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Quantitative characterization of Nanogranular film using contrast variation between small-angle X-ray and neutron scattering

Research Project

Project/Area Number 22604003
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Quantum beam science
Research InstitutionKyoto University (2012)
National Institute for Materials Science (2010-2011)

Principal Investigator

OBA Yojiro  京都大学, 原子炉実験所, 助教 (60566793)

Co-Investigator(Kenkyū-buntansha) ABE Seishi  電磁材料研究所, 光材料グループ, 主席研究員 (20202666)
OHNUMA Shigehiro  電磁材料研究所, 素形材開発材料グループ, 主席研究員 (50142633)
OHNUMA Masato  物質・材料研究機構, 量子ビームユニット, 主席研究員 (90354208)
SUZUKI Jun-ichi  総合科学研究機構, 東海事業センター, 主任研究員 (40354899)
Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2012: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2011: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2010: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords中性子小角散乱 / X線小角散乱 / ナノグラニュラー / 合金コントラスト変調法 / 中性子小角散乱法 / X線小角散乱法 / 量子ビーム / ナノ材料 / 小角散乱 / 複合材料・物性
Research Abstract

Since nanostructure of nanogranular films are closely related with their physical properties, the quantitative characterization of the nanostructure is an important issue. In this study, the analysis method using small-angle neutron and X-ray scattering has been utilized. As a result, the size distribution and the dispersion states of the nanoparticles in the nanogranular films were quantitatively evaluated. In addition, the partitioning state of chemical composition between the nanoparticles and the matrix was quantitatively analyzed.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (14 results)

All 2013 2012 2011 2010 Other

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (12 results) (of which Invited: 1 results) Remarks (1 results)

  • [Journal Article] Nanostructure Characterization of Co-Pd-Si-O Soft Magnetic Nanogranular Film using Small-Angle X-ray and Neutron Scattering2013

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, M. Furusaka, K. Suresh, and S. Takeda
    • Journal Title

      Journal of Magnetism and Magnetic Materials

      Volume: Vol. 334 Pages: 45-51

    • DOI

      10.1016/j.jmmm.2013.01.024

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Presentation] 中性子・X 線小角散乱法によるナノグラニュラー軟磁性体の解析2013

    • Author(s)
      大場 洋次郎
    • Organizer
      中性子産業利用推進協議会
    • Place of Presentation
      連合会館、東京
    • Year and Date
      2013-03-01
    • Related Report
      2012 Final Research Report
  • [Presentation] Characterization of Nanostructures in Co-Insulator Nanogranular Films Using Small-Angle Neutron and X-ray Scattering2013

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, K. Ohishi, S. Takata, J. Suzuki, and M. Sugiyama (Y. Oba)
    • Organizer
      The 8th Pacific Rim International Conference on Advanced Materials and Processing
    • Place of Presentation
      Hawaii, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] 中性子・X線小角散乱法によるナノグラニュラー軟磁性体の解析2013

    • Author(s)
      大場 洋次郎(大場 洋次郎)
    • Organizer
      中性子産業利用推進協議会
    • Place of Presentation
      連合会館、東京
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Characterization of Nanostructures in Co-Pd-Si-O Soft Magnetic Nanogranular Film Using Compact type Small-Angle Neutron Scattering2012

    • Author(s)
      Y.Oba, M.Ohnuma, S.Ohnuma, M.Furusaka
    • Organizer
      2012 TMS Annual Meeting & Exhibition
    • Place of Presentation
      Walt Disney World Swan and Dolphin Resort (Orlando)
    • Year and Date
      2012-03-14
    • Related Report
      2011 Annual Research Report
  • [Presentation]2012

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, K. Ohishi, K Takata, J. Suzuki, and M. Sugiyama
    • Organizer
      15th International Small-Angle Scattering Conference
    • Place of Presentation
      Sydney、Australia
    • Related Report
      2012 Final Research Report
  • [Presentation] Nanostructure and Chemical State of Co-Insulator Soft magnetic Nanogranular Film2012

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, K. Ohishi, K. Takata, J. Suzuki, and M. Sugiyama (Y. Oba)
    • Organizer
      15th International Small-Angle Scattering Conference
    • Place of Presentation
      Sydney, Australia
    • Related Report
      2012 Annual Research Report
  • [Presentation] 中性子小角散乱法によるCo基ナノグラニュラー薄膜のナノ構造解析2012

    • Author(s)
      大場 洋次郎、大沼 正人、大沼 繁弘、大石 一城、高田 慎一、鈴木 淳市、杉山 正明(大場 洋次郎)
    • Organizer
      第4回J-PARC/MLFシンポジウム・茨城県ビームライン平成23年度成果報告会
    • Place of Presentation
      日本科学未来館、東京
    • Related Report
      2012 Annual Research Report
  • [Presentation] Partitioning State of Co in Co-insulator Soft Magnetic Nanogranular Films Characterized by Small-Angle Scattering2012

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, and M. Furusaka (Y. Oba)
    • Organizer
      International Union of Materials Research Societies - International Conference on Electronic Materials 2012
    • Place of Presentation
      パシフィコ横浜、神奈川
    • Related Report
      2012 Annual Research Report
  • [Presentation] Microstructural Analysis of Metallic Materials using Small-Angle X-ray and Neutron Scattering2011

    • Author(s)
      Y.Oba, M.Ohnuma, P.Kozikowski
    • Organizer
      1st Asia-Oceania Conference on Neutron Scattering
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Year and Date
      2011-11-23
    • Related Report
      2011 Annual Research Report
  • [Presentation] X線・中性子小角散乱法によるCo-Pd-Si-Oナノグラニュラー膜の微細組織解析2011

    • Author(s)
      大場洋次郎, 大沼正人, 大沼繁弘, 古坂道弘
    • Organizer
      日本金属学会2011年度秋期大会
    • Place of Presentation
      沖縄コンベンションセンター(沖縄県)
    • Year and Date
      2011-11-07
    • Related Report
      2011 Annual Research Report
  • [Presentation] X線・中性子小角散乱法を併用したCo-Nb-Oナノグラニュラー膜におけるナノ組織の定量評価2010

    • Author(s)
      大場洋次郎
    • Organizer
      茨城県中性子利用促進研究会
    • Place of Presentation
      いばらき量子ビームセンター(茨城県)
    • Year and Date
      2010-09-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] Nanostructures and magnetic properties in Co-metal oxide nano-granular films2010

    • Author(s)
      Y.Oba, M.Ohnuma, K.Suresh, S.Ohnuma
    • Organizer
      International Symposium on Advanced Magnetic Materials and Applications 2010
    • Place of Presentation
      Sendai International Center(宮城県)
    • Year and Date
      2010-07-14
    • Related Report
      2010 Annual Research Report
  • [Remarks]

    • URL

      http://www.rri.kyoto-u.ac.jp/PSlab/index.html

    • Related Report
      2012 Final Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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