• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

Investigation on Fracture Mechanisms and Size Effects of Nano-Films Using Nano-Mechanical Testing System based upon in-situ Observations and Analyses

Research Project

Project/Area Number 23246026
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionOsaka University

Principal Investigator

MINOSHIMA Kohji  大阪大学, 工学(系)研究科(研究院), 教授 (50174107)

Co-Investigator(Kenkyū-buntansha) HIRAKATA Hiroyuki  大阪大学, 大学院工学研究科, 准教授 (40362454)
YONEZU Akio  大阪大学, 大学院工学研究科, 助教 (40398566)
Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥51,090,000 (Direct Cost: ¥39,300,000、Indirect Cost: ¥11,790,000)
Fiscal Year 2013: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2012: ¥6,240,000 (Direct Cost: ¥4,800,000、Indirect Cost: ¥1,440,000)
Fiscal Year 2011: ¥40,950,000 (Direct Cost: ¥31,500,000、Indirect Cost: ¥9,450,000)
Keywordsマイクロ材料力学 / 材料強度学 / 薄膜 / 破壊 / 疲労 / クリープ / マイクロ材料強度学 / 強度
Research Abstract

We developed an experimental setup for clarifying the mechanics and mechanisms of fracture in freestanding submicron-thick metallic films. This system can conduct in situ FESEM observation of deformation/fracture and EBSD crystallographic analysis on the local region at stress concentration sites such as crack tips under controlled mechanical conditions. Systematic experiments clarified the thickness effect on fracture toughness in copper nano-films where the fracture toughness decreases with a decrease in thickness, the characteristic fatigue crack growth mechanism of copper films where a fatigue crack propagates through intrusions/extrusions formed ahead of the crack tip, the presence of fatigue crack closure and the impact on the fatigue crack propagation property, and the effect of thickness on creep properties of aluminum nano-films.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (46 results)

All 2014 2013 2012 2011 Other

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (37 results) Remarks (4 results)

  • [Journal Article] Mechanics of fatigue crack propagation in submicron-thick freestanding copper films2014

    • Author(s)
      Hiroyuki Hirakata, Toshiyuki Kondo, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Advanced Materials Research

      Volume: Vols.891-892 Pages: 1681-1687

    • DOI

      10.4028/www.scientific.net/amr.891-892.1681

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effects of stress ratio on fatigue crack propagation properties of submicron-thick freestanding copper films2013

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Acta Materialia

      Volume: Vol.61 Issue: 16 Pages: 6310-6327

    • DOI

      10.1016/j.actamat.2013.07.017

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] The effect of thickness on steady state creep properties of freestanding aluminum nano-films2012

    • Author(s)
      Hiroyuki Hirakata, Naomichi Fukuhara, Shoichi Ajioka, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Acta Materialia

      Volume: Vol.60 Issue: 11 Pages: 4438-4447

    • DOI

      10.1016/j.actamat.2012.04.036

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Development of Fatigue Crack Propagation Technique for Freestanding Nano-Films2012

    • Author(s)
      近藤 俊之, 今岡 貴裕, 平方 寛之, 米津 明生, 﨑原 雅之, 箕島 弘二
    • Journal Title

      TRANSACTIONS OF THE JAPAN SOCIETY OF MECHANICAL ENGINEERS Series A

      Volume: 78 Issue: 790 Pages: 808-816

    • DOI

      10.1299/kikaia.78.808

    • NAID

      130002050309

    • ISSN
      0387-5008, 1884-8338
    • Related Report
      2013 Final Research Report 2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Size effect on fracture toughness of freestanding copper nano-films2011

    • Author(s)
      Hiroyuki Hirakata, Osamu Nishijima, Naomichi Fukuhara, Toshiyuki Kondo, Akio Yonezu, Kohji Minoshima
    • Journal Title

      Materials Science and Engineering A

      Volume: Vol.528 Issue: 28 Pages: 8120-8127

    • DOI

      10.1016/j.msea.2011.07.071

    • Related Report
      2013 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] Mechanics of fatigue crack propagation in submicron-thick freestanding copper films2014

    • Author(s)
      Hiroyuki Hirakata, Toshiyuki Kondo, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      11th International Fatigue Congress (Fatigue 2014)
    • Place of Presentation
      Melbourne Australia
    • Related Report
      2013 Final Research Report
  • [Presentation] Mechanics of fatigue crack propagation in submicron-thick freestanding copper films2014

    • Author(s)
      Hiroyuki Hirakata, Toshiyuki Kondo, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      11th International Fatigue Congress (Fatigue 2014), Poster 36230.
    • Place of Presentation
      Melbourne Cricket Ground, Melbourne, Australia
    • Related Report
      2013 Annual Research Report
  • [Presentation] ナノメートル厚自立銅薄膜の破壊じん性評価2014

    • Author(s)
      河尻隆宏, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第89期定時総会講演会講演論文集, No.144-1, p.12-1.
    • Place of Presentation
      大阪府立大学,堺市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜の破壊じん性試験のその場FESEM観察2014

    • Author(s)
      竹田裕紀, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第89期定時総会講演会講演論文集, No.144-1, p.12-2.
    • Place of Presentation
      大阪府立大学,堺市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜の疲労き裂進展特性に及ぼすき裂閉口の影響2014

    • Author(s)
      近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第89期定時総会講演会講演論文集, No.144-1, p.12-16.
    • Place of Presentation
      大阪府立大学,堺市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 結晶方位解析による自立銅ナノ薄膜の疲労き裂発生強度の力学的評価2014

    • Author(s)
      畢暁晨, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第89期定時総会講演会講演論文集, No.144-1, p.12-17.
    • Place of Presentation
      大阪府立大学,堺市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 金属単結晶自立ナノ薄膜の破壊じん性2014

    • Author(s)
      吉田卓哉, 松田友維名, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第63期学術講演会
    • Place of Presentation
      福岡大学,福岡市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 銅ナノ薄膜の疲労き裂開閉口挙動のその場観察2014

    • Author(s)
      近藤俊之, 吉川直樹, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第63期学術講演会
    • Place of Presentation
      福岡大学,福岡市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜の疲労き裂進展過程のその場FESEM 観察2013

    • Author(s)
      近藤俊之, 平方寛之, 﨑原雅之, 箕島弘二
    • Organizer
      日本機械学会M&M2013材料力学カンファレンス
    • Place of Presentation
      岐阜大学
    • Related Report
      2013 Final Research Report
  • [Presentation] ナノ観察とEBSD 援用応力解析による自立銅ナノ薄膜の疲労損傷発生機構の解明2013

    • Author(s)
      近藤俊之, 畢暁晨, 田村拓, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第62期学術講演会
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Final Research Report
  • [Presentation] ナノ観察とEBSD援用応力解析による自立銅ナノ薄膜の疲労損傷発生機構の解明2013

    • Author(s)
      近藤俊之, 畢暁晨, 田村拓, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第62期学術講演会講演論文集, 講演番号505.
    • Place of Presentation
      東京工業大学,東京都
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜のき裂進展機構と膜厚依存2013

    • Author(s)
      竹田裕紀, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会M&M2013材料力学カンファレンス講演論文集, OS1201.
    • Place of Presentation
      岐阜大学,岐阜市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜の疲労き裂進展過程のその場FESEM観察2013

    • Author(s)
      近藤俊之, 平方寛之, 﨑原雅之, 箕島弘二
    • Organizer
      日本機械学会M&M2013材料力学カンファレンス講演論文集, OS1202.
    • Place of Presentation
      岐阜大学,岐阜市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立ナノ薄膜の疲労損傷形成過程のナノ観察2013

    • Author(s)
      畢暁晨, 田村拓, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会M&M2013材料力学カンファレンス講演論文集, PS24.
    • Place of Presentation
      岐阜大学,岐阜市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜のき裂進展機構と膜厚依存2013

    • Author(s)
      竹田裕紀, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第8回若手シンポジウム講演資料集, pp.35-36.
    • Place of Presentation
      石切温泉ホテルセイリュウ,東大阪市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立ナノ薄膜の疲労損傷形成過程のナノ観察2013

    • Author(s)
      畢暁晨, 田村拓, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第8回若手シンポジウム講演資料集, pp.39-40.
    • Place of Presentation
      石切温泉ホテルセイリュウ,東大阪市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展特性に及ぼす膜厚効果2012

    • Author(s)
      今岡貴裕, 近藤俊之, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本材料学会第31回疲労シンポジウム
    • Place of Presentation
      慶応義塾大学
    • Year and Date
      2012-11-21
    • Related Report
      2013 Final Research Report
  • [Presentation] ナノメートル厚金属薄膜の破壊じん性に及ぼす膜厚効果2012

    • Author(s)
      平方寛之, 近藤俊之, 竹田裕紀, 河尻隆宏, 米津明生, 箕島弘二
    • Organizer
      日本機械学会M&M2012 材料力学カンファレンス
    • Place of Presentation
      愛媛大学
    • Year and Date
      2012-09-22
    • Related Report
      2013 Final Research Report
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展の下限界特性2012

    • Author(s)
      近藤俊之, 今岡貴裕, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本材料学会第61期学術講演会
    • Place of Presentation
      岡山大学
    • Year and Date
      2012-05-27
    • Related Report
      2013 Final Research Report
  • [Presentation] Size effects on creep property in aluminum nano-films2012

    • Author(s)
      Hiroyuki Hirakata, Naomichi Fukuhara, Akio Yonezu, Kohji Minoshima
    • Organizer
      Asia Pacific Conference on Fracture and Strength - Mechanics and Materials (APCFS-MM 2012)
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2012-05-15
    • Related Report
      2013 Final Research Report
  • [Presentation] Effects of stress ratio on fatigue crack propagation in freestanding Cu nano-films2012

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      Asia Pacific Conference on Fracture and Strength - Mechanics and Materials (APCFS-MM 2012)
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2012-05-15
    • Related Report
      2013 Final Research Report
  • [Presentation] 自立Cuナノ薄膜の疲労き裂進展に及ぼす応力比の影響2012

    • Author(s)
      近藤俊之, 今岡高裕, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本機械学会関西支部第87期定時総会講演会
    • Place of Presentation
      関西大学
    • Year and Date
      2012-03-17
    • Related Report
      2011 Annual Research Report
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展における膜厚効果2011

    • Author(s)
      平方寛之, 近藤俊之, 西嶋修, 米津明生, 箕島弘二
    • Organizer
      日本機械学会第3回マイクロ・ナノ工学シンポジウム
    • Place of Presentation
      タワーホール船堀(東京)
    • Year and Date
      2011-09-27
    • Related Report
      2013 Final Research Report
  • [Presentation] 自立金属ナノ薄膜のき裂進展におけるサイズ効果2011

    • Author(s)
      平方寛之, 近藤俊之, 西嶋修, 米津明生, 箕島弘二
    • Organizer
      日本機械学会第3回マイクロ・ナノ工学シンポジウム
    • Place of Presentation
      タワーホール船堀(東京)
    • Year and Date
      2011-09-27
    • Related Report
      2011 Annual Research Report
  • [Presentation] Fatigue crack propagation in freestanding copper nano-films2011

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      神戸国際会議場
    • Year and Date
      2011-09-20
    • Related Report
      2013 Final Research Report 2011 Annual Research Report
  • [Presentation] 自立Cuナノ薄膜の疲労き裂進展における膜厚効果2011

    • Author(s)
      近藤俊之, 今岡高裕, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本機械学会M&M材料力学カンファレンス
    • Place of Presentation
      九州工業大学
    • Year and Date
      2011-07-18
    • Related Report
      2011 Annual Research Report
  • [Presentation] 自立Cuナノ薄膜における疲労き裂進展特性2011

    • Author(s)
      近藤俊之, 今岡高裕, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本材料学会第60期学術講演会
    • Place of Presentation
      大阪大学
    • Year and Date
      2011-05-26
    • Related Report
      2011 Annual Research Report
  • [Presentation] デジタル画像相関法によるナノ薄膜の高ひずみ塑性特性評価法の開発

    • Author(s)
      伊東龍一, 近藤俊之, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪工業大学,大阪市
    • Related Report
      2012 Annual Research Report
  • [Presentation] ナノ観察と結晶方位解析による自立銅ナノ薄膜の疲労発生機構の解明

    • Author(s)
      近藤俊之, 畢暁晨, 平方寛之, 箕島弘二
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪工業大学,大阪市
    • Related Report
      2012 Annual Research Report
  • [Presentation] 自立銅ナノ薄膜の疲労き裂進展特性の膜厚依存と進展機構の解明

    • Author(s)
      今岡貴裕, 近藤俊之, 平方寛之, 﨑原雅之, 箕島弘二
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪工業大学,大阪市
    • Related Report
      2012 Annual Research Report
  • [Presentation] 自立金属ナノ薄膜における疲労き裂進展

    • Author(s)
      近藤俊之, 今岡貴裕, 平方寛之, 﨑原雅之, 箕島弘二
    • Organizer
      日本材料学会関西支部 第7回若手シンポジウム
    • Place of Presentation
      滋賀県大津市
    • Related Report
      2012 Annual Research Report
  • [Presentation] 自立Cuナノ薄膜の疲労き裂進展特性に及ぼす膜厚効果

    • Author(s)
      今岡貴裕, 近藤俊之, 平方寛之, 米津明生, 﨑原雅之, 箕島弘二
    • Organizer
      日本材料学会 第31回疲労シンポジウム
    • Place of Presentation
      慶応義塾大学,横浜市
    • Related Report
      2012 Annual Research Report
  • [Presentation] ナノメートル厚金属薄膜の破壊じん性に及ぼす膜厚効果

    • Author(s)
      平方寛之, 近藤俊之, 竹田裕紀, 河尻隆宏, 米津明生, 箕島弘二
    • Organizer
      日本機械学会M&M2012材料力学カンファレンス
    • Place of Presentation
      愛媛大学,松山市
    • Related Report
      2012 Annual Research Report
  • [Presentation] 自立Cuナノ薄膜の疲労き裂先端の疲労損傷観察

    • Author(s)
      近藤俊之, 今岡貴裕, 平方寛之, 米津明生, 﨑原雅之, 箕島弘二
    • Organizer
      日本機械学会M&M2012材料力学カンファレンス
    • Place of Presentation
      愛媛大学,松山市
    • Related Report
      2012 Annual Research Report
  • [Presentation] デジタル画像相関法を用いたナノ薄膜の高ひずみ領域における塑性特性評価

    • Author(s)
      伊東龍一, 近藤俊之, 平方寛之, 米津明生, 箕島弘二
    • Organizer
      日本機械学会M&M2012材料力学カンファレンス
    • Place of Presentation
      愛媛大学,松山市
    • Related Report
      2012 Annual Research Report
  • [Presentation] 自立Cuナノ薄膜の疲労き裂進展の下限界特性

    • Author(s)
      近藤俊之, 今岡貴裕, 平方寛之, 米津明生, 﨑原雅之, 箕島弘二
    • Organizer
      日本材料学会第61期学術講演会
    • Place of Presentation
      岡山大学,岡山市
    • Related Report
      2012 Annual Research Report
  • [Presentation] Effects of Stress Ratio on Fatigue Crack Propagation in Freestanding Cu Nano-films

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Akio Yonezu, Masayuki Sakihara and Kohji Minoshima
    • Organizer
      Asia Pacific Conference on Fracture and Strength - Mechanics and Materials (APCFS-MM 2012)
    • Place of Presentation
      Busan, Korea
    • Related Report
      2012 Annual Research Report
  • [Remarks] ホームページ

    • URL

      http://www-micro.mech.eng.osaka-u.ac.jp/home.html

    • Related Report
      2013 Final Research Report
  • [Remarks] 大阪大学大学院工学研究科機械工学専攻

    • URL

      http://www-micro.mech.eng.osaka-u.ac.jp/home.html

    • Related Report
      2013 Annual Research Report
  • [Remarks] 大阪大学大学院工学研究科機械工学専攻

    • URL

      http://www-micro.mech.eng.osaka-u.ac.jp/home.html

    • Related Report
      2012 Annual Research Report
  • [Remarks]

    • URL

      http://www-micro.mech.eng.osaka-u.ac.jp/home.html

    • Related Report
      2011 Annual Research Report

URL: 

Published: 2011-04-06   Modified: 2019-07-29  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi