Effect of mesoscale material structure in laser shock-produced ultrahigh pressure conditions
Project/Area Number |
22K18702
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Research Category |
Grant-in-Aid for Challenging Research (Exploratory)
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Allocation Type | Multi-year Fund |
Review Section |
Medium-sized Section 14:Plasma science and related fields
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Research Institution | Osaka University |
Principal Investigator |
尾崎 典雅 大阪大学, 大学院工学研究科, 准教授 (70432515)
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Project Period (FY) |
2022-06-30 – 2025-03-31
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Project Status |
Granted (Fiscal Year 2023)
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Budget Amount *help |
¥6,500,000 (Direct Cost: ¥5,000,000、Indirect Cost: ¥1,500,000)
Fiscal Year 2024: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2023: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2022: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
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Keywords | 超高圧 / 極限状態 / 高強度レーザー / X線自由電子レーザー / メゾスケール構造 / アルミナ / ダイヤモンド / 結晶粒界 |
Outline of Research at the Start |
超高圧・超高ひずみ速度圧縮における物質極限状態に対して、バルク物質材料が有するマイクロメートルスケールまでのメゾスケール構造が及ぼす影響を、フェムト秒分解のX線プローブ計測・観察によって直接的に検討する。これまでの高圧物質科学やレーザー極限科学の研究では、メゾスケール物質構造の極限物質状態への影響はほとんど検討されてこなかった。高強度レーザー駆動の超高圧極限環境において、これらメゾ構造が物質のミクロとマクロにどのように影響しているかを、X線自由電子レーザー利用の超高速時間分解観察によって検討する。原子分子とマクロ材料を繋ぐ新しい領域で新たな知見の獲得や方法論の構築に寄与する。
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Outline of Annual Research Achievements |
ハイパワーレーザーショック圧縮とXFELプローブを組み合わせた超高速ポンププローブ法に基づいた実験を継続した。これまでに申請者らが確立してきたフェムト秒X線回折(XRD)の原子レベル観察と相補的に、高エネルギー密度物質状態に対するメゾスケール観察も継続することができた。アルミナやダイヤモンドなどのセラミックス材料の日本が強みを有する高圧合成技術などを駆使して、ナノ-サブミクロンレベルの結晶粒径、粒界、空孔などの影響を初めて実験的に検討した。数100万気圧レベルまでピーク圧力とひずみ速度を変化させたレーザーショックを駆動し、高エネルギー密度状態の物質に関して、以下の実験を実施した。 1)衝撃圧縮特性計測:アルミナ多結晶試料に対して400万気圧超までの超高圧状態を生成し、衝撃波速度を高精度に計測することで、機械力学的特性を明らかにした。結晶粒径に対する依存性を詳しく明らかにすることを念頭に、ナノ多結晶アルミナ試料の開発も並行して開始した。 2) XFEL-X線回折:約250万気圧程度までの圧力域において、多結晶アルミナ試料に対するX線自由電子レーザーX線回折観察を実施した。130万気圧領域周辺でのアルミナ結晶格子の圧縮非等方性、およびRh2O3高圧構造などへの構造相転移を観察した。 3)XFEL超解像ラディオグラフ:X線自由電レーザービームを超高圧縮状態のターゲットに非集光で照射することで、独自の撮像技術を用いたフェムト秒・サブミクロン分解の超解像ラディオグラフ観察を実施した。試料中を伝搬するショック波面およびその背後の圧縮状態に関して、単結晶および多結晶試料間の違いを観察した。
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Current Status of Research Progress |
Current Status of Research Progress
1: Research has progressed more than it was originally planned.
Reason
X線自由電子レーザーによる超高速X線回折では、高精度に格子変形を計測することで、多結晶系における材料強度が定量的に可視化できるようになってきた。また、独自に確立してきたフッ化リチウム結晶撮像素子を利用したラジオグラフでは、ショック波面およびその背後におけるマクロ-メゾ構造の影響を具体的に明らかにすることができるようになってきている。以下のような特筆すべき成果が創出されている。 1)多結晶アルミナにおいて400万気圧超までの衝撃圧縮状態を初めて明らかにできた。単結晶アルミナの衝撃圧縮曲線と定量的に比較可能なデータから圧縮率の変化を検討することができた。 2) X線自由電子レーザーを用いたX線回折パターンの観察から、250万気圧の圧力までで多結晶アルミナの圧縮の非等方性を初めて定量的に明らかにした。また約130万気圧の圧力では、アルミナ高圧相のRh2O3構造の生成を示唆する回折ピークが出現すること、およびこのRh2O3とアルミナが圧力平衡の混合状態になる可能性が初めて示された。 3)X線自由電レーザーを用いた超解像ラジオグラフ観察から、単結晶と多結晶試料において欠陥伝搬の様子が明瞭に異なることが初めて明らかになった。
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Strategy for Future Research Activity |
開発を開始しているナノ多結晶試料に対する実験に拡張する。線結像速度干渉計(VISAR)と放射輝度温度計(SOP)からなる可視光観察と、X線観察を組み合わせて、実験によるデータの蓄積を行う。X線回折により圧縮の非等方性と圧縮率、融点近傍までの衝撃圧縮状態方程式、サブテラパスカル域での放射特性、などを解明するとともに、単結晶およびミクロ多結晶試料の結果と比較検討する。結果の公表を速やかに行う。
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Report
(2 results)
Research Products
(102 results)
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[Journal Article] Indirect evidence for elemental hydrogen in laser-compressed hydrocarbons2023
Author(s)
D. Kraus , Chekrygina,,R. W. Falcone, L. B. Fletcher, S. Frydrych, E. Galtier, D. O. Gericke, S. H. Glenzer, E. Granados, Y. Inubushi, N. Kamimura, K. Katagiri, M. J. MacDonald,A. J. MacKinnon, T. Matsuoka, K. Miyanishi,N. Ozaki,
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Journal Title
Physical Review Research
Volume: 5
Issue: 2
DOI
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[Journal Article] Damage threshold of LiF crystal irradiated by femtosecond hard XFEL pulse sequence2023
Author(s)
S. Makarov, S.Grigoryev, N.Inogamov, E. Filippov, T. Pikuz, N.Ozaki, M.Ishino, M. Nishikino, Thanh-Hung Dinh, T. Kawachi, M. Zanaveskin, M. Makita, M. Nakatsutsumi, T. R. Preston, K. Appel, Z.Konopkova,
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Journal Title
Optics Express
Volume: 31
Issue: 16
Pages: 26383-26383
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[Journal Article] Direct imaging of shock wave splitting in diamond at Mbar pressure2023
Author(s)
S.Makarov,S.Dyachkov,T.Pikuz,K. Katagiri ,H. Nakamura,V.Zhakhovsky,N.Inogamov,V.Khokhlov,A.Martynenko,B.Albertazzi,G.Rigon,P.Mabey,N.J.Hartley,Y.Inubushi,K.Miyanishi,K.Sueda,T.Togashi,M.Yabashi,T.Yabuuchi,T.Okuchi,R.Kodama,S.Pikuz,M.Koenig,N. Ozaki
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Journal Title
Matter and Radiation at Extremes
Volume: 8
Issue: 6666
Pages: 066601-066601
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[Journal Article] Transonic dislocation propagation in diamond2023
Author(s)
K.Katagiri,T.Pikuz,L.Fang,B.Albertazzi,S.Egashira,Y.Inubushi,G.Kamimura,R.Kodama, M.Koenig, B.Kozioziemski, G.Masaoka, K.Miyanishi, H.Nakamura, M.Ota, G.Rigon, Y.Sakawa, T.Sano, F.Schoofs, Z. J. Smith, , and N. Ozaki
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Science
Volume: 382
Issue: 12
Pages: 69-72
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[Journal Article] Simultaneous bright- and dark-field X-ray microscopy at X-ray free electron lasers2023
Author(s)
Dresselhaus-Marais Leora E.、Howard Marylesa、Katagiri Kento、Kim Seonghan、Kim Sunam、Kim Sungwon、Kim Hyunjung、Knudsen Erik Bergback、Kuschel Stephan、Lee Hae Ja、Lin Chuanlong、McWilliams R. Stewart、Nagler Bob、Nielsen Martin Meedom、Ozaki Norimasa、Pal Dayeeta、Pablo Pedro Ricardo、
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Journal Title
Scientific Reports
Volume: 13
Issue: 20
Pages: 175731-19
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[Journal Article] Direct LiF imaging diagnostics on refractive X-rat focusing at the EuXFEL High Energy Density instrument2023
Author(s)
. S. Makarov, M. Makita, M. Nakatsutsumi, T. Pikuz, N. Ozaki, T.R. Preston, K. Appel, Z. Konopkova, V. Cerantola, E. Brambrink, J.-P. Schwinkendorf, I. Mohacsi, T. Burian, J. Chalupsky, V. Hajkova, L. Juha, V. Vozda, B. Nagler, U. Zastrau, S. Pikuz
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Journal Title
Journal of Synchrotron Radiation
Volume: 30
Issue: 1
Pages: 1-9
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[Journal Article] Multibeam laser-plasma interaction at the Gekko XII laser facility in conditions relevant for direct-drive inertial confinement fusion2023
Author(s)
Cristoforetti G., Koester P., Atzeni S., Batani D., Fujioka S., Hironaka Y.、Huller S.、Idesaka T.、Katagiri K., Kawasaki K., Kodama R., Mancelli D., Nicolai Ph., Ozaki N.、Schiavi A.、Shigemori K.、Takizawa R., Tamagawa T., Tanaka D., Tentori A., Umeda Y., Yogo A., Gizzi L. A.
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High Power Laser Science and Engineering
Volume: 11
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[Journal Article] Phase transition and melting in zircon by nanosecond shock loading2022
Author(s)
Takagi Sota、Ichiyanagi Kouhei、Kyono Atsushi、Kawai Nobuaki、Nozawa Shunsuke、Ozaki Norimasa、Seto Yusuke、Okuchi Takuo、Nitta Souma、Okada Satoru、Miyanishi Kohei、Sueda Keiichi、Togashi Tadashi、Yabuuchi Toshinori
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Physics and Chemistry of Minerals
Volume: 49
Issue: 5
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[Journal Article] Direct observations of pure electron outflow in magnetic reconnection2022
Author(s)
Sakai K.、Moritaka T.、Morita T.、Tomita K.、Minami T.、Nishimoto T.、Egashira S.、Ota M.、Sakawa Y.、Ozaki N.、Kodama R.、Kojima T.、Takezaki T.、Yamazaki R.、Tanaka S. J.、Aihara K.、Koenig M.、Albertazzi B.、Mabey P.、Woolsey N.、Matsukiyo S.、Takabe H.、Hoshino M.、Kuramitsu Y.
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Journal Title
Scientific Reports
Volume: 12
Issue: 1
Pages: 1-9
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[Journal Article] Development of an experimental platform for the investigation of laser plasma interaction in conditions relevant to shock ignition regime2022
Author(s)
T. Tamagawa, Y. Hironaka, K. Kawasaki, D. Tanaka, T. Idesaka, N. Ozaki, R. Kodama, R. Takizawa, S. Fujioka, A. Yogo, D. Batani, Ph. Nicolai, G. Cristoforetti, P. Koester, L. A. Gizzi, and K. Shigemori
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Journal Title
Review of Scientific Instruments
Volume: 93
Issue: 6
Pages: 063505-063505
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[Journal Article] X-ray diffraction study of phase transformation dynamics of Fe and Fe-Si alloys along the shock Hugoniot using an x-ray free electron laser2022
Author(s)
A. Krygier, M. Harmand, B. Albertazzi, E. E. McBride, K. Miyanishi, D. Antonangeli, Y. Inubushi, R. Kodama, M. Koenig, T. Matsuoka, G. Mogni, F. Pietrucci, A. M. Saitta, T. Togashi, Y. Umeda, T. Vinci, M. Yabashi, T. Yabuuchi, G. Fiquet, and N. Ozaki
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Journal Title
Physical Review B
Volume: 105
Issue: 22
Pages: 1-7
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[Journal Article] High-power laser experiment on developing supercritical shock propagating in homogeneously magnetized plasma of ambient gas origin2022
Author(s)
S. Matsukiyo,R. Yamazaki T. Morita K. Tomita,Y. Kuramitsu ,T. Sano S. J. Tanaka ,T. Takezaki,Y. Horie, S. Sei K. Sugiyama, K. AiharaS. Kambayashi,M. Ota,S. Egashira,T. Izumi,T. Minami,Y. Nakagawa, K. Sakai,M. Iwamoto,N. Ozaki Y. Sakawa他
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Journal Title
Physical Review E
Volume: 106
Issue: 2
Pages: 1-7
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[Journal Article] Diamond formation kinetics in shock-compressed C─H─O samples recorded by small-angle x-ray scattering and x-ray diffraction2022
Author(s)
Z. HE,T. E. COWAN,A.DESCAMPS, M. FRENCH ,E. GALTIER,A. E. GLEASON ,G. D. GLENN ,N.OZAKI,S. PANDOLFI ,C.QU, D. RANJAN,R. REDMER ,C. SCHOENWAELDER, A. K. SCHUSTER, M. G. STEVENSON,K. SUEDA ,T.TOGASHI ,T. VINCI ,K. VOIGT,J. VORBERGER,M. YABASHI,T. YABUUCHI ,L. M. V. ZINTA ,A. RAVASIO AND D. KRAUS
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Journal Title
Science Advances
Volume: 8
Issue: 35
Pages: 1-7
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[Journal Article] Crystallinity in periodic nanostructure surface on Si substrates induced by near- and mid-infrared femtosecond laser irradiation2022
Author(s)
Miyagawa Reina, Kamibayashi Daisuke, Nakamura Hirotaka, Hashida Masaki, Zen Heishun, Somekawa Toshihiro, Matsuoka Takeshi, Ogura Hiroyuki、Sagae Daisuke, Seto Yusuke, Shobu Takahisa, Tominaga Aki, Eryu Osamu, Ozaki Norimasa
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Journal Title
Scientific Reports
Volume: 12
Issue: 1
Pages: 1-8
DOI
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Peer Reviewed / Open Access
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[Presentation] XFEL Radiographic Observation of SiO2 during Shock Compression Process2023
Author(s)
Gooru Masaoka, Tatiana Pikuz, Kento Katagiri, Ryousuke Kodama, Takuo Okuchi, Bruno Albertazzi, Michel Koenig, Kohei Miyanishi, Keiichi Sueda, Toshinori Yabuuchi, Makina Yabashi, Norimasa Ozaki
Organizer
OPTICS & PHOTONICS International Congress 2023
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[Presentation] Damage threshold of LiF crystal irradiated by femtosecond hard XFEL pulse sequence2023
Author(s)
Sergey Makarov, Sergey Grigorye, Tatiana Pikuz, Norimasa Ozaki, Masahiko Ishino, Tetsuya Kawachi, Masaharu Nishikino, Thanh-Hung Dinh, Maxim Zanaveskin, Mikako Makita, Motoaki Nakatsutsumi, Thomas Preston, Karen Appel, Zuzana Konopkova, Valerio Cerantola, Erik Brambrink,
Organizer
OPTICS & PHOTONICS International Congress 2023
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[Presentation] Mechanism of graphite-lonsdaleite phase transition under shock compression2023
Author(s)
Rei Sakaguchi, Hirotaka Nakamura, Yoichiro Hironaka, Kento Katagiri, Keita Nonaka , Kohei Miyanishi ,Keiichi Sueda, Makina Yabashi , Toshinori Yabuuchi , Ryosuke Kodama, Norimasa Ozaki
Organizer
The 11th International workshop on Warm Dense Matter ,WDM2023
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[Presentation] Spectroscopic radiation spectral observations of laser-induced damped shock compression states2023
Author(s)
M. Nakagawa, N. Ozaki, K. Yamagishi, G. Kamimura, R. Iwamoto1, K. Nonaka, K. Katagiri, Y. Hironaka, T. Sano, R. Kodama
Organizer
The 11th International workshop on Warm Dense Matter ,WDM2023
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[Presentation] Prediction of laser-irradiation parameters in high-power laser surface processing using deep convolutional neural network2023
Author(s)
K. Rani , N. Ozaki, Y. Hironaka, K. Hashimoto, K. Mukai , K. Miyake , R. Kodama, H. Nakamura, S. Takai , and H. Nagatomo
Organizer
The 11th International workshop on Warm Dense Matter ,WDM2023
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[Presentation] Research on freezing of materials under high pressure by Bessel-beam driven microexplosions in transparent materials2023
Author(s)
H. Nakamura, Y. Ota, H. Oguraa, D. Kamibayashi G. Kamimura, D. Murayama, L. Rapp, E. Gamaly A. Rode, T. Matsuoka, D. Sagae, Y. Seto T. Shobu, T. Somekawa, A. Tominaga,
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The 11th International workshop on Warm Dense Matter ,WDM2023
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[Presentation] 結晶中を超音速伝搬する転位のXFELラジオグラフ観察2023
Author(s)
尾崎典雅,片桐健登,Tatiana Pikuz,Lichao Fang,Bruno Albertazzi,江頭俊輔,犬伏雄一,上村拳生,兒玉了祐,Michel Koenig,Bernard Kozioziemski,政岡豪流,宮西宏併,中村浩隆,太田雅人,Gabriel Rigon,坂和洋一,佐野孝好,Frank Schoofs,Zoe J. Smith,末田敬一,冨樫格
Organizer
高速度イメージングとフォトニクスに関する総合シンポジウム2023 (JCHIS 2023)
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[Presentation] Calcite at extreme conditons with implications for hypervelocity planetary impacts2022
Author(s)
Yuhei Umeda, Keiya Fukui, Toshimori Sekine, Marco Guarguaglin, Alessandra Benuzzi-Mounaix, Nobuki Kamimura, Kento Katagiri, Ryosuke Kodama, Takeshi Matsuoka, Kohei Miyanishi, Alessandra Ravasio, Takayoshi Sano, Norimasa Ozaki
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International Conference on High energy density sciences 2022
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[Presentation] Laser Shock Experiments for Liquid Hydrogen Sulfide Pre-compressed in Diamond Anvil Cell2022
Author(s)
Souma Nitta, Mari Einaga, Katsuya Shimiz Misaki Sasaki, Seiji Matsumoto, Takayoshi Sano, Toshihiro Somekawa, Takuo Okuchi, Kento Katagiri, Ryota Iwamoto, Ryosuke Kodama, Norimasa Ozaki
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International Conference on High energy density sciences 2022
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[Presentation] Development of experimental platform for laser-plasma interactions in shock ignition scheme2022
Author(s)
Tomoyuki Idesaka, Takumi Tamagawa, Yoichiro Hironaka, Koki Kawasaki, Daisuke Tanaka, Norimasa Ozaki, Ryousuke Kodama, Ryunosuke Takizawa, Shinsuke Fujioka, Akifumi Yogo, Dimitri Batani, Gabriele Cristoforetti, Keisuke Shigemori
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International Conference on High energy density sciences 2022
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[Presentation] Research on freezing of materials under high pressure by Bessel-beam driven micro-explosions in transparent materials2022
Author(s)
Hirotaka Nakamura, Hiroyuki Ogura, Daisuke Kamibayashi, Genki Kamimur, Daisuke Murayama, Ludovic Rapp, Eugene Gamaly, Andrei Rode, Takeshi Matsuoka, Daisuke Sagae, Yusuke Seto, Takahisa Shobu, Aki Tominaga, Toshihiro Somekawa, Tatiana Pikuz, Ryosuke Kodama, Norimasa Ozaki
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International Conference on High energy density sciences 2022
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[Presentation] Crystallinity evaluation in periodic structures induced by femtosecond laser pulses2022
Author(s)
Reina Miyagawa, Daisuke Kamibayashi, Hirotaka Nakamura, Masaki Hashida, Heishun Zen, Takeshi Matsuoka, Hiroyuki Ogura, Daisuke Sagae, Yusuke Seto, Takahisa Shobu, Ai Tominaga, Osamu Eryu, Norimasa Ozaki
Organizer
International Conference on High energy density sciences 2022
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Int'l Joint Research / Invited
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[Presentation] In-situ X-ray diffraction of shock-released tantalum2022
Author(s)
K.Katagiri, N. Ozaki, S.Ohmura, B.Albertazzi, Y.Hironaka, Y. Inubushi, K. Ishida, M.Koenig, K.Miyanishi, H. Nakamura, M. Nishikino, T.Okuchi, T.Sato, Y. Seto, K.Shigemori, K. Sueda, Y.Tange, T.Togashi, Y.Umeda, M.Yabashi, T. Yabuuchi, R.Kodama
Organizer
International Conference on High energy density sciences 2022
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[Presentation] Ultrahigh Pressure Creation by Hot Electron-Assisted Laser Ablation2022
Author(s)
K.Kawasaki, Y. Hironaka, D.anaka, T.Idesaka, K.Yamanoi, R. Takizawa, S. Fujioka, A. Yogo, H.Nagatomo, Ya. Sentoku, Y.Arikawa, N. Ozaki, R. Kodama, K.Katagir, K. Mima, Y.Mori, T. Jozaki, H. Yamada, D.Batani, G. Cristoforetti, K.Shigemori
Organizer
International Conference on High energy density sciences 2022
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[Presentation] High-density-plasma formation with multiple spherical shock waves driven by high-power laser2022
Author(s)
Shinsuke Fujioka, Ryunosuke Takizawa, Tamaki Maegawa, Kento Katagiri, Hiroki Morita, Shuwang Guo, Jiyang Dun, Yoichiro Hironaka, Norimasa Ozaki, Keisuke Shigemori, Yasunobu Arikawa, Yuji Nagasawa, Tomoyuki Johzaki, Hideo Nagatomo, Yasuhiko Sentoku, Ryosuke Kodama
Organizer
International Conference on High energy density sciences 2022
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[Presentation] Phase transition and melting in zircon by nanosecond shock loading2022
Author(s)
Sota Takagi, Kouhei Ichiyanagi, Atsushi Kyono, Nobuaki Kawai, Shunsuke Nozawa, Norimasa Ozaki, Yusuke Seto, Takuo Okuchi, Souma Nitta, Satoru Okada, Kohei Miyanishi, Keiichi Sueda, Tadashi Togashi, Toshinori Yabuuchi
Organizer
International Conference on High energy density sciences 2022
Related Report
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[Presentation] 衝撃圧縮過程におけるクォーツのXFELラジオグラフ観察2022
Author(s)
政岡豪流,PIKUZ Tatiana, 片桐健登 , 兒玉了祐 , 奥地拓生 , ALBERTAZZI Bruno, KOENIG Michel, 宮西宏併 , 末田敬一 , 籔内俊毅 , 矢橋牧名 , 尾崎典雅
Organizer
第63回高圧討論会
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[Book] Ultrafast Laser Nanostructuring2023
Author(s)
Ludovic Rapp,,Ryosuke Kodama,Yusuke Seto,Takahisa Shobu,Aki Tominaga,Makina Yabashi Norimasa Ozaki
Total Pages
1245
Publisher
Springer International Publishing
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