Development of scanning three-dimensional x-ray diffraction microscopy and in-situ observation of plastic deformation of polycrystalline metals
Project/Area Number |
22760571
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Research Category |
Grant-in-Aid for Young Scientists (B)
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Allocation Type | Single-year Grants |
Research Field |
Material processing/treatments
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Research Institution | Toyota Central R&D Lab., Inc. |
Principal Investigator |
HAYASHI Yujiro 株式会社豊田中央研究所, 分析・計測研究部 ナノ解析研究室, 研究員 (30435953)
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Project Period (FY) |
2010 – 2012
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Project Status |
Completed (Fiscal Year 2012)
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Budget Amount *help |
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2011: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Fiscal Year 2010: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
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Keywords | 塑性加工 / 放射光 / X線回折 / その場観察 / 塑性変形 / 3DXRD顕微鏡法 / 多結晶 / 金属材料 / 多結晶金属材料 |
Research Abstract |
The three-dimensional x-ray diffraction (3DXRD) microscopy is a novel method for non-destructively three-dimensional observation of crystal orientation and stress of each crystal grain in polycrystalline metallic materials. It may be often difficulty to observe ideal polycrystalline deformation in a typical measurement technique due to the limit of number of grains in an observed cross section. In this study, the approach named scanning 3DXRD which allows us to observe specimens with as a large number of grains as possible in the cross section is proposed. The principle of the scanning 3DXRD that identifies the grain at an arbitrary point in a specimen was experimentally proved. The BCC slip deformation of a polycrystalline ferrite was observed from in-situ three-dimensional mapping of orientation under a tensile load.
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Report
(3 results)
Research Products
(10 results)