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Development of Stress Relaxation probe microscopy for Nanorheology Mapping

Research Project

Project/Area Number 22750195
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Polymer/Textile materials
Research InstitutionTohoku University

Principal Investigator

FUJINAMI So  東北大学, 原子分子材料科学高等研究機構, 助教 (50455325)

Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2012: ¥390,000 (Direct Cost: ¥300,000、Indirect Cost: ¥90,000)
Fiscal Year 2011: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2010: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Keywords応力緩和 / 粘弾性 / ゴム弾性 / 原子間力顕微鏡 / ゴム材料 / 高分子構造・物性 / 高分子材料物性
Research Abstract

Based on atomic force microscopy (AFM), I have developed “AFM load relaxation measurement technique," in which an AFM probe is pushed on a sample surface and then kept the position so that the relaxing load is measured. I fulfilled quantitative measurement of therelaxation behavior of elastic materials caused by viscoelasticity and adhesion of the surface. I also extended the system to mapping measurement so that the distribution of viscoelasticity can be visualized on nanoscale lateral resolution. The mapping system showed the capability of application to evaluate the nanomechanical properties of elastomer composite materials.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (15 results)

All 2012 2011 2010

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (14 results)

  • [Journal Article] Viscoelasticity Analysis of Elastomer Blend Using Force Measurements of Atomic Force Microscope2012

    • Author(s)
      藤波想、中嶋健、西俊夫
    • Journal Title

      KOBUNSHI RONBUNSHU

      Volume: 69 Issue: 7 Pages: 435-442

    • DOI

      10.1295/koron.69.435

    • NAID

      10030932501

    • ISSN
      0386-2186, 1881-5685
    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Presentation] Viscoelasticity and Adhesion, Extended JKR theory in ForceMeasurement2011

    • Author(s)
      藤波想
    • Organizer
      19th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      洞爺湖 万世閣
    • Year and Date
      2011-12-19
    • Related Report
      2012 Final Research Report
  • [Presentation] Viscoelasticity and Adhesion, Extended JKR theory in Force Measurement2011

    • Author(s)
      藤波想
    • Organizer
      19th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      洞爺湖方世閣
    • Year and Date
      2011-12-19
    • Related Report
      2011 Annual Research Report
  • [Presentation] AFMフォース測定によるナノスケール粘弾性評価2011

    • Author(s)
      藤波想
    • Organizer
      第59回レオロジー討論会
    • Place of Presentation
      桐生市市民文化会館
    • Year and Date
      2011-10-06
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] 高分子表面のナノレオロジー[IX]-周波数依存性2011

    • Author(s)
      藤波想
    • Organizer
      第60回高分子討論会
    • Place of Presentation
      岡山大学津山キャンパス
    • Year and Date
      2011-09-28
    • Related Report
      2012 Final Research Report
  • [Presentation] 高分子表面のナノレオロジー[IX]-周波数依存性2011

    • Author(s)
      藤波想
    • Organizer
      第60回高分子討論会
    • Place of Presentation
      岡山大学津島キャンパス
    • Year and Date
      2011-09-28
    • Related Report
      2011 Annual Research Report
  • [Presentation] 原子間力顕微鏡を用いた粘弾性の高分解能画像化手法52011

    • Author(s)
      藤波想
    • Organizer
      日本ゴム協会2011年年次大会
    • Place of Presentation
      東京理科大学森戸記念館
    • Year and Date
      2011-05-30
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] 高分子表面のナノレオロジー[VIII]-粘弾性測定手法の最近の進展2011

    • Author(s)
      藤波想
    • Organizer
      第60回高分子学会年次大会
    • Place of Presentation
      大阪国際会議場
    • Year and Date
      2011-05-26
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] Method to derive viscoelasticity and adhesion separately from force measurement 22010

    • Author(s)
      藤波 想
    • Organizer
      18th International Conference of Scanning Probe Microscopy
    • Place of Presentation
      熱川ハイツ (伊豆熱川)
    • Year and Date
      2010-12-09
    • Related Report
      2012 Final Research Report
  • [Presentation] Method to derive viscoelasticity and adhesion separately from force measurement 22010

    • Author(s)
      So Fujinami, Dong Wang, Hao Liu, Ken Nakajima, Toshio Nishi
    • Organizer
      18^<th> International Conference of Scanning Probe Microscopy (ICSPM18)
    • Place of Presentation
      熱川ハイツ(伊豆熱川)
    • Year and Date
      2010-12-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] 原子間力顕微鏡を用いた粘弾性の高分解能測定手法42010

    • Author(s)
      藤波想
    • Organizer
      第22回エラストマー討論会
    • Place of Presentation
      京都工芸繊維大学
    • Year and Date
      2010-12-02
    • Related Report
      2012 Final Research Report 2010 Annual Research Report
  • [Presentation] フォースボリュームモードAFMによるナノ力学物性測定とその表面物性評価への応用[IV]2010

    • Author(s)
      藤波想
    • Organizer
      第58回レオロジー討論会
    • Place of Presentation
      仙台国際センター
    • Year and Date
      2010-10-06
    • Related Report
      2012 Final Research Report
  • [Presentation] フォースボリュームモードAFMによるナノ力学物性測定とその表面物性評価への応用[IV]2010

    • Author(s)
      藤波想・中嶋健・西敏夫
    • Organizer
      2010年度レオロジー討論会
    • Place of Presentation
      仙台国際センター
    • Year and Date
      2010-10-06
    • Related Report
      2010 Annual Research Report
  • [Presentation] Novel technique to visualize nanoscle viscoelastic distribution based on atomic force microscopy2010

    • Author(s)
      藤波想
    • Organizer
      5th Pacific Rim Conference on Rheology
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-08-02
    • Related Report
      2012 Final Research Report
  • [Presentation] Novel technique to visualize nanoscle viscoelastic distribution based on atomic force microscopy2010

    • Author(s)
      So Fujinami, Dong Wang, Ken Nakajima, Toshio Nishi
    • Organizer
      5^<th> Pacific Rim Conference on Rheology (PRCR-5)
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-08-02
    • Related Report
      2010 Annual Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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