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Evaluation of grain-boundaries and critical current properties in MgB2 superconductors

Research Project

Project/Area Number 22860019
Research Category

Grant-in-Aid for Research Activity Start-up

Allocation TypeSingle-year Grants
Research Field Physical properties of metals
Research InstitutionThe University of Tokyo

Principal Investigator

YAMAMOTO Akiyasu  東京大学, 大学院・工学系研究科, 助教 (20581995)

Project Period (FY) 2010 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥3,146,000 (Direct Cost: ¥2,420,000、Indirect Cost: ¥726,000)
Fiscal Year 2011: ¥1,508,000 (Direct Cost: ¥1,160,000、Indirect Cost: ¥348,000)
Fiscal Year 2010: ¥1,638,000 (Direct Cost: ¥1,260,000、Indirect Cost: ¥378,000)
Keywords超伝導材料 / ナノ材料 / 環境材料
Research Abstract

We have studied the microstructure, normal-state electrical connectivity and critical current density of ex-situ MgB_2 polycrystalline bulks prepared using systematically varied heating conditions under ambient pressure. The samples heated at high-temperatures of~900℃for a long period showed an increased packing factor, a larger intergrain contact area and a significantly improved electrical connectivity, all of which show the evidence of solid-state self-sintering of MgB_2. The sintered ex-situ MgB_2 bulks from the laboratory-made prereacted MgB_2 powder showed largely enhanced connectivity of~20%, which is the highest among pressureless ex-situ MgB_2 bulks, wires and tapes. Owing to the improved inter-grain coupling, high critical current density exceeding 0. 3 MA/cm^2 at 20 K under self-field was achieved. This study shows that moderately high-temperature, long-time processing is a simple but forcible way to extract the superior current carrying potential of high bulk density ex-situ MgB_2 through strengthening of inter-grain coupling by the self-sintering.

Report

(3 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • Research Products

    (33 results)

All 2012 2011 2010

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (24 results) Book (2 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Towards the realization of higherconnectivity in MgB2 conductors-in-situor sintered ex-situ?2012

    • Author(s)
      A. Yamamoto, H. Tanaka, J. Shimoyama, H. Ogino, K. Kishio, and T. Matsushita
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 51巻 Pages: 0101051-6

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Towards the realization of higher connectivity in MgB2 conductors-in-situ or sintered ex-situ?2012

    • Author(s)
      A.Yamamoto, H.Tanaka, J.Shimoyama, H.Ogino, K.Kishio, T.Matsushita
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 51 Issue: 1R Pages: 010105-010105

    • DOI

      10.1143/jjap.51.010105

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Critical current properties at highmagnetic fields in polycrystalline MgB2 superconductors2010

    • Author(s)
      T. Matsushita, M. Kiuchi, E. S. Otabe, A. Yamamoto, J. Shimoyama, K. Kishio
    • Journal Title

      Physica C

      Volume: 470巻 Pages: 1406-1410

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] 磁場配向法によるc軸配向MgB2バルクの開発2010

    • Author(s)
      望月利彦, 山本明保, 荻野拓, 下山淳一, 岸尾光二, 堀井滋, 和田恭輔, 山田豊
    • Journal Title

      日本金属学会誌

      Volume: 74巻 Pages: 444-452

    • Related Report
      2011 Final Research Report 2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Critical current properties at high magnctic fields in polycrystalline MgB2 superconductors2010

    • Author(s)
      T.Matsushita, M.Kiuchi, E.S.Otabe, A.Yamamoto, J.Shimoyama, K.Kishio
    • Journal Title

      Physica C

      Volume: 470 Pages: 1406-1410

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] 高温焼結ex-situ法によるMgB2線材の作製2012

    • Author(s)
      山本明保,田中裕也,下山淳一,伊藤明植,荻野拓,岸尾光二
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      東京、日本
    • Year and Date
      2012-03-17
    • Related Report
      2011 Final Research Report
  • [Presentation] 高温焼結ex-situ法によるMgB2線材の作製2012

    • Author(s)
      山本明保, 田中裕也, 下山淳一, 伊藤明植, 荻野拓, 岸尾光二
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      早稲田大学(東京都)
    • Year and Date
      2012-03-17
    • Related Report
      2011 Annual Research Report
  • [Presentation] MgB2超電導線材および単結晶・バルク材の磁束ピンニング機構とJc制限因子、低温工学・超電導学会2011

    • Author(s)
      山本明保
    • Organizer
      第2回材料研究会/九州・西日本支部合同研究会
    • Place of Presentation
      福岡、日本
    • Year and Date
      2011-12-26
    • Related Report
      2011 Final Research Report
  • [Presentation] MgB2超電導線材および単結晶・バルク材の磁束ピンニング機構とJc制限因子2011

    • Author(s)
      山本明保
    • Organizer
      低温工学・超電導学会第2回材料研究会/九州・西日本支部合同研究会
    • Place of Presentation
      九州工業大学(福岡県)(招待講演)
    • Year and Date
      2011-12-26
    • Related Report
      2011 Annual Research Report
  • [Presentation] MgB4を介したMgB2バルクの作製2011

    • Author(s)
      伊藤明植,山本明保,田中裕也,下山淳一,荻野拓,岸尾光二
    • Organizer
      第85回2011年度秋季低温工学・超電導学会
    • Place of Presentation
      金沢、日本
    • Year and Date
      2011-11-11
    • Related Report
      2011 Final Research Report
  • [Presentation] Ex-situ法MgB2バルクの臨界電流特性における原料MgB2粉末依存性2011

    • Author(s)
      田中裕也,山本明保,伊藤明植,下山淳一,荻野拓,岸尾光二
    • Organizer
      第85回2011年度秋季低温工学・超電導学会
    • Place of Presentation
      金沢、日本
    • Year and Date
      2011-11-11
    • Related Report
      2011 Final Research Report
  • [Presentation] MgB4を介したMgB2バルクの作製2011

    • Author(s)
      伊藤明植, 山本明保, 田中裕也, 下山淳一, 荻野拓, 岸尾光二
    • Organizer
      第85回2011年度秋季低温工学・超電導学会
    • Place of Presentation
      金沢歌舞伎座(金沢県)
    • Year and Date
      2011-11-11
    • Related Report
      2011 Annual Research Report
  • [Presentation] Ex-situ法MgB2バルクの臨界電流特性における原料MgB2粉末依存性2011

    • Author(s)
      田中裕也, 山本明保, 伊藤明植, 下山淳一, 荻野拓, 岸尾光二
    • Organizer
      第85回2011年度秋季低温工学・超電導学会
    • Place of Presentation
      金沢歌舞伎座(金沢県)
    • Year and Date
      2011-11-11
    • Related Report
      2011 Annual Research Report
  • [Presentation] MgB2 Bulk Superconducting Magnet2011

    • Author(s)
      A. Yamamoto
    • Organizer
      The 15th Japan-US Workshop on Advanced Superconductors
    • Place of Presentation
      大阪、日本
    • Year and Date
      2011-10-29
    • Related Report
      2011 Final Research Report
  • [Presentation] MgB2 Bulk Superconducting Magnet2011

    • Author(s)
      A.Yamamoto
    • Organizer
      The 15th Japan-US Workshop on Advanced Super conductors
    • Place of Presentation
      住友倶楽部(大阪府)(招待講演)
    • Year and Date
      2011-10-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] Microstructure and critical current density of sinteredex-situ MgB2 polycrystals2011

    • Author(s)
      H. Tanaka, A. Yamamoto, J. Shimoyama, H. Ogino, K. Kishio
    • Organizer
      24 thInternational Symposium on Superconductivity
    • Place of Presentation
      東京、日本
    • Year and Date
      2011-10-24
    • Related Report
      2011 Final Research Report
  • [Presentation] Microstructure and critical current density of sintered ex-situ MgB2 polycrystals2011

    • Author(s)
      H.Tanaka, A.Yamamoto, J.Shimoyama, H.Ogino, K.Kishio
    • Organizer
      24th International Symposium on Superconductivity
    • Place of Presentation
      Funabori Tower Hall (東京都)
    • Year and Date
      2011-10-24
    • Related Report
      2011 Annual Research Report
  • [Presentation] Ex-situ法MgB2多結晶体のコネクティビティ(2)2011

    • Author(s)
      山本明保,田中裕也,下山淳一,伊藤明植,荻野拓,岸尾光二
    • Organizer
      第68回応用物理学会学術講演会
    • Place of Presentation
      山形、日本
    • Year and Date
      2011-09-01
    • Related Report
      2011 Final Research Report
  • [Presentation] Ex-situ法MgB2多結晶体のコネクティビティ(2)2011

    • Author(s)
      山本明保, 田中裕也, 下山淳一, 伊藤明植, 荻野拓, 岸尾光二
    • Organizer
      第68回応用物理学会学術講演会
    • Place of Presentation
      山形大学(山形県)
    • Year and Date
      2011-09-01
    • Related Report
      2011 Annual Research Report
  • [Presentation] Ex-situ法MgB2多結晶体のコネクティビティ2011

    • Author(s)
      山本明保,田中裕也,下山淳一,湯本英宏,荻野拓,岸尾光二
    • Organizer
      第58回応用物理学関係連合講演会
    • Place of Presentation
      日本
    • Year and Date
      2011-03-09
    • Related Report
      2011 Final Research Report
  • [Presentation] Ex-situ法MgB2多結晶体のコネクティビティ2011

    • Author(s)
      山本明保, 田中裕也, 下山淳一, 湯本英宏, 荻野拓, 岸尾光二
    • Organizer
      第58回応用物理学関係連合講演会
    • Place of Presentation
      厚木、日本
    • Year and Date
      2011-03-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] HPCVD法により作製したチルトMgB2薄膜の輸送臨界電流特性2010

    • Author(s)
      山本明保, Marina Putti, Anatolii Polyanskii, Fumitake Kametani, Dmytro Abraimov, Alexander Gurevich, David Larbalestier, Chenggang Zhuang, XiaoxingXi,下山淳一,岸尾光二
    • Organizer
      第83回2010年度秋季低温工学・超電導学会
    • Place of Presentation
      鹿児島、日本
    • Year and Date
      2010-12-01
    • Related Report
      2011 Final Research Report
  • [Presentation] HPCVD法により作製したチルトMgB2薄膜の輸送臨界電流特性2010

    • Author(s)
      山本明保, Marina Putti, Anatolii Polyanskii, Fumitake Kametani, Dmytro Abraimov, Alexander Gurevich, David Larbalestier, Chenggang Zhuang, Xiaoxing Xi, 下山淳一, 岸尾光二
    • Organizer
      第83回2010年度秋季低温工学・超電導学会
    • Place of Presentation
      鹿児島、日本(口頭発表)
    • Year and Date
      2010-12-01
    • Related Report
      2010 Annual Research Report
  • [Presentation] Development of MgB2 Bulk Superconducting Magnet2010

    • Author(s)
      A. Yamamoto, H. Yumoto, J. Shimoyama, K. Kishio, A. Ishihara, M. Tomita
    • Organizer
      23th International Symposium on Superconductivity
    • Place of Presentation
      つくば、日本
    • Year and Date
      2010-11-03
    • Related Report
      2011 Final Research Report
  • [Presentation] Development of MgB2 Bulk Superconducting Magnet2010

    • Author(s)
      A.Yamamoto, H.Yumoto, J.Shimoyama, K.Kishio, A.Ishihara, M.Tomita
    • Organizer
      23th International Symposium on Superconductivity
    • Place of Presentation
      つくば、日本(ポスター発表)
    • Year and Date
      2010-11-03
    • Related Report
      2010 Annual Research Report
  • [Presentation] Novel c-axisoriented ex-situ MgB2 conductors2010

    • Author(s)
      A. Yamamoto, T. Mochizuki, H. Tanaka, H. Ogino, J. Shimoyama, K. Kishio, S. Horii, K. Wada, Y. Yamada, Y. Shimada, S. Hata, K. Ikeda, H. Nakashima
    • Organizer
      Applied Superconductivity Conference 2010
    • Place of Presentation
      ワシントンDC、米国
    • Year and Date
      2010-08-05
    • Related Report
      2011 Final Research Report
  • [Presentation] Novel c-axis oriented ex-situ MgB2 conductors2010

    • Author(s)
      A.Yamamoto, T.Mochizuki, H.Tanaka, H.Ogino, J.Shimoyama, K.Kishio, S.Horii, K.Wada, Y.Yamada, Y.Shimada, S.Hata, K.Ikeda, H.Nakashima
    • Organizer
      Applied Superconductivity Conference 2010
    • Place of Presentation
      ワシントンDC、米国(口頭発表)
    • Year and Date
      2010-08-05
    • Related Report
      2010 Annual Research Report
  • [Presentation] Understanding the multi-band effects oncurrent transport in tilted MgB2 films2010

    • Author(s)
      A. Yamamoto, M. Putti, A. Polyanskii, F. Kametani, D. Abraimov, A. Gurevich, D. Larbalestier, C. Zhuang, X. Xi
    • Organizer
      Applied Superconductivity Conference 2010
    • Place of Presentation
      ワシントンDC、米国
    • Year and Date
      2010-08-02
    • Related Report
      2011 Final Research Report
  • [Presentation] Understanding the multi-band effects on current transport in tilted MgB2 films2010

    • Author(s)
      A.Yamamoto, M.Putti, A.Polyanskii, F.Kametani, D.Abraimov, A.Gurevich, D.Larbalestier, C.Zhuang, X.Xi
    • Organizer
      Applied Superconductivity Conference 2010
    • Place of Presentation
      ワシントンDC、米国(口頭発表)
    • Year and Date
      2010-08-02
    • Related Report
      2010 Annual Research Report
  • [Book] chemical doping andcritical current properties-2010

    • Author(s)
      A. Yamamoto, J. Shimoyama, K. Kishio
    • Total Pages
      33
    • Publisher
      Nova Science Publishers、Advances inCondensed Matter and Materials Research, Volume 6, Chapter 4. Development inmaterials processing of MgB2-microstructure
    • Related Report
      2011 Final Research Report
  • [Book] Advances in Condensed Matter and Materials Research, Volume 6 Chapter 4. Development in materials processing of MgB2・microstructure, chemical doping and critical current properties.2010

    • Author(s)
      A-Yamamoto, J. Shimoyama, K.Kishio
    • Total Pages
      33
    • Publisher
      Nova Science Publishers
    • Related Report
      2010 Annual Research Report
  • [Patent(Industrial Property Rights)] MgB2超電導バルク磁石の製造方法、およびMgB2超電導バルク磁石2010

    • Inventor(s)
      山本明保、富田優、岸尾光二、石原篤、下山淳一
    • Filing Date
      2010-10-29
    • Related Report
      2011 Final Research Report
  • [Patent(Industrial Property Rights)] MgB2超電導バルク磁石の製造方法、およびMgB2超電導バルク磁石2010

    • Inventor(s)
      山本明保、石原篤、富田優、下山淳一、岸尾光二
    • Industrial Property Rights Holder
      山本明保、石原篤、富田優、下山淳一一、岸尾光二
    • Industrial Property Number
      2010-244166
    • Filing Date
      2010-10-29
    • Related Report
      2010 Annual Research Report

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Published: 2010-08-27   Modified: 2016-04-21  

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