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Fabrication of carbon nanofiber reinforced aluminum matrix composites by infiltration method

Research Project

Project/Area Number 22560685
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Physical properties
Research InstitutionWaseda University

Principal Investigator

MASUDA Chitoshi  早稲田大学, 理工学術院, 教授 (20350407)

Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2012: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2011: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2010: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywords金属基複合材料 / カーボンナノファイバー(CNF) / 金属被覆 / アルミ合金 / 浸透法 / CNF / Al / 界面組織 / 濡れ性 / カーボンナノファイバー / 金属コーティング / アルミニュウム / 複合材料 / 材料工学 / 複合材料・物性 / 分散強化 / コーティング / ナノファイバー
Research Abstract

In order to fabricate the CNF reinforced Al matrix composites, the surface of CNF was examined to coat the several metal, and wettability was evaluated using the coated CNF preforms. Moreover, the infiltration was performed using the preform including the coating CNF. After CNF, metal powder and catalyst were mixed and heated at several temperature in vacuum, the Al , Cu, Mg, Ni were coated on the surface of CNF. The sessile angle was about 174°(reference data) and not succeeded for Al coated CNF preformat 950℃, while it was 145°for AlN coated preform at 900℃. Moreover, the sessile angle was about reduced to 125°for Ni coated CNF preform. Finally, the infiltration was examined for several conditions, such as preform fabrication, Mg/Al ratios, N2 gas flow. The maximum infiltration depth(more than 2/3 of preform thickness) was obtained under the maximum porous preform condition(at room temperature at 200kPa), Mg/Al=0.3, and 1000ml.min in gas flow at 800℃. The volume fraction of CNF was about 15%, which was not fabricated by powder metallurgy method. The composites was fabricated by compo-casting method using Cu coating CNF in Al alloy.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (19 results)

All 2013 2012 2011 2010 Other

All Journal Article (8 results) (of which Peer Reviewed: 1 results) Presentation (11 results)

  • [Journal Article] 高強度カーボンナノファイバー(CNF)強化銅複合材料の開発2013

    • Author(s)
      増田
    • Journal Title

      天野財団研究概要報告書

      Pages: 133-137

    • Related Report
      2012 Final Research Report
  • [Journal Article] プラズマCVD法により作製した窒素添加DLCの構造とトライボロジー特性2012

    • Author(s)
      山本修二、日高徳昭、川名淳雄、増田千利
    • Journal Title

      表面技術

      Volume: Vol.63 Pages: 35-40

    • NAID

      10030476322

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
  • [Journal Article] Relationship between tribological properties and sp3/sp2 structure of nitrogenated diamond-like carbon deposited by Plasma CVD2012

    • Author(s)
      Shuji Yamamoto, Atsuo Kawana, Hiroshi Ichimura, Chitoshi Masuda
    • Journal Title

      Surface and Coatings Technology

      Volume: Vol.210 Pages: 1-9

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
  • [Journal Article] Al-VGCF複合材料の作製を目的としたIn-Situ CVD法によるVGCF表面へのアルミニウムコーティング2012

    • Author(s)
      小川文雄、平川起也、増田千利
    • Journal Title

      材料

      Volume: Vol.61

    • NAID

      130002084985

    • Related Report
      2012 Final Research Report
  • [Journal Article] Al-VGCF複合材料の作製を目的とした In-Situ CVD法によるVGCF表面へのアルミニウムコーティング2012

    • Author(s)
      小川文雄、平川 起也、増田 千利
    • Journal Title

      材料

      Volume: Vol.61 Pages: 454-461

    • NAID

      130002084985

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] アルミコーティングしたCNFプリフォームとアルミとの濡れ性評価2011

    • Author(s)
      増田、小川、平川
    • Journal Title

      大阪大学接合科学共同利用・共同研究拠点共同研究報告書

      Pages: 166-167

    • Related Report
      2012 Final Research Report
  • [Journal Article] Modeling of grain boundary stability of materials under severe plastic deformation and experimental verification2010

    • Author(s)
      Y. Saito, and C. Masuda
    • Journal Title

      Mat. Sci. Forum

      Volume: 638-642 Pages: 2724-2729

    • Related Report
      2012 Final Research Report
  • [Journal Article] ニッケルコーティングしたCNFプリフォームとAlとの濡れ性評価

    • Author(s)
      小川、児玉
    • Journal Title

      大阪大学接合科学共同利用・共同研究拠点共同研究報告書

      Volume: (印刷中)

    • Related Report
      2012 Final Research Report
  • [Presentation] Fabrication of extruded Al composite reinforced VGCF and properties2011

    • Author(s)
      F.Ogawa, T.Nishmura, C.Masuda
    • Organizer
      TMS 2011 Annual Meeting
    • Place of Presentation
      カリフォルニヤ、サンディエゴ
    • Year and Date
      2011-02-28
    • Related Report
      2010 Annual Research Report
  • [Presentation] プラズマCVD法による窒素添加DLCのトライボロジー特性2011

    • Author(s)
      山本、日高、川奈、増田
    • Organizer
      表面処理技術協会
    • Related Report
      2012 Final Research Report
  • [Presentation] Fabrication of extruded Al composites reinforced by CVD and characterization, modeling of their properties2011

    • Author(s)
      F. Ogawa, T. Nishimura, and C. Masuda
    • Organizer
      TMS Annual Meeting
    • Place of Presentation
      San Diego, USA
    • Related Report
      2012 Final Research Report
  • [Presentation] CVD法によるVGCFへのAl被覆における界面組織の観察2010

    • Author(s)
      平川、小川、増田、西村
    • Organizer
      日本金属学会2010秋季大会
    • Place of Presentation
      札幌
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] CVD法によるMg粉末上へのCNT成長条件の検討2010

    • Author(s)
      平川、小川、増田、西村
    • Organizer
      日本金属学会2010秋季大会
    • Place of Presentation
      札幌
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] Al粉末表面へ成長させたCNT強化複合材料の作成2010

    • Author(s)
      平川、小川、増田、西村
    • Organizer
      日本金属学会2010秋季大会
    • Place of Presentation
      札幌
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] Fabrication of carbon nanofiber reinforced Al matrix composite by pressureless infiltration2010

    • Author(s)
      F. Ogawa, C. Masuda, T. Nishimura
    • Organizer
      TMS Annual Meeting
    • Place of Presentation
      Seattle, USA
    • Related Report
      2012 Final Research Report
  • [Presentation] Fabrication of carbon nanotubes grown on Al powders reinforced Al matrix composites2010

    • Author(s)
      C. Masuda, F. Ogawa, R. Hirashima
    • Organizer
      TMS Annual Meeting
    • Place of Presentation
      Seattle, USA
    • Related Report
      2012 Final Research Report
  • [Presentation] Fabrication of Al matrix composites reinforced by Al coated CNF and CNTs2010

    • Organizer
      4^<th> Int. Conf. on Carbon based nanocomposites
    • Place of Presentation
      Sept Germany
    • Related Report
      2012 Final Research Report
  • [Presentation] Al粉末表面へ成長させたCNT強化Al基複合材料の作成2010

    • Author(s)
      平嶋、小川、西村、増田
    • Place of Presentation
      北海道
    • Related Report
      2012 Final Research Report
  • [Presentation] CVD法によるCNFhenoAlコーティングの界面組織観察2010

    • Author(s)
      平川、小川、西村、増田
    • Organizer
      日本金属学会
    • Place of Presentation
      北海道
    • Related Report
      2012 Final Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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