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Realization of reversible plasticity in metals by mechanical control of self-organized dislocation structure

Research Project

Project/Area Number 22K18754
Research Category

Grant-in-Aid for Challenging Research (Exploratory)

Allocation TypeMulti-year Fund
Review Section Medium-sized Section 18:Mechanics of materials, production engineering, design engineering, and related fields
Research InstitutionKyoto University

Principal Investigator

Sumigawa Takashi  京都大学, エネルギー科学研究科, 教授 (80403989)

Project Period (FY) 2022-06-30 – 2024-03-31
Project Status Completed (Fiscal Year 2023)
Budget Amount *help
¥6,370,000 (Direct Cost: ¥4,900,000、Indirect Cost: ¥1,470,000)
Fiscal Year 2023: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2022: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords自己組織化 / 転位構造 / 金属 / 可逆塑性 / 繰り返し負荷
Outline of Research at the Start

半導体電子デバイスの重要性が世界的に急拡大している一方、デバイスに生じる熱応力に起因して、内部のナノ~マイクロサイズの金属素子が疲労破壊することが問題となっている。この問題の本質的な解決のためには、従来概念を超越した「可逆塑性変形を示す“しなやか金属”」による素子を実現する必要がある。本研究では、ナノ・マイクロ金属に形成される自己組織化転位構造の力学的支配因子を明らかにし、可逆塑性変形能を有する「しなやか金属」実現のための力学設計基盤の構築を行う。

Outline of Final Research Achievements

The purpose of this study was to create a material that undergoes reversible plastic deformation by focusing on the peculiar self-organized dislocation structure formed inside micro-sized single crystal metals under cyclic loading. Nickel single crystals with a square cross section of two micrometers on a side were subjected to tension-compression cyclic loading at stress amplitudes lower than the fatigue crack initiation limit of bulk Ni. The specimen oriented to a particular crystallographic orientation showed elastic deformation in the early stages, but exhibited large plastic strain from the middle of the testing. Internal observation of the specimen after the experiment revealed that a structure similar to the ladder-like dislocation one found in the bulk was formed throughout the gauge section of the specimen, and analysis of reaction-diffusion system revealed that surface effects produced the peculiar dislocation structure.

Academic Significance and Societal Importance of the Research Achievements

本研究では、ミクロンサイズの材料では、繰り返し負荷によって形成される転位の自己組織化転位構造に対して表面の影響が材料全体に及ぼされることを実験および解析によって明らかにし、結晶方位や材料寸法を調節することで目的とする転位構造を材料全体に発現できる可能性を示した。本成果は、転位の自己組織化構造の制御によって材料に特有の機械特性を生み出すという新しい学術分野を開拓するものであることに加え、将来的にはこれを利用した高機能構造物の創出の可能性も見込まれることから、学術界のみならず産業界や社会へ大きく貢献するものである。

Report

(3 results)
  • 2023 Annual Research Report   Final Research Report ( PDF )
  • 2022 Research-status Report
  • Research Products

    (35 results)

All 2024 2023 2022 Other

All Int'l Joint Research (2 results) Journal Article (9 results) (of which Peer Reviewed: 9 results,  Open Access: 5 results) Presentation (21 results) (of which Int'l Joint Research: 5 results,  Invited: 5 results) Book (1 results) Remarks (2 results)

  • [Int'l Joint Research] 浙江大学(中国)

    • Related Report
      2022 Research-status Report
  • [Int'l Joint Research] ノルウェー科学技術大学(ノルウェー)

    • Related Report
      2022 Research-status Report
  • [Journal Article] Characteristic fatigue damage near the Σ3(111) coherent twin boundary in micron-sized copper specimen2024

    • Author(s)
      Kim Byungwoon、Yasui Chihiro、Abe Masataka、Shima Hiroyuki、Umeno Yoshitaka、Sumigawa Takashi
    • Journal Title

      Materials Science and Engineering: A

      Volume: 899 Pages: 146470-146470

    • DOI

      10.1016/j.msea.2024.146470

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Dislocation Random Walk under Cyclic Deformation2024

    • Author(s)
      Atsushi Kubo, Emi Kawai, Takashi Sumigawa, Hiroyuki Shima, Yoshitaka Umeno
    • Journal Title

      Physical Review E

      Volume: accepted

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Spot?Ladder Selection of Dislocation Patterns in Metal Fatigue2023

    • Author(s)
      Shima Hiroyuki、Umeno Yoshitaka、Sumigawa Takashi
    • Journal Title

      Symmetry

      Volume: 15 Issue: 5 Pages: 1028-1028

    • DOI

      10.3390/sym15051028

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Experimental investigation on magnetomechanical effect of carbon steel under high-cycle loading2023

    • Author(s)
      安部 正高, 澄川 貴志, 三戸 慎也, 宮澤 和紀
    • Journal Title

      Transactions of the JSME (in Japanese)

      Volume: 89 Issue: 923 Pages: 22-00319-22-00319

    • DOI

      10.1299/transjsme.22-00319

    • ISSN
      2187-9761
    • Related Report
      2023 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Defect formation mechanisms in metal nanowire under cyclic loading: a molecular dynamics study2023

    • Author(s)
      Kubo Atsushi、Kawai Emi、Sumigawa Takashi、Shima Hiroyuki、Umeno Yoshitaka
    • Journal Title

      Modelling and Simulation in Materials Science and Engineering

      Volume: 31 Issue: 6 Pages: 065020-065020

    • DOI

      10.1088/1361-651x/acea3b

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Surface outflow effect on dislocation structures in micrometer-sized metals2023

    • Author(s)
      Tobise Akihiro、Shima Hiroyuki、Akiba Yuri、Umeno Yoshitaka、Kawai Emi、Kubo Atsushi、Abe Masataka、Sumigawa Takashi
    • Journal Title

      Extreme Mechanics Letters

      Volume: 65 Pages: 102094-102094

    • DOI

      10.1016/j.eml.2023.102094

    • Related Report
      2023 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Inductive Determination of Rate-Reaction Equation Parameters for Dislocation Structure Formation Using Artificial Neural Network2023

    • Author(s)
      Umeno Yoshitaka、Kawai Emi、Kubo Atsushi、Shima Hiroyuki、Sumigawa Takashi
    • Journal Title

      Materials

      Volume: 16 Issue: 5 Pages: 2108-2108

    • DOI

      10.3390/ma16052108

    • Related Report
      2022 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Analytic formulation of elastic field around edge dislocation adjacent to slanted free surface2022

    • Author(s)
      Shima Hiroyuki、Umeno Yoshitaka、Sumigawa Takashi
    • Journal Title

      Royal Society Open Science

      Volume: 9 Issue: 6 Pages: 220151-220151

    • DOI

      10.1098/rsos.220151

    • Related Report
      2022 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Nonsingular Stress Distribution of Edge Dislocations near Zero-Traction Boundary2022

    • Author(s)
      Shima Hiroyuki、Sumigawa Takashi、Umeno Yoshitaka
    • Journal Title

      Materials

      Volume: 15 Issue: 14 Pages: 4929-4929

    • DOI

      10.3390/ma15144929

    • Related Report
      2022 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] ナノ~マイクロ材料に関するその場観察力学実験2024

    • Author(s)
      澄川貴志
    • Organizer
      電子情報通信学会 システムナノ技術に関する特別研究専門委員会主催 第5期 第3回研究会
    • Related Report
      2023 Annual Research Report
    • Invited
  • [Presentation] 転位を起点とするナノ SrTiO3の破壊とその力学基準2023

    • Author(s)
      澄川貴志
    • Organizer
      日本セラミックス協会 第36回秋季シンポジウム
    • Related Report
      2023 Annual Research Report
    • Invited
  • [Presentation] Elucidation of formation mechanism of fatigue dislocation structures in micro-sized Ni single crystal under tension-compression cyclic load2023

    • Author(s)
      Kota SUGISAKA
    • Organizer
      The Advanced Technology in Experimental Mechanics and International DIC Society Joint Conference 2023
    • Related Report
      2023 Annual Research Report
    • Int'l Joint Research
  • [Presentation] ナノ金属の引張圧縮疲労試験手法の開発2023

    • Author(s)
      池田大輝
    • Organizer
      日本材料学会第9回材料WEEK
    • Related Report
      2023 Annual Research Report
  • [Presentation] Σ3(111)境界を有するマイクロ銅双結晶試験片の引張圧縮疲労損傷2023

    • Author(s)
      Kim byungwoon
    • Organizer
      日本材料学会第9回材料WEEK
    • Related Report
      2023 Annual Research Report
  • [Presentation] 引張圧縮繰り返し負荷を受けるマイクロNi単結晶試験片の疲労転位組織形成過程の観察2023

    • Author(s)
      杉坂 浩太
    • Organizer
      日本材料学会第9回材料WEEK
    • Related Report
      2023 Annual Research Report
  • [Presentation] 非圧電性材料におけるナノ電界勾配に起因した Converse Flexoelectricity の形状効果2023

    • Author(s)
      池本 翔太郎
    • Organizer
      日本機械学会 M&M 2023 材料力学カンファレンス
    • Related Report
      2023 Annual Research Report
  • [Presentation] 異材界面を有するマイクロ金属単結晶の疲労2023

    • Author(s)
      Kim byungwoon
    • Organizer
      日本機械学会 M&M 2023 材料力学カンファレンス
    • Related Report
      2023 Annual Research Report
  • [Presentation] 力学系理論による疲労転位構造の安定性解析2023

    • Author(s)
      島 弘幸
    • Organizer
      日本機械学会 M&M 2023 材料力学カンファレンス
    • Related Report
      2023 Annual Research Report
  • [Presentation] 引張圧縮負荷を受けるマイクロ Ni 単結晶中の疲労転位構造形成過程の観察2023

    • Author(s)
      杉坂 浩太
    • Organizer
      日本機械学会 M&M 2023 材料力学カンファレンス
    • Related Report
      2023 Annual Research Report
  • [Presentation] 日本機械学会 M&M 2023 材料力学カンファレンス2023

    • Author(s)
      向井 健将
    • Organizer
      集中荷重に対するひずみ分散機能を有するメカニカルメタマテリアルの開発
    • Related Report
      2023 Annual Research Report
  • [Presentation] Observation of fatigue dislocation structure in micro-sized Ni single crystal specimen2023

    • Author(s)
      Takashi Sumigawa
    • Organizer
      2023 International Joint Symposium on Convergence Technology of Mechanical Engineering
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] In Situ Observation of Fracture Dominated by a Single Dislocation and its Governing Mechanics2022

    • Author(s)
      Takashi Sumigawa
    • Organizer
      MS&T22 Technical meeting and Exhibitio
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Experimental Investigation of the Fatigue Behavior of Three-dimensionally Small Micro-sized Metals2022

    • Author(s)
      Takashi Sumigawa
    • Organizer
      MATERIALS STRUCTURE & MICROMECHANICS OF FRACTURE (MSMF10)
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 曲げ負荷を受けるBaTiO3ナノ単結晶のドメイン構造変化の観察2022

    • Author(s)
      高木敏行
    • Organizer
      日本材料学会第8回材料WEEK
    • Related Report
      2022 Research-status Report
  • [Presentation] 単一すべり方位を有するナノNi単結晶のTEM内引張圧縮負荷挙動観察2022

    • Author(s)
      石坂大和
    • Organizer
      日本材料学会第8回材料WEEK
    • Related Report
      2022 Research-status Report
  • [Presentation] 引張圧縮負荷を受けるマイクロNi単結晶の疲労転位組織形成過程観察2022

    • Author(s)
      穴田悠樹
    • Organizer
      日本材料学会第8回材料WEEK
    • Related Report
      2022 Research-status Report
  • [Presentation] VO2単結晶ナノ薄膜のモット転移に関する面内単軸ひずみ感受性評価2022

    • Author(s)
      角田純平
    • Organizer
      日本機械学会 M&M 2022 材料力学カンファレンス
    • Related Report
      2022 Research-status Report
  • [Presentation] マイクロ金属の疲労転位組織形成パターンに関する数値シミュレーション2022

    • Author(s)
      飛世昂大
    • Organizer
      日本機械学会 M&M 2022 材料力学カンファレンス
    • Related Report
      2022 Research-status Report
  • [Presentation] 疲労した金属の転位組織形成メカニズム解明への数理的アプローチ2022

    • Author(s)
      飛世昂大
    • Organizer
      日本材料学会第7回マルチスケール材料力学シンポジウム 2022年5月
    • Related Report
      2022 Research-status Report
  • [Presentation] Characteristic Fatigue of Micro-Sized Single Crystal Nickel2022

    • Author(s)
      Takashi Sumigawa
    • Organizer
      The 6th International Conference on Materials and Reliability
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research
  • [Book] 金属疲労の基礎とメカニクス―結晶学と力学から読み解く金属の疲労2024

    • Author(s)
      兼子 佳久,田中 啓介,高橋 可昌,澄川 貴志,平方 寛之,梅野 宜崇
    • Total Pages
      248
    • Publisher
      内田老鶴圃
    • ISBN
      9784753655069
    • Related Report
      2023 Annual Research Report
  • [Remarks] 京都大学大学院 エネルギー科学研究科 エネルギー材料設計研究室ホームページ

    • URL

      https://www.force.energy.kyoto-u.ac.jp/

    • Related Report
      2023 Annual Research Report
  • [Remarks] 京都大学大学院 エネルギー科学研究科 エネルギー変換科学専攻 エネルギー材料設計研究室

    • URL

      http://www.force.energy.kyoto-u.ac.jp/

    • Related Report
      2022 Research-status Report

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Published: 2022-07-05   Modified: 2025-01-30  

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