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Development of nanometer-resolution XAFS imaging method and structural evaluation of nanostructured materials

Research Project

Project/Area Number 22651040
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeSingle-year Grants
Research Field Nanomaterials/Nanobioscience
Research InstitutionOsaka University

Principal Investigator

TAKAHASHI Yukio  大阪大学, 大学院・工学研究科, 准教授 (00415217)

Project Period (FY) 2010 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥3,070,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥270,000)
Fiscal Year 2011: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2010: ¥1,900,000 (Direct Cost: ¥1,900,000)
KeywordsコヒーレントX線光学 / X線顕微鏡 / X線構造解析 / 金属ナノ組織解析
Research Abstract

In principle, X-ray absorption spectrum at the nanometer scale can be derived from the coherent X-ray diffraction imaging at the X-ray energies around the X-ray absorption edge of a specific element. In such an experiment, the dose per surface unit of X-rays illuminated onto a sample has to be determined. In this study, incident X-ray intensity monitoring system for coherent X-ray diffraction imaging was developed. By using this system, we determined the dose of X-rays illuminated onto a nanostructured sample and quantitatively derived the electron density distribution of the sample.

Report

(3 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • Research Products

    (49 results)

All 2012 2011 2010 Other

All Journal Article (14 results) (of which Peer Reviewed: 14 results) Presentation (31 results) Book (1 results) Remarks (3 results)

  • [Journal Article] Multiscale element mapping of buried structures by ptychographic x-ray diffraction microscopy using anomalous scattering2011

    • Author(s)
      Y. Takahashi, A. Suzuki, N. Zettsu, Y. Kohmura, K. Yamauchi and T. Ishikawa
    • Journal Title

      Appl. Phys. Lett.

      Volume: 99 Pages: 131905-131905

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Towards High-Resolution Ptychographic X-ray Diffraction Microscopy2011

    • Author(s)
      Y. Takahashi, A. Suzuki, N. Zettsu, Y. Kohmura, Y. Senba, H. Ohashi, K. Yamauchi and T. Ishikawa
    • Journal Title

      Phys. Rev. B

      Volume: 83 Pages: 214109-214109

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Coherent diffraction microscopy at SPring-8 : instrumentation, data acquisition and data analysis2011

    • Author(s)
      R.Xu, S.Salha, K.Raines, H.Jiang, C-.C.Chen, Y.Takahashi, Y.Kohmura, Y.Nishino, C.Song, T.Ishikawa, J.Miao
    • Journal Title

      Journal of Synchrotron Radiation

      Volume: 18 Issue: 2 Pages: 293-298

    • DOI

      10.1107/s0909049510051733

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Element-specific High-resolution Diffraction Microscopy using Focused Hard X-ray Beam2011

    • Author(s)
      Y.Takahashi, Y.Nishino, R.Tsutsumi, H.Kubo, N.Zettsu, K.Yamauchi, T.Ishikawa, E.Matsubara
    • Journal Title

      Diamond Light Source Proceedings(SRMS-7 2011)

      Volume: 1 Issue: SRMS-7

    • DOI

      10.1017/s2044820111000013

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of Coherent X-ray Diffraction Apparatus with Kirkpatrick-Baez Mirror Optics2011

    • Author(s)
      Y.Takahashi, R.Tsutsumi, H.Kubo, Y.Nishino, H.Mimura, S.Matsuyama, T.Ishikawa, K.Yamauchi
    • Journal Title

      AIP Conference Proceedings (The 10th International Conference on x-ray microscopy)

      Volume: 1635 Pages: 231-234

    • DOI

      10.1063/1.3625346

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Towards High-Resolution Ptychographic X-ray Diffraction Microscopy2011

    • Author(s)
      Y.Takahashi, A.Suzuki, N.Zettsu, Y.Kohmura, Y.Senba, H.Ohashi, K.Yamauchi, T.Ishikawa
    • Journal Title

      Physical Review B

      Volume: 83 Issue: 21 Pages: 214109-214109

    • DOI

      10.1103/physrevb.83.214109

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Multiscale element mapping of buried structures by ptychographic x-ray diffraction microscopy using anomalous scattering2011

    • Author(s)
      Y.Takahashi, A.Suzuki, N.Zettsu, Y.Kohmura, K.Yamauchi, T.Ishikawa
    • Journal Title

      Applied Physics Letters

      Volume: 99 Issue: 13 Pages: 131905-131905

    • DOI

      10.1063/1.3644396

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High-Resolution Projection Image Reconstruction of Thick Objects by Hard X-ray Diffraction Microscopy2010

    • Author(s)
      Y. Takahashi, Y. Nishino, R. Tsutsumi, N. Zettsu, E. Matsubara, K. Yamauchi and T. Ishikawa
    • Journal Title

      Phys. Rev. B

      Volume: 82 Pages: 214102-214102

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Three-dimensional electron density mapping of shape-controlled nanoparticle by focused hard x-ray diffraction microscopy2010

    • Author(s)
      Y. Takahashi, N. Zettsu, Y. Nishino, R. Tsutsumi, E. Matsubara, T. Ishikawa and K. Yamauchi
    • Journal Title

      Nano Lett.

      Volume: 10 Pages: 1922-1926

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Two-dimensional measurement of focused x-ray beam profile using coherent x-ray diffraction of isolated nanoparticle2010

    • Author(s)
      Y. Takahashi, H. Kubo, R. Tsutsumi, S. Sakaki, N. Zettsu, Y. Nishino, T. Ishikawa and K. Yamauchi
    • Journal Title

      Nuclear Instruments and Methods in Physics Research Section A : Accelerators, Spectrometers, Detectors and Associated Equipment

      Volume: 616 Pages: 266-269

    • Related Report
      2011 Final Research Report 2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] An experimental procedure for precise evaluation of electron density distribution of a nanostructured material by coherent x-ray diffraction microscopy2010

    • Author(s)
      Y. Takahashi, H. Kubo, Y. Nishino, H. Furukawa, R. Tsutsumi, K. Yamauchi, T. Ishikawa and E. Matsubara
    • Journal Title

      Rev. Sci. Instrum.

      Volume: 81 Pages: 33707-33707

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Three-dimensional electron density mapping of shape-controlled nanoparticle by focused hard x-ray diffraction microscopy2010

    • Author(s)
      Y.Takahashi, N.Zettsu, Y.Nishino, R.Tsutsumi, E.Matsubara, T.Ishikawa, K.Yamauchi
    • Journal Title

      Nano Letters

      Volume: 10 Pages: 1922-1926

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High-Resolution Projection Image Reconstruction of Thick Objects by Hard X-ray Diffraction Microscopy2010

    • Author(s)
      Y.Takahashi, Y.Nishino, R.Tsutsumi, N.Zettsu, E.Matsubara, K.Yamauchi, T.Ishikawa
    • Journal Title

      Physical Review B

      Volume: 82 Pages: 214102-214102

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] An experimental procedure for precise evaluation of electron density distribution of a nanostructured material by coherent x-ray diffraction microscopy2010

    • Author(s)
      Y.Takahashi, H.Kubo, Y.Nishino, H.Furukawa, R.Tsutsumi, K.Yamauchi, T.Ishikawa, E.Matsubara
    • Journal Title

      Review of Scientific Instruments

      Volume: 81 Pages: 33707-33707

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] X線集光ビームを利用したコヒーレント回折技術の開発と応用2012

    • Author(s)
      高橋幸生
    • Organizer
      アモルファス・ナノ材料第147委員会第112回研究会
    • Place of Presentation
      弘済会館
    • Year and Date
      2012-05-27
    • Related Report
      2011 Final Research Report
  • [Presentation] コヒーレントX線回折による構造可視化の新手法2012

    • Author(s)
      高橋幸生
    • Organizer
      多元物質科学研究所若手交流研究会
    • Place of Presentation
      東北大学多元物質科学研究所
    • Year and Date
      2012-02-24
    • Related Report
      2011 Final Research Report
  • [Presentation] コヒーレントX線回折による構造可視化の新手法2012

    • Author(s)
      高橋幸生
    • Organizer
      多元物質科学研究所若手交流研究会
    • Place of Presentation
      東北大学多元物質科学研究所(仙台市)(招待講演)
    • Year and Date
      2012-02-24
    • Related Report
      2011 Annual Research Report
  • [Presentation] 高分解能X線タイコグラフィーの開発と元素識別イメージング2012

    • Author(s)
      鈴木明大、高橋幸生、是津信行、香村芳樹、仙波泰得、大橋治彦、山内和人、石川哲也
    • Organizer
      第25回日本放射光学会年会
    • Place of Presentation
      鳥栖中央公民館(鳥栖市)
    • Year and Date
      2012-01-07
    • Related Report
      2011 Annual Research Report
  • [Presentation] 高分解能コヒーレントX線回折顕微法の現状と将来展望,様々なイメージング技術の現況と展望2012

    • Author(s)
      高橋幸生
    • Organizer
      日本顕微鏡学会の電顕技術開発若手研究部会ワークショップ
    • Place of Presentation
      名古屋ファインセラミックスセンター
    • Year and Date
      2012-01-05
    • Related Report
      2011 Final Research Report
  • [Presentation] 高分解能コヒーレントX線回折顕微法の現状と将来展望2012

    • Author(s)
      高橋幸生
    • Organizer
      日本顕微鏡学会の電顕技術開発若手研究部会ワークショップ「様々なイメージング技術の現況と展望」
    • Place of Presentation
      名古屋ファインセラミックスセンター(名古屋市)(招待講演)
    • Year and Date
      2012-01-05
    • Related Report
      2011 Annual Research Report
  • [Presentation] 高分解能走査型コヒーレントX線回折顕微法の開発と金属材料のナノ組織解析への応用2011

    • Author(s)
      鈴木明大、高橋幸生、山内和人、是津信行、香村芳樹、石川哲也
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      ロワジールホテル那覇(那覇市)
    • Year and Date
      2011-11-08
    • Related Report
      2011 Annual Research Report
  • [Presentation] 高分解能走査型コヒーレントX線回折顕微法の開発と金属材料のナノ組織解析への応用2011

    • Author(s)
      鈴木明大、高橋幸生、山内和人、是津信行、香村芳樹、石川哲也
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      沖縄コンベンションセンター
    • Year and Date
      2011-11-07
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of High-Resolution Ptychographic X-ray Diffraction Microscopy using Focused Hard X-ray Beam2011

    • Author(s)
      A.Suzuki, Y.Takahashi, N.Zettsu, Y.Kohmura, K.Yamauchi, T.Ishikawa
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2011
    • Place of Presentation
      Osaka University Nakanoshima Center, Osaka, Japan
    • Year and Date
      2011-11-01
    • Related Report
      2011 Annual Research Report
  • [Presentation] Element-Specific Ptychographic X-ray Diffraction Microscopy using Anomalous Scattering2011

    • Author(s)
      Y.Takahashi, A.Suzuki, N.Zettsu, Y.Kohmura, K.Yamauchi, T.Ishikawa
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2011
    • Place of Presentation
      Osaka University Nakanoshima Center, Osaka, Japan
    • Year and Date
      2011-11-01
    • Related Report
      2011 Annual Research Report
  • [Presentation] High-resolution coherent diffraction imaging using focused hard x-ray beam at SPring-82011

    • Author(s)
      Y. Takahashi, A. Suzuki, Y. Kohmura, Y. Nishino, K. Yamauchi and Tetsuya Ishikawa
    • Organizer
      CXS Annual Workshop 2011, Bio21 Institute
    • Place of Presentation
      Melbourne, Victoria, Australia
    • Year and Date
      2011-10-10
    • Related Report
      2011 Final Research Report
  • [Presentation] High-resolution coherent diffraction imaging using focused hard x-ray beam at SPring-82011

    • Author(s)
      Y.Takahashi, A.Suzuki, Y.Kohmura, Y.Nishino, K.Yamauchi, T.Ishikawa
    • Organizer
      CXS Annual Workshop 2011
    • Place of Presentation
      Bio21 Institute, Melbourne, Victoria, Australia(招待講演)
    • Year and Date
      2011-10-10
    • Related Report
      2011 Annual Research Report
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard x-ray beam2011

    • Author(s)
      Y. Takahashi
    • Organizer
      The 4th International Workshop on FEL Science, Peppers Beach Club and Spa, Palm Cove
    • Place of Presentation
      Cairns, Queensland, Australia
    • Year and Date
      2011-09-01
    • Related Report
      2011 Final Research Report
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard x-ray beam2011

    • Author(s)
      Y.Takahashi
    • Organizer
      The 4th International Workshop on FEL Science
    • Place of Presentation
      Cairns, Queensland, Australia(招待講演)
    • Year and Date
      2011-08-31
    • Related Report
      2011 Annual Research Report
  • [Presentation] Development of high-resolution coherent X-ray diffraction microscopy and its application in materials science2011

    • Author(s)
      Y. Takahashi
    • Organizer
      International conference on processing & manufacturing of advanced materials, Quebec city convention centre
    • Place of Presentation
      Quebec, Canada
    • Year and Date
      2011-08-03
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of high-resolution coherent X-ray diffraction microscopy and its application in materials science2011

    • Author(s)
      Y.Takahashi
    • Organizer
      International conference on processing & manufacturing of advanced materials
    • Place of Presentation
      Quebec city convention centre, Quebec, Canada(招待講演)
    • Year and Date
      2011-08-03
    • Related Report
      2011 Annual Research Report
  • [Presentation] X線集光ビームを利用したコヒーレント回折技術の開発と応用2011

    • Author(s)
      高橋幸生
    • Organizer
      アモルファス・ナノ材料第147委員会第112回研究会
    • Place of Presentation
      弘済会館(東京都)(招待講演)
    • Year and Date
      2011-05-27
    • Related Report
      2011 Annual Research Report
  • [Presentation] KBミラー集光X線を用いた高分解能走査型回折顕微法の開発2011

    • Author(s)
      鈴木明大、高橋幸生、堤良輔、西野吉則、松原英一郎、山内和人、石川哲也
    • Organizer
      第24回日本放射光学会年会
    • Place of Presentation
      エポカルつくば(筑波市)
    • Year and Date
      2011-01-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 高分解能コヒーレントX線回折顕微法による金銀ナノボックスの三次元電子密度マッピング2011

    • Author(s)
      堤良輔、高橋幸生、鈴木明大、西野吉則、是津信行、松原英一郎、石川哲也、山内和人
    • Organizer
      第24回日本放射光学会年会
    • Place of Presentation
      エポカルつくば(筑波市)
    • Year and Date
      2011-01-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 試料厚さの効果を考慮した高分解能コヒーレントX線回折顕微法2011

    • Author(s)
      高橋幸生、堤良輔、西野吉則、是津信行、松原英一郎、山内和人、石川哲也
    • Organizer
      第24回日本放射光学会年会
    • Place of Presentation
      エポカルつくば(筑波市)
    • Year and Date
      2011-01-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 試料厚さの効果を考慮した高分解能コヒーレントX線回折顕微法2011

    • Author(s)
      高橋幸生、堤良輔、西野吉則、是津信行、松原英一郎、山内和人、石川哲也
    • Organizer
      第24回日本放射光学会年会
    • Place of Presentation
      エポカルつくば
    • Year and Date
      2011-01-08
    • Related Report
      2011 Final Research Report
  • [Presentation] Development and application of high-resolution X-ray diffraction microscopy using advanced mirror optics2010

    • Author(s)
      Y.Takahashi
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2010
    • Place of Presentation
      大阪大学中之島センター(大阪市)
    • Year and Date
      2010-11-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development and application of high-resolution X-ray diffraction microscopy using advanced mirror optics2010

    • Author(s)
      Y. Takahashi
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2010
    • Place of Presentation
      Osaka University Nakanoshima Center, Osaka, Japan
    • Year and Date
      2010-11-24
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of high-resolution X-ray diffraction microscopy using Kirkpatrick and Baez mirrors2010

    • Author(s)
      R.Tsutsumi, Y.Takahashi, N.Zettsu, A.Suzuki, Y.Nishino, E.Matsubara, T.Ishikawa, K.Yamauchi
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2010
    • Place of Presentation
      大阪大学中之島センター(大阪市)
    • Year and Date
      2010-11-24
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development and application of high-resolution X-ray diffraction microscopy2010

    • Author(s)
      Y.Takahashi
    • Organizer
      International Symposium at Frontier Research Base for Global Young Researchers
    • Place of Presentation
      大阪大学銀杏会館(吹田市)
    • Year and Date
      2010-11-16
    • Related Report
      2010 Annual Research Report
  • [Presentation] 高分解能コヒーレントX線回折顕微法による金属ナノ粒子の三次元電子密度マッピング2010

    • Author(s)
      高橋幸生、是津信行、堤良輔、山内和人、西野吉則、石川哲也、松原英一郎
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      北海道大学(札幌市)
    • Year and Date
      2010-09-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] 高分解能コヒーレントX線回折顕微法による金属ナノ粒子の三次元電子密度マッピング2010

    • Author(s)
      高橋幸生、是津信行、堤良輔、山内和人、西野吉則、石川哲也、松原英一郎
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-09-25
    • Related Report
      2011 Final Research Report
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard X-ray beam2010

    • Author(s)
      Y.Takahashi, Y.Nishino, E.Matsubara, T.Ishikawa, K.Yamauchi
    • Organizer
      The 10th International Conference of X-ray Microscopy
    • Place of Presentation
      Chicago, Illinois, U.S.A
    • Year and Date
      2010-08-17
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard X-ray beam2010

    • Author(s)
      Y. Takahashi, Y. Nishino, E. Matsubara, T. Ishikawa and Kazuto Yamauchi
    • Organizer
      the 10th International Conference of X-ray Microscopy
    • Place of Presentation
      chicago, illinois, USA.
    • Year and Date
      2010-08-16
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of coherent x-ray diffraction microscopy and its application in materials science2010

    • Author(s)
      Y.Takahashi
    • Organizer
      The 7th International Conference on Synchrotron Radiation in Materials Science
    • Place of Presentation
      The Said Business School, Oxford, UK
    • Year and Date
      2010-07-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development of coherent x-ray diffraction microscopy and its application in materials science2010

    • Author(s)
      Y. Takahashi
    • Organizer
      The 7th International Conference on Synchrotron Radiation in Materials Science
    • Place of Presentation
      Oxford, UK
    • Year and Date
      2010-07-12
    • Related Report
      2011 Final Research Report
  • [Book] SPring-8 Research Frontiers 20102011

    • Author(s)
      Y.Takahashi, N.Zettsu
    • Publisher
      SPring-8
    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www-up.prec.eng.osaka-u.ac.jp/takahashi/

    • Related Report
      2011 Final Research Report
  • [Remarks]

    • URL

      http://www-up.prec.eng.osaka-u.ac.jp/takahashi/

    • Related Report
      2011 Annual Research Report
  • [Remarks]

    • URL

      http://www.wakate.frc.eng.osaka-u.ac.jp/takahashi/

    • Related Report
      2010 Annual Research Report

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Published: 2010-08-23   Modified: 2016-04-21  

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