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Fabrication of Ni-based Bulk Nanocrystalline Materials for the understanding of ductility and toughness in Nanocrystalline Materials

Research Project

Project/Area Number 22560726
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionOsaka Prefecture University

Principal Investigator

TAKIGAWA Yorinobu  大阪府立大学, 大学院・工学研究科, 准教授 (70382231)

Co-Investigator(Kenkyū-buntansha) HIGASHI Kenji  大阪府立大学, 大学院・工学研究科, 教授 (50173133)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Fiscal Year 2012: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2011: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2010: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
KeywordsNi基バルクナノ結晶材料 / 電解析出法 / 高強度 / 高延性 / 内部応力 / 配向性 / バルクナノ結晶材料 / Ni-W
Research Abstract

Bulk nanocrystalline Ni-based materials with a millimeter thick and minimized internal stress, concentration gradient and fluctuation were fabricated by electrodeposition, and improvement of tensile ductility was demonstrated. We obtain tensile strength of 1.2GPa and tensile elongation of 15% in Ni and 1.4GPa and 13% in Ni-W. There was the relationship between tensile ductility and the orientation index for the (200) plane in the bulk nanocrystalline Ni-W alloys. This result should be related to the crystal growth mechanism, and this study point to that the colony structure of electrodeposits has an effect on the tensile ductility.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (46 results)

All 2013 2012 2011 2010 Other

All Journal Article (15 results) (of which Peer Reviewed: 15 results) Presentation (27 results) Remarks (4 results)

  • [Journal Article] Effect of orientation on tensile ductility of electrodeposited bulk nanocrystalline Ni-W alloys2013

    • Author(s)
      I. Matusi, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Mater. Sci. Eng

      Volume: A578 Pages: 318-322

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of additives on tensile properties of bulk nanocrystalline Ni-W alloys electrodeposited from a sulfamate bath2013

    • Author(s)
      I. Matusi, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Mater. Lett

      Volume: 99 Pages: 65-67

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of interstitial carbon on the mechanical properties of electrodeposited bulk nanocrystalline Ni2013

    • Author(s)
      I. Matusi, T. Uesugi, Y. Takigawa and K. Higashi
    • Journal Title

      Acta Mater

      Volume: 61 Pages: 3360-3369

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of interstitial carbon on the mechanical properties of electrodeposited bulk nanocrystalline Ni2013

    • Author(s)
      I. Matsui, T. Uesugi, Y. Takigawa, K. Higashi
    • Journal Title

      Acta Materialia

      Volume: 61 Issue: 9 Pages: 3360-3369

    • DOI

      10.1016/j.actamat.2013.02.025

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of additives on tensile properties of bulk nanocrystalline Ni-W alloys electrodeposited from a sulfamate bath2013

    • Author(s)
      I. Matsui, Y. Takigawa, T. Uesugi. K. Higashi
    • Journal Title

      Materials Letters

      Volume: 99 Pages: 65-67

    • DOI

      10.1016/j.matlet.2013.02.067

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improvement in Tensile Ductility of Electrodeposited Bulk Nanocrystalline Ni-W by Sulfamate Bath using Propionic Acid2012

    • Author(s)
      I. Matusi, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Microelectronic Eng.

      Volume: 91 Pages: 98-101

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Improvement in Tensile Ductility of Electrodeposited Bulk Nanocrystalline Ni-W by Sulfamate Bath Using Propionic Acid2012

    • Author(s)
      I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Journal Title

      Microelectronic Engineering

      Volume: 91 Pages: 98-101

    • DOI

      10.1016/j.mee.2011.10.018

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 各種光沢剤を添加したスルファミン酸浴から作製したバルクナノ結晶 Ni の引張特性2011

    • Author(s)
      松井功, 岩見英明, 瀧川順庸, 上杉徳照, 東健司
    • Journal Title

      表面技術

      Volume: 62 Pages: 686-690

    • NAID

      10030476035

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Enhanced Tensile Ductility in Bulk Nanocrystalline Nickel Electrodeposited by Sulfamate Bath2011

    • Author(s)
      I. Matusi, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Mater. Lett.

      Volume: 65 Pages: 2351-2353

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Influence of Bath Composition on Tensile Ductility in Electrodeposited Bulk Nanocrystalline Nickel2011

    • Author(s)
      I. Matusi, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Mater. Trans

      Volume: 52 Pages: 142-146

    • NAID

      10027837465

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Enhanced Tensile Ductility in Bulk Nanocrystalline Nickel Electrodeposited by Sulfamate Bath2011

    • Author(s)
      I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Journal Title

      Materials Letters

      Volume: 65 Issue: 15-16 Pages: 2351-2353

    • DOI

      10.1016/j.matlet.2011.05.002

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 各種光沢剤を添加したスルファミン酸浴から作製したバルクナノ結晶Niの引張特性2011

    • Author(s)
      松井功, 岩見英明, 瀧川順庸, 上杉徳照, 東健司
    • Journal Title

      表面技術

      Volume: 62(未定) Pages: 686-690

    • NAID

      10030476035

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Influence of Bath Composition on Tensile Ductility in Electrodeposited Bulk Nanocrystalline Nickel2011

    • Author(s)
      I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Journal Title

      Mater.Trans

      Volume: 52 Pages: 142-146

    • NAID

      10027837465

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Tensile Properties of Bulk Nanocrystalline Ni and Ni-W Fabricated by Sulfamate Bath2010

    • Author(s)
      I. Matsui, Y. Takigawa, T. Uesugi and K. Higashi
    • Journal Title

      Mater. Sci. Forum

      Volume: 654-656 Pages: 1114-1117

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Tensile Properties of Bulk Nanocrystalline Ni and Ni-W Fabricated by Sulfamate Bath2010

    • Author(s)
      I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Journal Title

      Mater.Sci.Forum

      Volume: 654-656 Pages: 1114-1117

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] Fabrication of bulk nanocrystalline Ni-W with plastic deformability electrodeposited from a sulfamate bath2013

    • Author(s)
      I.Matsui, Y. Takigawa, T. Uesugi and K. Higashi
    • Organizer
      8th Pacific Rim International Conference on Advanced Materials and Processing (PRICM 8)
    • Place of Presentation
      Hawaii, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] Fabrication of Bulk Nanocrystalline Ni and Ni-W by Electrodeposition2012

    • Author(s)
      Y. Takigawa, I. Matsui, T. Uesugi and K. Higashi
    • Organizer
      The 5th International Symposium on Designing, Processing and Properties of Advanced Engineering Materials (ISAEM-2012)
    • Place of Presentation
      豊橋.
    • Year and Date
      2012-11-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 電解析出法によるバルクナノ結晶 Ni の作製とその室温引張特性評価2012

    • Author(s)
      瀧川順庸, 松井功, 岩見英明, 上杉徳照, 東健司
    • Organizer
      日本金属学会第150回春期大会
    • Place of Presentation
      横浜国立大学 (横浜)
    • Year and Date
      2012-03-28
    • Related Report
      2012 Final Research Report
  • [Presentation] 電解析出法によるバルクナノ結晶Niの作製とその室温引張特性評価2012

    • Author(s)
      瀧川順庸, 松井功, 岩見英明, 上杉徳照, 東健司
    • Organizer
      日本金属学会第150回春期大会
    • Place of Presentation
      横浜国立大学(横浜)
    • Year and Date
      2012-03-28
    • Related Report
      2011 Annual Research Report
  • [Presentation] バルクナノ結晶Ni-W合金作製に向けた電析浴の最適化2012

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会第150回春期大会
    • Place of Presentation
      横浜国立大学(横浜)
    • Year and Date
      2012-03-28
    • Related Report
      2011 Annual Research Report
  • [Presentation] 各種光沢剤の電析バルクナノ結晶Niにおける機械的特性への影響2012

    • Author(s)
      松井功, 岩見英明, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      表面技術協会第125回講演大会
    • Place of Presentation
      東京都市大学(東京)
    • Year and Date
      2012-03-13
    • Related Report
      2011 Annual Research Report
  • [Presentation] 電析バルクナノ結晶Niの機械的特性に及ぼす各種光沢剤の影響2011

    • Author(s)
      松井功, 岩見英明, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      第13回関西表面技術フォーラム
    • Place of Presentation
      キャンパスプラザ京都(京都)
    • Year and Date
      2011-11-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] 電解析出バルクナノ結晶Ni-W合金の作製とその引張特性2011

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会第149回秋期大会
    • Place of Presentation
      コンベンションセンター(沖縄)
    • Year and Date
      2011-11-09
    • Related Report
      2011 Annual Research Report
  • [Presentation] 各種光沢剤を添加した電析バルクナノ結晶Niの機械的特性2011

    • Author(s)
      岩見英明, 松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会第149回秋期大会
    • Place of Presentation
      コンベンションセンター(沖縄)
    • Year and Date
      2011-11-09
    • Related Report
      2011 Annual Research Report
  • [Presentation] Influence of Gloss Agents on Mechanical Properties of Electrodeposited Bulk Nanocrystalline Ni2011

    • Author(s)
      H. Iwami, I. Matsui, Y. Takigawa, T. Uesugi and K. Higashi
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      ポートピアホテル(神戸
    • Year and Date
      2011-09-19
    • Related Report
      2012 Final Research Report
  • [Presentation] Influence of Gloss Agents on Mechanical Properties of Electrodeposited Bulk Nanocrystalline Ni2011

    • Author(s)
      H.Iwami, I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      ポートピアホテル(神戸)
    • Year and Date
      2011-09-19
    • Related Report
      2011 Annual Research Report
  • [Presentation] Fabrication of Bulk Nanocrystalline Ni-W with Plastic Deformability by Electrodeposition2011

    • Author(s)
      I.Matsui, Y.Takigawa, T.Uesugi, K.Higashi
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      ポートピアホテル(神戸)
    • Year and Date
      2011-09-19
    • Related Report
      2011 Annual Research Report
  • [Presentation] Fabrication of Bulk Nanocrystalline Ni-W Alloy with Minimized W-concentration Fluctuation2011

    • Author(s)
      Y. Takigawa, I. Matsui, T. Uesugi and K. Higashi
    • Organizer
      2011 International Conference on Processing & Manufacturing of Advanced Materials
    • Place of Presentation
      Quebec city, Canada.
    • Year and Date
      2011-08-02
    • Related Report
      2012 Final Research Report
  • [Presentation] Effect of Gloss Agent on Mechanical Property in Electrodeposited Bulk Nanocrystalline Ni2011

    • Author(s)
      I. Matsui, H. Iwami, Y. Takigawa, T. Uesugi and K. Higashi
    • Organizer
      2011 International Conference on Processing & Manufacturing of Advanced Materials
    • Place of Presentation
      Quebec city, Canada.
    • Year and Date
      2011-08-02
    • Related Report
      2012 Final Research Report
  • [Presentation] Fabrication of Bulk Nanocrystalline Ni-W Alloy with Minimized W-concentration Fluctuation2011

    • Author(s)
      Y.Takigawa, I.Matsui, T.Uesugi, K.Higashi
    • Organizer
      THERMEC'2011 International Conference on Processing & Manufacturing of Advanced Materials
    • Place of Presentation
      Quebec city, Canada(招待講演)
    • Year and Date
      2011-08-02
    • Related Report
      2011 Annual Research Report
  • [Presentation] Effect of Gloss Agent on Mechanical Property in Electrodeposited Bulk Nanocrystalline Ni2011

    • Author(s)
      I.Matsui, H.Iwami, Y.Takigawa, T.Uesugi, K.Higashi
    • Organizer
      THERMEC'2011 International Conference on Processing & Manufacturing of Advanced Materials
    • Place of Presentation
      Quebec city, Canada
    • Year and Date
      2011-08-02
    • Related Report
      2011 Annual Research Report
  • [Presentation] 電解析出法による高延性を示すバルクナノ結晶 Ni の作製2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      第12回関西表面技術フォーラム
    • Place of Presentation
      京都大学宇治おうばくプラザ(京都)
    • Year and Date
      2010-12-02
    • Related Report
      2012 Final Research Report
  • [Presentation] 電解析出法による高延性を示すバルクナノ結晶Niの作製2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      第12回関西表面技術フォーラム
    • Place of Presentation
      京都大学宇治おうばくプラザ(京都)
    • Year and Date
      2010-12-02
    • Related Report
      2010 Annual Research Report
  • [Presentation] 電解析出法によるバルクナノ結晶 Ni-W 合金の作製とその引張特性2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会 2010 年秋期(第147回)大会
    • Place of Presentation
      北海道大学(北海道).
    • Year and Date
      2010-09-25
    • Related Report
      2012 Final Research Report
  • [Presentation] 電解析出法によるバルクナノ結晶Ni-W合金の作製とその引張特性2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会2010年秋期(第147回)大会
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2010-09-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] 高強度と高延性を両立する均質バルクナノ結晶 Ni-W 作製プロセスの開発2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      表面技術協会第122回講演大会
    • Place of Presentation
      東北大学(宮城).
    • Year and Date
      2010-09-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 高強度と高延性を両立する均質バルクナノ結晶Ni-W作製プロセスの開発2010

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      表面技術協会第122回講演大会
    • Place of Presentation
      東北大学(宮城)
    • Year and Date
      2010-09-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] Tensile Properties of Bulk Nanocrystalline Ni and Ni-W Fabricated by Sulfamate Bath2010

    • Author(s)
      I. Matsui, Y. Takigawa, T. Uesugi and K. Higashi
    • Organizer
      The 7th Pacific Rim International Conference on Advanced Materials and Processing (PRICM-7)
    • Place of Presentation
      Cairns, Australia
    • Year and Date
      2010-08-02
    • Related Report
      2012 Final Research Report 2010 Annual Research Report
  • [Presentation] Fabrication of Bulk Nanocrystalline Ni and Ni-W by Electrodeposition

    • Author(s)
      Y. Takigawa, I. Matsui, T. Uesugi and K. Higashi
    • Organizer
      The 5th International Symposium on Designing, Processing and Properties of Advanced Engineering Materials (ISAEM-2012)
    • Place of Presentation
      豊橋
    • Related Report
      2012 Annual Research Report
  • [Presentation] Effect of Additives on Mechanical Properties of Electrodeposited Bulk Nanocrystalline Ni–W Alloys

    • Author(s)
      I.Matsui, Y. Takigawa, T. Uesugi and K. Higashi
    • Organizer
      The 5th International Symposium on Designing, Processing and Properties of Advanced Engineering Materials (ISAEM-2012)
    • Place of Presentation
      豊橋
    • Related Report
      2012 Annual Research Report
  • [Presentation] 各種光沢剤の電析バルクナノ結晶Ni-Wにおける機械的特性への影響

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      第14回関西表面技術フォーラム
    • Place of Presentation
      宇治
    • Related Report
      2012 Annual Research Report
  • [Presentation] 電解析出法による高延性バルクナノ結晶Ni-W合金の作製

    • Author(s)
      松井功, 瀧川順庸, 上杉徳照, 東健司
    • Organizer
      日本金属学会第152回春期大会
    • Place of Presentation
      東京
    • Related Report
      2012 Annual Research Report
  • [Remarks]

    • URL

      http://www2.mtl.osakafu-u.ac.jp/list.htm

    • Related Report
      2012 Final Research Report
  • [Remarks] 東研究室

    • URL

      http://www2.mtl.osakafu-u.ac.jp/

    • Related Report
      2012 Annual Research Report
  • [Remarks]

    • URL

      http://www2.mtl.osakafu-u.ac.jp/list.htm

    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www2.mtl.osakafu-u.ac.jp/list.htm

    • Related Report
      2010 Annual Research Report

URL: 

Published: 2010-08-23   Modified: 2019-07-29  

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