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Solid-state 33S NMR study of organic solids

Research Project

Project/Area Number 22750009
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Physical chemistry
Research InstitutionTokyo Institute of Technology

Principal Investigator

YAMADA Kazuhiko  東京工業大学, 理工学研究科, 助教 (80373380)

Project Period (FY) 2010-04-01 – 2013-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2012: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2011: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2010: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywords硫黄 / NMR / 有機物 / 生体分子 / 生物物理化学 / 分子構造
Research Abstract

Nuclear magnetic resonance (NMR) is one of the most standard analytical methods in chemistry and biochemistry. In this measurement, the NMR signal can provide valuable information on the molecule and electronic properties of a sample. The selectivity of an atom as a measuring target is one of the important features in this method, but a hydrogen or a carbon atom is mostly used in conventional NMR experiments. In this research, I try to develop the NMR method of sulfur-33 in organic and biological solids.

Report

(4 results)
  • 2013 Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (41 results)

All 2014 2013 2012 2011 2010 Other

All Journal Article (10 results) (of which Peer Reviewed: 3 results) Presentation (31 results) (of which Invited: 5 results)

  • [Journal Article] A Visible-light-responsive Photocatalyst of Nitrogen-doped Solid Acid HNb_3O_8-N Studied by Ultra-high-field 1H MAS NMR and ^1H^<-93>Nb/^1H^<-15>N HETCOR NMR in Solids2014

    • Author(s)
      T. Shimizu, T. Nakai, K. Deguchi, K. Yamada, B. Yue, and J. Ye
    • Journal Title

      Chem. Lett

      Volume: 43 Pages: 80-82

    • Related Report
      2013 Final Research Report
  • [Journal Article] A Visible-light-responsive Photocatalyst of Nitrogen-doped Solid Acid HNb3O8-N Studied by Ultra-high-field 1H MAS NMR and 1H-93Nb/1H-15N HETCOR NMR in Solids2014

    • Author(s)
      Shimizu, T., Nakai, T., Deguchi, K., Yamada, K., Yue, B., Ye, J
    • Journal Title

      Chem. Lett

      Volume: 43 Pages: 80-82

    • NAID

      130004427089

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Solid-state ^<13>C NMR Study of Cholesteric Liquid Crystals2013

    • Author(s)
      K. Yamada, K. Marumo, S. Kang, K. Deguchi, T. Nakai, T. Shimizu, and J. Watanabe
    • Journal Title

      J. Phys. Chem. B

      Volume: 117 Pages: 16325-16335

    • Related Report
      2013 Final Research Report
  • [Journal Article] Structural Analysis of a Banana-Liquid Crystal in the B4 Phase by Solid-State NMR2013

    • Author(s)
      K. Yamada, S. Kang, K Takimoto, M. Hattori, K. Shirata, S. Kawauchi, K. Deguchi, T. Shimizu, and J. Watanabe
    • Journal Title

      J. Phys. Chem. B

      Volume: 117 Pages: 6830-6838

    • Related Report
      2013 Final Research Report 2012 Annual Research Report
  • [Journal Article] A Solid-State ^<93>Nb NMR Study of Nitrogen-Doped Lamellar Niobic Acid2013

    • Author(s)
      K. Yamada, T. Shimizu, T. Nakai, K. Deguchi, B. Yue, and J. Ye
    • Journal Title

      Chem. Lett

      Volume: 42 Pages: 1223-1224

    • NAID

      10031201317

    • Related Report
      2013 Final Research Report
  • [Journal Article] Solid-state NMR and wide-angle X-ray diffraction study of hydrofluoroether/β-cyclodextrin inclusion complex2013

    • Author(s)
      Y. Koito, K. Yamada, S. Ando
    • Journal Title

      J. Incl. Phenom. Macrocycl. Chem

      Volume: 76 Pages: 143-150

    • Related Report
      2013 Final Research Report
  • [Journal Article] Solid-state 13C NMR Study of Cholesteric Liquid Crystals,2013

    • Author(s)
      Yamada, K., Marumo, K., Kang, S., Deguchi, K., Nakai, T., Shimizu, T., Watanabe, J.,
    • Journal Title

      J. Phys. Chem. B

      Volume: 117 Pages: 16325-16335

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A Solid-State 93Nb NMR Study of Nitrogen-Doped Lamellar Niobic Acid2013

    • Author(s)
      Yamada, K., Shimizu, T., Nakai, T., Deguchi, K., Yue, B., Ye, J.
    • Journal Title

      Chem. Lett

      Volume: 42 Pages: 1223-1224

    • NAID

      10031201317

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Valence XPS, IR, and ^<13>C NMR spectral analysis of 6 polymers by quantum chemical calculations2012

    • Author(s)
      K. Endo, T. Ida, S. Shimada, J. V. Ortiz, K. Deguchi, T. Shimizu, K. Yamada
    • Journal Title

      J. Mol. Struct

      Volume: 1027 Pages: 20-30

    • Related Report
      2013 Final Research Report
  • [Journal Article] A solid-state NMR study of boric acid doped in Poly(vinyl Alcohol), In "NMR Spectroscopy of Polymers : Innovative NMR Strategies for Complex Macromolecular Systems"2011

    • Author(s)
      K. Yamada
    • Journal Title

      American Chemical Society; ACS series book

      Volume: 8 Pages: 133-146

    • Related Report
      2013 Final Research Report
  • [Presentation] 半整数四極子核固体NMR 法が切り開く材料開発2014

    • Author(s)
      山田和彦
    • Organizer
      NIMS 微細構造解析プラットフォーム 2013年度第3回地域セミナー
    • Place of Presentation
      茨城
    • Year and Date
      2014-02-04
    • Related Report
      2013 Final Research Report
  • [Presentation] 半整数四極子核固体NMR 法の基礎と応用2014

    • Author(s)
      山田和彦
    • Organizer
      第39回先端計測オープンセミナー
    • Place of Presentation
      茨城
    • Year and Date
      2014-01-24
    • Related Report
      2013 Final Research Report
  • [Presentation] 半整数四極子核固体NMR 法の基礎と応用2013

    • Author(s)
      山田和彦
    • Organizer
      お茶の水女子大学理学部化学科公開セミナー
    • Place of Presentation
      東京
    • Year and Date
      2013-11-05
    • Related Report
      2013 Final Research Report
  • [Presentation] 固体NMRの基礎2013

    • Author(s)
      山田和彦
    • Organizer
      固体NMRの基礎
    • Place of Presentation
      京都
    • Year and Date
      2013-10-25
    • Related Report
      2013 Final Research Report
  • [Presentation] 酸素NMR法を用いた水分子の動的挙動解析2013

    • Author(s)
      山田和彦
    • Organizer
      第54回固体NMR・材料フォーラム
    • Place of Presentation
      奈良
    • Year and Date
      2013-10-24
    • Related Report
      2013 Final Research Report
  • [Presentation] A Solid-state 17O NMR Study of molecular dynamics for water in organic compounds2013

    • Author(s)
      K. Yamada, S. Yamada, N. Sako, K. Deguchi, T. Shimizu, and J. Watanabe
    • Organizer
      第52回NMR 討論会, 日本核磁気共鳴学会
    • Place of Presentation
      石川県立音楽堂
    • Related Report
      2013 Final Research Report
  • [Presentation] 固体核磁気共鳴法を用いたPB-10 Polyesterにおけるラメラ構造解析2013

    • Author(s)
      山田和彦, 吉原俊輔, 高橋千春, 姜聲敏, 戸木田雅利, 出口健三, 清水禎, 渡辺順次
    • Organizer
      第62回高分子討論会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Final Research Report 2012 Annual Research Report
  • [Presentation] A Solid-state 17O NMR Study of molecular dynamics for water in organic compounds2013

    • Author(s)
      Yamada, K., Yamada, S., Sako, N., Deguchi, K., Shimizu, T., Watanabe, J
    • Organizer
      第52回NMR討論会
    • Place of Presentation
      金沢大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 四極子核固体NMRの基礎と応用2012

    • Author(s)
      山田和彦
    • Organizer
      第38回理研ケミカルバイオロジー領域研究会
    • Place of Presentation
      理化学研究所和光研究所
    • Year and Date
      2012-05-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Structural Analysis of Banana Liquid Crystals2012

    • Author(s)
      K. Yamada, S. Kang, K. Takimoto, E. W. Lee, T. Shimizu, and J. Watanabe
    • Organizer
      The 1st Asian Conference on Liquid Crystals
    • Place of Presentation
      Japanese Liquid Crystal Society, Fuji Calm Shizuoka, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] A Solid-state NMR Study of Banana Liquid Crystals2012

    • Author(s)
      K. Yamada, S. Kang, E. W. Lee, E-J. Choi, K. Deguchi, T. Shimizu and J. Watanabe
    • Organizer
      第51回NMR討論会
    • Place of Presentation
      日本核磁気共鳴学会, ウインクあいち
    • Related Report
      2013 Final Research Report
  • [Presentation] 固体NMR法を用いたバナナ型液晶分子の構造解析2012

    • Author(s)
      山田 和彦
    • Organizer
      第51回NMR討論会(日本核磁気共鳴学会)
    • Place of Presentation
      名古屋
    • Related Report
      2011 Annual Research Report
  • [Presentation] Structural analysis of banana liquid crystals2012

    • Author(s)
      山田 和彦
    • Organizer
      ACLC2012
    • Place of Presentation
      富士吉田
    • Related Report
      2011 Annual Research Report
  • [Presentation] 半整数四極子核固体NMR法の基礎と応用2012

    • Author(s)
      山田 和彦
    • Organizer
      ケミカルバイオロジー・理研セミナー
    • Place of Presentation
      和光市
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] 固体NMRを用いたポリビニルアルコールにおけるホウ酸架橋構造に関する考察2011

    • Author(s)
      山田和彦, 他5名
    • Organizer
      高分子学会固体NMR研究会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2011-12-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 多核固体NMR法を用いたポリビニルアルコールにおけるホウ酸架橋構造解析2011

    • Author(s)
      山田和彦
    • Organizer
      第14回固体NMR技術交流会
    • Place of Presentation
      東京工業大学すずかけ台キャンパス
    • Year and Date
      2011-11-29
    • Related Report
      2013 Final Research Report
  • [Presentation] 多核固体NMR法を用いたポリビニルアルコールにおけるホウ酸架橋構造の解析2011

    • Author(s)
      山田和彦
    • Organizer
      第14回固体NMR技術交流会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2011-11-29
    • Related Report
      2010 Annual Research Report
  • [Presentation] New insights into cross-linking structures of boric acid doped in poly(vinyl alcohol)2011

    • Author(s)
      K.Yamada
    • Organizer
      第50回NMR討論会記念国際シンポジウム
    • Place of Presentation
      横浜大桟橋ホール
    • Year and Date
      2011-11-18
    • Related Report
      2010 Annual Research Report
  • [Presentation] 超高磁場多核固体NMR法を用いたポリビニルアルコールにおけるホウ酸架橋構造解析2011

    • Author(s)
      山田和彦、清水禎、出口健三
    • Organizer
      文部科学省先端研究施設共用イノベーション創出事業ナノテクノロジー・ネットワーク平成23年度成果報告
    • Place of Presentation
      東京工業大学
    • Year and Date
      2011-11-08
    • Related Report
      2010 Annual Research Report
  • [Presentation] 固体1H,11B NMRを用いたポリビニルアルコールにおけるホウ酸架橋構造に関する考察2011

    • Author(s)
      山田和彦、清水禎、出口健三、鎌田英樹、小林利章
    • Organizer
      第60回高分子討論会
    • Place of Presentation
      岡山大学
    • Year and Date
      2011-09-29
    • Related Report
      2010 Annual Research Report
  • [Presentation] A Solid-state NMR study of boric acid doped in poly(vinyl alcohol)2011

    • Author(s)
      K.Yamada, T.Shimizu, K, Deguchi, H。Kamada, T.Kobayashi
    • Organizer
      EUROMAR 2011
    • Place of Presentation
      ドイツ・フランクフルト市
    • Year and Date
      2011-08-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] 高磁場固体NMR法を用いたポリビニルアルコールにおけるホウ酸架橋構造の解析2011

    • Author(s)
      山田和彦、清水禎、出口健三、鎌田英樹、小林利章
    • Organizer
      第60回高分子学会年次学会
    • Place of Presentation
      大阪国際会議場
    • Year and Date
      2011-05-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] New Insights into Cross-linking Structures of Boric Acid Doped in Poly(vinyl alcohol)2011

    • Author(s)
      K. Yamada, K. Deguchi, T. Shimizu, S. Ando, H. Kamada, T. Kobayashi
    • Organizer
      The International Symposium on Nuclear Magnetic Resonance
    • Place of Presentation
      Yokohama, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] 固体1H, 11B-NMR を用いたポリビニルアルコールにおけるホウ酸架橋構造に関する考察2011

    • Author(s)
      山田和彦, 出口健三, 清水禎, 安藤慎二, 鎌田英樹, 小林利章
    • Organizer
      第60回高分子討論会
    • Place of Presentation
      岡山大学
    • Related Report
      2013 Final Research Report
  • [Presentation] A Solid-state NMR Study of Boric Acid Doped in Poly(vinyl alcohol)2011

    • Author(s)
      K. Yamada, K. Deguchi, T. Shimizu, S. Ando, H. Kamada, T. Kobayashi
    • Organizer
      EUROMAR
    • Place of Presentation
      Groupement Ampere, Frankfurt, Germany
    • Related Report
      2013 Final Research Report
  • [Presentation] 高磁場固体NMR法を用いたポリビニルアルコールにおけるホウ酸架橋構造の解析2011

    • Author(s)
      山田和彦, 出口健三, 清水禎, 安藤慎二, 鎌田英樹, 小林利章
    • Organizer
      第60回高分子学会年次会
    • Place of Presentation
      大阪国際会議場
    • Related Report
      2013 Final Research Report
  • [Presentation] 四極子核固体NMRスペクトル解析の基礎と応用2010

    • Author(s)
      山田和彦
    • Organizer
      第48回固体NMR・材料フォーラムおよび第5回NIMSナノ計測センターシンポジウム
    • Place of Presentation
      物質・材料研究機構
    • Year and Date
      2010-10-14
    • Related Report
      2013 Final Research Report
  • [Presentation] 酸素NMR法を用いた水分子の動的挙動解析

    • Author(s)
      山田和彦
    • Organizer
      第54 回固体NMR・材料フォーラム
    • Place of Presentation
      奈良女子大学
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] 固体NMRの基礎

    • Author(s)
      山田和彦
    • Organizer
      高分子学会第25回NMR講座
    • Place of Presentation
      京都大学
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] 半整数四極子核固体NMR法の基礎と応用

    • Author(s)
      山田和彦
    • Organizer
      第39回先端計測オープンセミナー
    • Place of Presentation
      物質・材料研究機構
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] 半整数四極子核固体NMR法が切り開く材料開発

    • Author(s)
      山田和彦
    • Organizer
      NIMS 微細構造解析プラットフォーム 2013年度 第3回地域セミナー
    • Place of Presentation
      物質・材料研究機構
    • Related Report
      2012 Annual Research Report
    • Invited

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Published: 2010-08-23   Modified: 2019-07-29  

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