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Fabrication of glass-ceramics containing nanocrystallites of oxide semiconductor and metal nanoparticles

Research Project

Project/Area Number 22750182
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Inorganic industrial materials
Research InstitutionKyoto University

Principal Investigator

MASAI Hirokazu  京都大学, 化学研究所, 助教 (10451543)

Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2012: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2011: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2010: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywordsガラス / セラミックス / 複合材料・物性 / ナノ材料 / 結晶化ガラス / 酸化物ガラス / 結晶化
Research Abstract

We have investigated the preparation condition of transparent glass-ceramics containing TiO2or ZnO nanocrystalllites. The preparation of dielectric nano-crystallites and metal nano-particles has also examined. We have demonstrated a surface orientated crystallization (ZnO) or a phase selective crystallization (TiO2) by careful investigation of relationship between chemical composition of glass and the precipitated crystalline phase. On the other hand, we examined correlation between the melt-temperature and network structure ofglass, and reported Pt nano-crystallites containing glass and the glass-ceramics. These results have shown that self-organized heterogeneous nanostructure can be made in a monolithic glass-ceramics.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (20 results)

All 2012 2011 2010 Other

All Journal Article (13 results) (of which Peer Reviewed: 13 results) Presentation (4 results) Book (2 results) Remarks (1 results)

  • [Journal Article] Effect of melt temperature on the structure of BaO-TiO2-GeO2glass2012

    • Author(s)
      正井博和、浜口克己、岩崎謙一郎、井原梨恵、高橋儀宏、藤原巧
    • Journal Title

      Materials Research Bulletin

      Volume: Vol.47No.12 Pages: 4065-4070

    • URL

      http://dx.doi.org/10.1016/j.materresbull.2012.08.058

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] 、Formation of TiO2 Nanocrystallites in the TiO2-ZnO-B2O3-Al2O3 Glass-Ceramics2012

    • Author(s)
      正井博和、平川圭佑、吉田和貴、宮崎孝道、高橋儀宏、井原梨恵、藤原巧
    • Journal Title

      Journal of American Ceramics Society

      Volume: Vol.95No.10 Issue: 10 Pages: 3138-3143

    • DOI

      10.1111/j.1551-2916.2012.05397.x

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation of Pt Nano-Crystallites from BaO-TiO2-GeO2 Re-Melted Glass2012

    • Author(s)
      正井博和、浜口克己、鈴木善之、岩崎謙一郎、井原梨恵、高橋儀宏、藤原巧
    • Journal Title

      Journal of Applied Physics

      Volume: Vol.111No.12

    • URL

      http://dx.doi.org/10.1063/1.4729488

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation of Pt Nano-Crystallites from BaO-TiO2-GeO2 Re-Melted Glass2012

    • Author(s)
      正井博和
    • Journal Title

      Jouranl of Applied Physics

      Volume: 111 Issue: 12 Pages: 123513-123513

    • DOI

      10.1063/1.4729488

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of melt temperature on the structure of BaO-TiO2-GeO2 glass2012

    • Author(s)
      正井博和
    • Journal Title

      Materials Research Bulletin

      Volume: 47 Issue: 12 Pages: 4065-4070

    • DOI

      10.1016/j.materresbull.2012.08.058

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation of ZnO in Al_2O_3-doped zinc borate glass ceramics2011

    • Author(s)
      H.Masai
    • Journal Title

      Optical Materials

      Volume: 33 Issue: 12 Pages: 1980-1983

    • DOI

      10.1016/j.optmat.2011.03.051

    • Related Report
      2012 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Correlation between Surface- Crystallized ZnO and the Amount of Al2O3in Borate-Based Glass-Ceramics2011

    • Author(s)
      正井博和、上野貴寛、高橋儀宏、藤原巧
    • Journal Title

      Journal of American Ceramics Society

      Volume: Vol.94No.8 Issue: 8 Pages: 2452-2457

    • DOI

      10.1111/j.1551-2916.2011.04604.x

    • Related Report
      2012 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Processing and photoluminescence properties of surface crystallized ZnO glass-ceramics2010

    • Author(s)
      正井博和、上野貴寛、戸田達也、高橋儀宏、藤原巧
    • Journal Title

      Journal of Non-Crystalline Solids

      Volume: Vol.356No.52-54 Pages: 3080-3084

    • URL

      http://dx.doi.org/10.1016/j.jnoncrysol.2010.04.055

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Surface crystallization of CaO-Bi2O3-B2O3-Al2O3-TiO2glass using IR furnace2010

    • Author(s)
      正井博和、金森英児、高橋儀宏、藤原巧
    • Journal Title

      Journal of Non-Crystalline Solid

      Volume: Vol.356,No.52-54 Pages: 2977-2979

    • URL

      http://dx.doi.org/10.1016/j.jnoncrysol.2010.03.046

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication of surface crystallized glasses with α-Zn3B2O6 and their optical property2010

    • Author(s)
      正井博和、上野貴寛、高橋儀宏、藤原巧
    • Journal Title

      Journal of Non-Crystalline Solids

      Volume: Vol.356,No.44-49 Pages: 2689-2692

    • URL

      http://dx.doi.org/10.1016/j.jnoncrysol.2010.04.046

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication of Bi-free TiO2nano-crystallized glass2010

    • Author(s)
      正井博和、戸田達也、高橋儀宏、藤原巧
    • Journal Title

      Journal of Non-Crystalline Solids

      Volume: Vol.356,No.44-49 Pages: 2674-2676

    • NAID

      130006980219

    • URL

      http://dx.doi.org/10.1016/j.jnoncrysol.2010.04.047

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation of heterogeneous nanostructures: Metal nanoparticles and dielectric nanocrystallites2010

    • Author(s)
      正井博和、高橋儀宏、藤原巧、徳田陽明、横 尾 俊 信
    • Journal Title

      Journal of Applied Physics

      Volume: Vol.108,No.2 Issue: 2

    • DOI

      10.1063/1.3457790

    • NAID

      120002514710

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation of heterogeneous nano-structure : Metal nanoparticles and dielectric nano-crystallites2010

    • Author(s)
      H.Masai, Y.Takahashi, T.Fujiwara, Y.Tokuda, T.Yoko
    • Journal Title

      Journal of Applied Physics

      Volume: 108

    • NAID

      120002514710

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] BaO-TiO2-GeO2再溶融ガラスにおける Pt ナノ結晶析出2012

    • Author(s)
      正井博和、浜口克己、岩崎謙一郎、井原梨恵、高橋儀宏、 藤原巧
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学
    • Year and Date
      2012-09-12
    • Related Report
      2012 Final Research Report
  • [Presentation] BaO-TiO2-GeO2再溶融ガラスにおけるPtナノ結晶析出2012

    • Author(s)
      正井博和
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Glass-Ceramics containing Nano-Crystallites of Oxide Semiconductor2011

    • Author(s)
      正井博和、 藤 原 巧
    • Organizer
      BIT's 1stannual world congress of nano-S&T 2011
    • Place of Presentation
      大連(中国)
    • Year and Date
      2011-10-26
    • Related Report
      2012 Final Research Report
  • [Presentation] Glass-Ceramics containing Nano-Crystallites of Oxide Semiconductor2011

    • Author(s)
      正井博和
    • Organizer
      BIT's 1st Annual World Congress of Nano-S&T-2011
    • Place of Presentation
      大連(中国)
    • Year and Date
      2011-10-26
    • Related Report
      2011 Annual Research Report
  • [Book] Glass-Ceramics Containing Nano-Crystallites of Oxide Semiconductor2010

    • Author(s)
      正井博和、高橋儀宏、藤原巧
    • Publisher
      Ceramic Materials
    • Related Report
      2012 Final Research Report
  • [Book] Glass-Ceramics Containing Nano-Crystallites of Oxide Semiconductor (Ceramic Materials)2010

    • Author(s)
      H.Masai, Y.Takahashi, T.Fujiwara(分担)
    • Publisher
      Sciyo社
    • Related Report
      2010 Annual Research Report
  • [Remarks]

    • URL

      http://noncry.kuicr.kyoto-u.ac.jp

    • Related Report
      2012 Final Research Report

URL: 

Published: 2010-08-23   Modified: 2019-07-29  

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