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Hydrogen behavior in the metal detected by stress measurement and ESD measurement.

Research Project

Project/Area Number 22560709
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionNational Institute for Materials Science

Principal Investigator

ITAKURA Akiko  独立行政法人物質・材料研究機構, その他部局等, その他 (20343858)

Co-Investigator(Renkei-kenkyūsha) TAKAGI Shoji  東邦大学, 理学部, 教授 (60171419)
MURASE Yoshiharu  (独)物質材料研究機構, 主任研究員 (10354193)
Project Period (FY) 2010-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2013: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2012: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2011: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2010: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords破壊・疲労 / 応力腐食割れ / 微小応力 / 水素 / マイクロカンチレバー / 材料強度 / 表面応力 / 水素脆化 / 金属表面 / 真空 / 材料表面 / 水素放出 / 電子衝撃脱離 / ステンレス鋼 / ステンレス鋼薄膜 / 表面構造
Research Abstract

Hydrogen in metals causes hydrogen embrittlement, which is the process of various metals to become brittle and fracture. Hydrogen detection seems to be one of the most difficult aspects of the problem and the phenomenon was not completely understood.
We have measured a surface stress of metal thin film during hydrogen plasma irradiation and detected compressive surface stress, which had a hysteresis. Alloys of complex structure are used as structural materials. It is not known where the hydrogen is in the alloy. We have tried to investigate hydrogen behavior in metal alloys from observation of two-dimensional hydrogen concentration on metal surface using electron stimulated desorption (ESD) method. We have detected micron order surface modification of hydrogen distribution.

Report

(5 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (47 results)

All 2014 2013 2012 2011 2010

All Journal Article (8 results) (of which Peer Reviewed: 8 results) Presentation (39 results) (of which Invited: 5 results)

  • [Journal Article] Thin Polyelectrolyte Multilayers Made by Inkjet Printing and Their Characterization by Nano-mechanical Cantilever Sensors2014

    • Author(s)
      M.Toda, Y.Chen, S.Nett, A.N.Itakura, J.Gutemann, R.Berger
    • Journal Title

      Journal of Physical Chemistry C

      Volume: 118(印刷中) Issue: 15 Pages: 8071-8078

    • DOI

      10.1021/jp501464j

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] 水素放出に及ぼすステンレス鋼の表面加工の効果2013

    • Author(s)
      板倉明子、鈴木真司、高木祥示、村瀬義治、土佐正弘
    • Journal Title

      真空

      Volume: 57 Pages: 23-26

    • NAID

      130003394491

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effective Young's Modulus Measurement of Thin Film Using Micromechanical Cantilever Sensors2013

    • Author(s)
      A.N.Itakura, M.Toda, K.Miyake, R.Foerch, R.Berger
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 52

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Stress inversion from initial tensile to compressive side during ultrathin oxide growth of the Si(100) surface2013

    • Author(s)
      M.Kitajima, T.Narishima, T.Kurashina, A.N.Itakura, S.Takami, A.Miyamoto
    • Journal Title

      Journal of Physics-Condensed Matter

      Volume: 25 Issue: 35 Pages: 355007-355007

    • DOI

      10.1088/0953-8984/25/35/355007

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effective Young’s Modulus Measurement of Thin Film Using Micromechanical Cantilever Sensors2013

    • Author(s)
      A.N.Itakura, M.Toda, K.Miyake, R.Foerch, R.Berger
    • Journal Title

      JAPANESE JOURNAL OF APPLIED PHYSICS

      Volume: 52 Issue: 11R Pages: 110111-110111

    • DOI

      10.7567/jjap.52.110111

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 水素放出に及ぼすステンレス鋼の表面加工の効果2013

    • Author(s)
      板倉明子、土佐正弘、村瀬義治、鈴木真司、高木祥示、後藤哲二
    • Journal Title

      JOURNAL OF THE VACUUM SOCIETY OF JAPAN

      Volume: 57 Pages: 23-26

    • NAID

      130003394491

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 真空技術と表面科学を用いた大気分析の新しい展望2012

    • Author(s)
      板倉明子
    • Journal Title

      真空

      Volume: 55 Pages: 383-388

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] マイクロカンチレバー表面への分子吸着を利用した大気分析の新しい展望2012

    • Author(s)
      板倉明子
    • Journal Title

      真空

      Volume: 55 Pages: 383-388

    • NAID

      10031055224

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Presentation] Gas sensing by micro cantilever and thin film2014

    • Author(s)
      A.N.Itakura, M.Toda, R.Berger
    • Organizer
      BIT's 4th World Congress of Advanced Materials 2014
    • Place of Presentation
      Chongqing Yuelai International Conference & EXPO Center, Chongqing, China
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Surface Stress Evolution during Hydrogen irradiation on Metals2014

    • Author(s)
      A.N.Itakura, S.Suzuki, S.Takagi, T.Goto, Y.Murase, M.Tosa
    • Organizer
      11th Annual International Workshop on Nano-mechanical Sensing
    • Place of Presentation
      Hotel NH Eurobuilding, Madrid, Spain
    • Related Report
      2013 Final Research Report
  • [Presentation] SURFACE STRESS EVOLUTION DURING HYDROGEN IRRADIATION ON METALS2014

    • Author(s)
      板倉明子、鈴木真司、田中健一郎、高木祥示、村瀬義治、土佐正弘
    • Organizer
      11th Annual International Workshop on Nanomechanical Sensing
    • Place of Presentation
      Hotel NH Eurobuilding,Madrid,Spain
    • Related Report
      2013 Annual Research Report
  • [Presentation] 電子衝撃脱離法によるステンレス隔膜水素透過特性2013

    • Author(s)
      平田健一郎、鈴木真司、村瀬義治、高木祥示、後藤哲二、板倉明子
    • Organizer
      第33回表面科学学術講演会・第54回真空に関する連合講演会
    • Place of Presentation
      つくば国際会議場,つくば市
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] ステンレス隔膜水素透過特性に及ぼす同位体効果2013

    • Author(s)
      鈴木真司、村瀬義治、高木祥示、後藤哲二、板倉明子、坂上裕之
    • Organizer
      第33回表面科学学術講演会・第54回真空に関する連合講演会
    • Place of Presentation
      つくば国際会議場,つくば市
    • Related Report
      2013 Final Research Report
  • [Presentation] Measurement of hydrogen permeability of stainless steel membrane by ESD ion mapping2013

    • Author(s)
      A.N.Itakura, S.Suzuki, S.Takagi, T.Goto, Y.Murase, M.Tosa
    • Organizer
      19th International Vacuum Congress
    • Place of Presentation
      Paris Palais des Congrès, Paris, France
    • Related Report
      2013 Final Research Report
  • [Presentation] Measurement of hydrogen permeability of stainless steel membrane by ESD ion mapping2013

    • Author(s)
      板倉明子、鈴木真司、高木祥示、後藤哲二、土佐正弘、村瀬義治
    • Organizer
      19th International Vacuum Congress
    • Place of Presentation
      Paris Palais des Congrès,Paris
    • Related Report
      2013 Annual Research Report
  • [Presentation] ステンレス隔膜水素透過特性に及ぼす同位体効果2013

    • Author(s)
      鈴木真司、田中健一郎、高木祥示、後藤哲二、板倉明子
    • Organizer
      第33回表面科学学術講演会・第54回真空に関する連合講 演会
    • Place of Presentation
      つくば国際会議場,つくば市
    • Related Report
      2013 Annual Research Report
  • [Presentation] Measurement of hydrogen permeability of stainless steel membrane by ESD ion mapping2013

    • Author(s)
      Akiko N. Itakura
    • Organizer
      19th International Vacuum Congress
    • Place of Presentation
      Paris Palais des Congrès,Paris,
    • Related Report
      2012 Annual Research Report
  • [Presentation] 電子衝撃脱離によるステンレス鋼の水素透過特性の観察2012

    • Author(s)
      鈴木真司、村瀬義治、土佐正弘、高木祥示、後藤哲二、板倉明子
    • Organizer
      第32回日本表面科学会年会
    • Place of Presentation
      東北大学片平キャンパス,仙台
    • Related Report
      2013 Final Research Report
  • [Presentation] ステンレス表面上の透過水素分布の観察2012

    • Author(s)
      鈴木真司、村瀬義治、高木祥示、後藤哲二、板倉明子
    • Organizer
      第53回真空に関する連合講演会
    • Place of Presentation
      甲南大学ポートアイランドキャンパス,神戸
    • Related Report
      2013 Final Research Report
  • [Presentation] Surface Stress Evolution during Hydrogen irradiation on Stainless Steel2012

    • Author(s)
      A.N.Itakura, S.Suzuki, S.Takagi, T.Goto, Y.Murase, M.Tosa
    • Organizer
      38th International Conference on Micro and Nano Engineering
    • Place of Presentation
      Halls Caravelle Concorde, Toulouse
    • Related Report
      2013 Final Research Report
  • [Presentation] Surface stress under hydrogen exposure on stainless steel and paradium films on micro cantilevers2012

    • Author(s)
      A.N.Itakura, S.Takagi, T.Goto, M.Tosa
    • Organizer
      JST-DFG joint meeting 2012
    • Place of Presentation
      University of Duisburg-Essen, Krefeld, Germany
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] ステンレス表面上の透過水素分布の観察2012

    • Author(s)
      鈴木信司(学生)
    • Organizer
      第53回真空に関する連合講演会
    • Place of Presentation
      神戸大学・ポートアイランドキャンパス(兵庫)
    • Related Report
      2012 Annual Research Report
  • [Presentation] 電子衝撃脱離によるステンレス鋼の水素透過特性の観察2012

    • Author(s)
      鈴木信司(学生)
    • Organizer
      第32回日本表面科学会
    • Place of Presentation
      東北大学(宮城)
    • Related Report
      2012 Annual Research Report
  • [Presentation] Surface stress under hydrogen exposure on stainless steel and paradium films on micro cantilevers2012

    • Author(s)
      Akiko N. Itakura
    • Organizer
      JST-DFG meeting
    • Place of Presentation
      Krefeld (Germany)
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Surface Stress Evolution during Hydrogen irradiation on Stainless Steel2012

    • Author(s)
      Akiko N. Itakura
    • Organizer
      38th International Conference on Micro and Nano Engineering
    • Place of Presentation
      Halls Caravelle Concorde,Toulouse(France)
    • Related Report
      2012 Annual Research Report
  • [Presentation] Surface Stress generation under hydrogen plasma irradiation on metal thin film2011

    • Author(s)
      Akiko N.Itakura, Masahiro Tosa, Saransh Singh, Shoji Takagi, Tetsuji Gotoh
    • Organizer
      6th International Symposium on Surface Science
    • Place of Presentation
      タワーホール船堀橋(東京)
    • Year and Date
      2011-12-12
    • Related Report
      2011 Annual Research Report
  • [Presentation] 水素照射下で生じるステンレス鋼の表面応力2011

    • Author(s)
      板倉明子, 土佐正弘, Saransh Singh, 高木祥示, 後藤哲二
    • Organizer
      第52回真空に関する連合講演会
    • Place of Presentation
      学習院創立百周年記念会館(東京)
    • Year and Date
      2011-11-18
    • Related Report
      2011 Annual Research Report
  • [Presentation] Measurement of Hydrogen Permeability of Stainless Steel Membrane2011

    • Author(s)
      Shoji Takagi, Shinji Suzuki, Tetsuji Gotoh, Yoshiharu Murase, Masahiro Tosa, Akiko N.Itakura
    • Organizer
      15th International Conference on Thin Films
    • Place of Presentation
      京都テルサ(京都)
    • Year and Date
      2011-11-10
    • Related Report
      2011 Annual Research Report
  • [Presentation] Surface Stress Generation during Hydrogen irradiation on Metal Surfaces2011

    • Author(s)
      Akiko N.Itakura, Saransh Singh, Shoji Takagi, Tetsuji Gotoh
    • Organizer
      15th International Conference on Thin Films
    • Place of Presentation
      京都テルサ(京都)
    • Year and Date
      2011-11-09
    • Related Report
      2011 Annual Research Report
  • [Presentation] 真空技術と表面科学を用いた大気分析の新しい展望2011

    • Author(s)
      板倉明子
    • Organizer
      日本真空協会産業部会平成23年5月例会(第249回)
    • Place of Presentation
      機械振興会館,東京都港区
    • Year and Date
      2011-05-18
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] 真空技術と表面科学を用いた大気分析の新しい展望2011

    • Author(s)
      板倉明子
    • Organizer
      真空産業部会
    • Place of Presentation
      機械振興会館(東京)(招待講演)
    • Year and Date
      2011-05-18
    • Related Report
      2011 Annual Research Report
  • [Presentation] 真空技術と表面科学を用いた大気分析の新しい展望2011

    • Author(s)
      板倉明子
    • Organizer
      日本真空協会産業部会
    • Place of Presentation
      機械振興会館(東京都)
    • Year and Date
      2011-05-18
    • Related Report
      2010 Annual Research Report
  • [Presentation] Stress generation during Hydrogen plasma irradiation on Stainless steel thin film2011

    • Author(s)
      A.N.Itakura, Shoji Takagi, Shinji Suzuki, Tetsuji Gotoh, Yoshiharu Murase, Masahiro Tosa
    • Organizer
      8th International warkshop on Nanomechanical Cantilever Sensors
    • Place of Presentation
      Trinity College Dublin(ダブリン/アイルランド)
    • Year and Date
      2011-05-12
    • Related Report
      2011 Annual Research Report
  • [Presentation] Stress generation during Hydrogen Plasma Irradiation on Stainless steel2011

    • Author(s)
      A.N.Itakura, D.Sakai, S.Takagi, T.Goto
    • Organizer
      8^<th> International workshop on Nano-mechanical Sensing
    • Place of Presentation
      ダブリン(アイルランド)
    • Year and Date
      2011-05-11
    • Related Report
      2010 Annual Research Report
  • [Presentation] Stress generation during Hydrogen plasma irradiation On Stainless steel thin film2011

    • Author(s)
      A.N.Itakura, S.Takagi, T.Gotoh
    • Organizer
      Max-Planck Institute for Polymer Research May Meeting
    • Place of Presentation
      Max-Planck Institute for Polymer Research (Mainz/独)(invited)
    • Year and Date
      2011-05-09
    • Related Report
      2011 Annual Research Report
  • [Presentation] Surface Stress of Stainless Steel under Hydrogen Plasma Irradiation2011

    • Author(s)
      A.N.Itakura, S.Takagi, T.Goto
    • Organizer
      Seminar in Max-Planck Institute for Polymer Research
    • Place of Presentation
      マインツ(ドイツ)
    • Year and Date
      2011-05-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] ステンレス薄板を横切る水素の透過特性2011

    • Author(s)
      高木祥示, 板倉明子, 土佐正弘, Saransh Singh, 酒井大樹, 後藤哲二
    • Organizer
      第58回応用物理学関係連合講演会(*震災のため予稿発表のみ)
    • Place of Presentation
      神奈川工科大学(厚木市)
    • Year and Date
      2011-03-25
    • Related Report
      2011 Annual Research Report
  • [Presentation] ステンレス薄板を横切る水素の透過特性2011

    • Author(s)
      板倉明子・高木祥示・後藤哲二
    • Organizer
      日本応用物理学会
    • Place of Presentation
      (震災のため中止(予稿集))
    • Year and Date
      2011-03-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] Stress generation under hydrogen plasma irradiation on metal thin film2011

    • Author(s)
      A.N.Itakura, S.Shin, S.Takagi, M.Tosa
    • Organizer
      6th International Symposium on Surface Science
    • Place of Presentation
      Tower Hall Funabori,Tokyo
    • Related Report
      2013 Final Research Report
  • [Presentation] 水素照射下で生じるステンレス鋼の表面応力"2011

    • Author(s)
      板倉明子、Saran Shin、高木祥示、後藤哲二
    • Organizer
      第52回真空に関する連合講演会
    • Place of Presentation
      学習院創立百周年記念会館,東京
    • Related Report
      2013 Final Research Report
  • [Presentation] Surface Stress Generation during Hydrogen irradiation on Metal Surfaces2011

    • Author(s)
      A.N.Itakura, S.Shin, S.Takagi, M.Tosa
    • Organizer
      15th international Conference on Thin Films
    • Place of Presentation
      Kyoto TERRSA,京都
    • Related Report
      2013 Final Research Report
  • [Presentation] Measurement of Hydrogen Permeability of Stainless Steel Membrane2011

    • Author(s)
      S.Takagi, D.Sakai, T.Goto, Y.Murase, A.N.Itakura
    • Organizer
      15th international Conference on Thin Films
    • Place of Presentation
      Kyoto TERRSA,京都
    • Related Report
      2013 Final Research Report
  • [Presentation] Stress generation during Hydrogen Irradiation on Stainless Steel2011

    • Author(s)
      A.N.Itakura, S.Takagi, D.Sakai, T.Goto, Y.Murase, M.Tosa
    • Organizer
      Max-Planck Institute for Polymer Research May Meeting
    • Place of Presentation
      Max-Planck Institute for Polymer Research, Mainz, Germany
    • Related Report
      2013 Final Research Report
  • [Presentation] Stress generation during Hydrogen plasma irradiation on Stainless steel thin film2011

    • Author(s)
      A.N.Itakura, S.Takagi, D.Sakai, T.Goto
    • Organizer
      8th International workshop on Nano-mechanical Cantilever Sensors
    • Place of Presentation
      Trinity College Dublin, Ireland
    • Related Report
      2013 Final Research Report
  • [Presentation] ステンレス薄板を横切る水素の透過特性2011

    • Author(s)
      板倉明子、高木祥示、酒井大樹、後藤哲二
    • Organizer
      2011年春季第58回応用物理学関係連合後援会
    • Place of Presentation
      神奈川工科大学,神奈川県厚木市
    • Related Report
      2013 Final Research Report
  • [Presentation] Young's Modulus measurement of organic thin films using Cantilever sensors2010

    • Author(s)
      A.N.Itakura, A.Grinevich, M.Toda, R.Foerch, R.Berger
    • Organizer
      18th International Vacuum Congress (IVC-18)
    • Place of Presentation
      Beijing International Convention Center, Beijing, China
    • Related Report
      2013 Final Research Report
  • [Presentation] Young's Modulus measurement of Plasma Polymerized Allylamine films using Cantilever sensors2010

    • Author(s)
      A.N.Itakura, M.Toda, R.Foerch, R.Berger
    • Organizer
      International Workshop on Nano-mechanical Cantilever Sensors 2010
    • Place of Presentation
      Banff Conference Center,Banff,CANADA
    • Related Report
      2013 Final Research Report
    • Invited

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Published: 2010-08-23   Modified: 2019-07-29  

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