NB02

    • DOI

      10.1143/jjap.50.09nb02

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microwave Absorbing Property of Stacked Polypyrrole-Coated Nonwoven Textiles2011

    • Author(s)
      T.Yamamoto, Y.Egami, K.Nishida, K.Suzuki, H.Inou
    • Journal Title

      Jpn.J.Appl.Phys

      Volume: 50 Issue: 9S2 Pages: 09NF04-09NF04

    • DOI

      10.1143/jjap.50.09nf04

    • NAID

      210000071324

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Investigation of Oxygen vacancies in Micro-patterned PZT Thin Films using Raman spectroscopy2010

    • Author(s)
      K.Nishida, et al.
    • Journal Title

      Key Engineering Materials

      Volume: 421-422 Pages: 135-138

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of Relative Volume Fraction of Tetragonal Phase and Rhombohedral Phase in Pb(Zr, Ti)O3_ Film by Raman Spectroscopy2010

    • Author(s)
      M.Nishide, et al.
    • Journal Title

      Journal of the Ceramic Society of Japan

      Volume: 118 Pages: 644-647

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] Structural investigation of SrRuO3 films prepared by sputtering method using Raman spectroscopy and X-ray photoemission spectroscopy2012

    • Author(s)
      T. Tai, M. Nishide, M. Matsuoka, J. Kim, T. Kamo, H. Funakubo, T. Katoda, H. Shima, K. Nishida and T. Yamamoto
    • Organizer
      IUMRS-International Conference on Electronic Materials (IUMRS-ICEM 2012)
    • Place of Presentation
      Pacifico Yokohama, Yokohama, Japan
    • Related Report
      2012 Annual Research Report 2012 Final Research Report
  • [Presentation] ラマン分光法によるスパッタリング法で作製したSrRuO3薄膜のスパッタダメージ評価と特性に及ぼす影響-ラマン分光法、X線分光法による構造解析-2012

    • Author(s)
      田井丈嗣
    • Organizer
      第29回強誘電体応用会議(FMA29)
    • Place of Presentation
      コープイン京都
    • Related Report
      2012 Annual Research Report
  • [Presentation] Structural Investigation of Highly Polarized Single c-Domain PZT Thin Films Grown by Magnetron Sputtering2012

    • Author(s)
      T. Tai
    • Organizer
      International Symposium on Integrated Functionalities(ISIF) 2012
    • Place of Presentation
      The Hong Kong Polytechnic University, Hong Kong, China
    • Related Report
      2012 Annual Research Report
  • [Presentation] Investigation of crystal structure change in PZT powder, ceramics and polarized ceramics using Raman spectroscopy2012

    • Author(s)
      T. Tai
    • Organizer
      IUMRS-International Conference on Electronic Materials (IUMRS-ICEM 2012)
    • Place of Presentation
      Pacifico Yokohama, Yokohama, Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Investigation of Growth Condition Dependence of Pb(Zr, Ti)O3-based Films Prepared by RF Magnetron Sputtering with Raman Spectroscopy2012

    • Author(s)
      T. Tai
    • Organizer
      4 th China-Japan Symposium on Ferroelectric Materials and Their Applications
    • Place of Presentation
      Taikanso, Matsushima, Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Raman Spectroscopy Evaluation of Residual Stress and Oxygen Vacancy in MLCC Capacitor2012

    • Author(s)
      T. Tai
    • Organizer
      The 29 th International Korea-Japan Seminar on Ceramics 2012
    • Place of Presentation
      EXCO, Daegu, Korea
    • Related Report
      2012 Annual Research Report
  • [Presentation] Influence of Substrate Clamping on Thermooptic Property of Epitaxial and Polycrystalline BiFeO_3 Thin Films2011

    • Author(s)
      H.Shima, K.Tsutsumi, M.Suzuki, S.Okamura, T.Iijima, H.Funakubo, K.Nishida, T.Yamamoto
    • Organizer
      15th US-Japan Seminar on Dielectric and Piezoelectric Ceramics
    • Place of Presentation
      Castle Park Hotel, Kagoshima, Japan(招待講演)
    • Year and Date
      2011-11-08
    • Related Report
      2011 Annual Research Report
  • [Presentation] Raman Spectroscopy Evaluation of Oxygen Vacancy Migration by Electrical Field in Electroceramics2011

    • Author(s)
      T. Yamamoto、H. Shima、K. Nishida、 T. Tai 、M. Nishide 、H. Kishi
    • Organizer
      15th US-Japan Seminar on Dielectric and Piezoelectric Ceramics
    • Place of Presentation
      Castle Park Hotel, Kagoshima, Japan
    • Year and Date
      2011-11-07
    • Related Report
      2012 Final Research Report
  • [Presentation] Raman Spectroscopy Evaluation of Oxygen Vacancy Migration by Electrical Field in Electroceramics2011

    • Author(s)
      T.Yamamoto, H.Shima, K.Nishida, T.Tai, M.Nishide, H.Kishi
    • Organizer
      15th US-Japan Seminar on Dielectric and Piezoelectric Ceramics
    • Place of Presentation
      Castle Park Hotel, Kagoshima, Japan(招待講演)
    • Year and Date
      2011-11-07
    • Related Report
      2011 Annual Research Report
  • [Presentation] ラマン分光法によるスパッタSrRuO3薄膜の構造評価とスパッタリングダメージが特性に及ぼす影響2011

    • Author(s)
      田井丈嗣, 宮崎亘, 大住剛, 金鎮雄, 西出正道, 加茂嵩史, 舟窪浩, 島宏美, 西田謙, 山本孝
    • Organizer
      2011年秋季第72回応用物理学会学術講演会
    • Place of Presentation
      山形大学小白河キャンパス(山形県)
    • Year and Date
      2011-09-01
    • Related Report
      2011 Annual Research Report
  • [Presentation] マルチフェロイックBiFeO_3薄膜の熱光学特性に対する基板拘束の影響2011

    • Author(s)
      島宏美, 曽根圭太, 中嶋宇史, 堤浩一, 鈴木道夫, 田所利康, 永沼博, 飯島高志, 西田謙, 山本孝, 岡村総一郎
    • Organizer
      第28回強誘電体応用会議(FMA-28)
    • Place of Presentation
      コープイン京都(京都府)(招待講演)
    • Year and Date
      2011-05-27
    • Related Report
      2011 Annual Research Report
  • [Presentation] Microwave Absorbing Property of Piled Polyprrole-coated Non woven textiles2010

    • Author(s)
      Y.Takashi, et al.
    • Organizer
      The 27th International Korea-Japan Seminar on Ceramics
    • Place of Presentation
      Incheon, Korea
    • Year and Date
      2010-11-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] Rapid and High Sensitive Structure Evaluation of Ferroelectric Filmsusing Micro-Raman Spectroscopy2010

    • Author(s)
      M.Nishide, Y.Takashi, et al.
    • Organizer
      13nd International Congress on Ceramics(ICC3)
    • Place of Presentation
      大阪国際会議場(大阪府)
    • Year and Date
      2010-11-17
    • Related Report
      2010 Annual Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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