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Development of X-ray diffractomator to realize in-situ observation of crystal growth

Research Project

Project/Area Number 23360009
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Applied materials science/Crystal engineering
Research InstitutionNagoya University

Principal Investigator

TABUCHI MASAO  名古屋大学, シンクロトロン光研究センター, 特任教授 (90222124)

Co-Investigator(Renkei-kenkyūsha) TAKEDA Yoshikazu  名古屋大学, 工学研究科, 名誉教授 (20111932)
UJIHARA Thoru  名古屋大学, 工学研究科, 教授 (60312641)
OKUDA Hiroshi  京都大学, 工学研究科, 准教授 (50214060)
Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥20,410,000 (Direct Cost: ¥15,700,000、Indirect Cost: ¥4,710,000)
Fiscal Year 2013: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Fiscal Year 2012: ¥8,190,000 (Direct Cost: ¥6,300,000、Indirect Cost: ¥1,890,000)
Fiscal Year 2011: ¥9,490,000 (Direct Cost: ¥7,300,000、Indirect Cost: ¥2,190,000)
KeywordsX線回折測定 / その場観察 / 結晶成長 / 分光集光結晶 / 回転機構排除 / X線集光光学系 / X線回折 / X線散乱 / その場測定 / X線反射率測定 / ヨハンソン分光結晶 / 稼動部のない測定
Research Abstract

Recently, surface and interface structures of advanced semiconductor devices should be controlled in an atomic scale, and the technique to investigate the real structures of the surfaces and interfaces is getting much important. In order to realize in-situ observation of the semiconductor device structures in conventional crystal growth system via X-ray diffraction and scattering measurements, a special X-ray diffractomator in which all the components, the X-ray source, the detector and the sample, were fixed was developed. A insident X-ray optics using two Johanson monochromator crystals were newly designed and developed to realize the in-situ observation with no motions. Using a compact vacuum chamber specially designed to use with the new optics, a evidence that semiconductor surfaces can really be observed using the system was obtained.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (19 results)

All 2014 2013 2012 2011 Other

All Journal Article (7 results) (of which Peer Reviewed: 3 results) Presentation (12 results)

  • [Journal Article] In situ X-ray investigation of changing barrier growth temperatures on InGaN single quantum wells in metal-organic vapor phase epitaxy2014

    • Author(s)
      Guangxu Ju, Yoshio Honda, Masao Tabuchi, Yoshikazu Takeda, and Hiroshi Amano
    • Journal Title

      J. Appl. Phys

      Volume: 115

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Analysis of Cs/GaAs NEA surface by XAFS2013

    • Author(s)
      K.Tsubota, M.Tabuchi, T.Nishitani, A.Era, Y.Takeda
    • Journal Title

      J. Phys. : Conf. Ser.

      Volume: Vol. 430 Pages: 12079-12079

    • Related Report
      2013 Final Research Report
  • [Journal Article] In-situ X-ray measurements of MOVPE growth of InGaN single quantum wells2013

    • Author(s)
      G. Ju
    • Journal Title

      J. Cryst. Growth

      Volume: 0 Pages: 0-0

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of X-ray diffractometer for in-situ observation of thin-film crystal growth equipped with focusing monochromator2011

    • Author(s)
      H.Tameoka, T.Kawase, M.Tabuchi, and Y.Takeda
    • Journal Title

      Physica Status Solidi C

      Volume: 8, No.2 Pages: 294-296

    • Related Report
      2013 Final Research Report
  • [Journal Article] Initial Stages of High-Temperature CaF2/Si(001) Epitaxial Growth Studied by Surface X-Ray Diffraction2011

    • Author(s)
      S.Suturin, N.Sokolov, A.Banshchikov, R.Kyutt, O.Sakata, T.Shimura, J.Harada, M.Tabuchi, and Y.Takeda
    • Journal Title

      J. Nanoscience and Nanotechnology

      Volume: Volume11, Number 4 Pages: 2990-2996

    • Related Report
      2013 Final Research Report
  • [Journal Article] Evaluation of newly developed X-ray diffractometer equipped with Johansson monochromator2011

    • Author(s)
      M.Tabuchi, H.Tameoka, T.Kawase, and Y.Takeda
    • Journal Title

      IOP Conf. Ser.

      Volume: Vol. 24 Pages: 12007-12007

    • Related Report
      2013 Final Research Report
  • [Journal Article] Evaluation of newly developed X-ray diffractometer equipped with Johansson monochromator2011

    • Author(s)
      M.Tabuchi, H.Tameoka, T.Kawase, Y.Takeda
    • Journal Title

      IOP Conf.Ser.

      Volume: 24 Pages: 12007-12007

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] 化合物半導体界面構造のX 線CTR 散乱測定による解析 -あいちSR の現状をまじえて-2013

    • Author(s)
      田渕雅夫
    • Organizer
      Workshop: CROSSroads of Users and J-PARC, 第7回「機能する界面、反応する表面」
    • Place of Presentation
      いばらき量子ビーム研究センター
    • Related Report
      2013 Final Research Report
  • [Presentation] 窒化物半導体結晶の特異構造形成を理解するためのX線によるその場観察装置の開2012

    • Author(s)
      田渕雅夫、益田征典、安西孝太、鞠光旭、二木浩之、森康博、渕真悟、竹田美和
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      早稲田大学早稲田キャンパス
    • Year and Date
      2012-03-15
    • Related Report
      2011 Annual Research Report
  • [Presentation] Analysis of Cs/GaAs NEA surface by XAFS2012

    • Author(s)
      K.Tsubota, A.Era, M.Tabuchi, T.Nishitani, Y.Takeda
    • Organizer
      The 15th Inter. Conf. X-ray Absorption Fine Structure (XAFS15), I1274
    • Place of Presentation
      Bejin, China
    • Related Report
      2013 Final Research Report
  • [Presentation] Observation of Position Dependence of InP/GaInAsP/InP Quantum Well Structure Grown on Pattern-Masked Substrate2012

    • Author(s)
      M.Tabuchi, K.Fujii, O.Sakata, M.Sugiyama, and Y.Takeda
    • Organizer
      Interational Union of Materials Research Scientists Inter. Conf. Electronic Materials 2012 (IUMRS-ICEM 2012), D7-101756
    • Place of Presentation
      Yokohama, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] GaAs に吸着したCs が作るNEA 表面のXAFS測定2012

    • Author(s)
      坪田光治、恵良淳史、田渕雅夫、竹田美和、西谷智博
    • Organizer
      第28回PF シンポジウム、UG-01-08
    • Place of Presentation
      つくば国際会議場
    • Related Report
      2013 Final Research Report
  • [Presentation] 窒化物半導体結晶の特異構造形成を理解するためのX 線によるその場観察装置の開発2012

    • Author(s)
      田渕雅夫、益田征典、安西孝太、鞠光旭、二木浩之、森康博、渕真悟、竹田美和
    • Organizer
      第59回応用物理学関係連合講演会、15p-F11-3
    • Place of Presentation
      早稲田大学 早稲田キャンパス
    • Related Report
      2013 Final Research Report
  • [Presentation] GaAs(110)基板上に作製したCs/GaAs-NEA表面2012

    • Author(s)
      坪田光治、恵良淳史、西谷智博、田渕雅夫
    • Organizer
      第15回XAFS 討論会、1O12
    • Place of Presentation
      白兎会館、鳥取
    • Related Report
      2013 Final Research Report
  • [Presentation] Observation of Position Dependence of InP/GaInAsP/InP Quantum Well Structure Grown on Pattern-Masked Substrate2012

    • Author(s)
      M. Tabuchi
    • Organizer
      Interational Union of Materials Research Scientists - Inter. Conf. Electronic Materials 2012 (IUMRS-ICEM 2012)
    • Place of Presentation
      Yokohama, Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] GaAs(110)基板上に作製したCs/GaAs-NEA表面2012

    • Author(s)
      坪田光治
    • Organizer
      第15回XAFS討論会
    • Place of Presentation
      白兎会館、鳥取
    • Related Report
      2012 Annual Research Report
  • [Presentation] ヨハンソン分光結晶を用いたX 線CTR 散乱の短時間測定系の開発2011

    • Author(s)
      二木浩之、益田征典、森康博、田渕雅夫、竹田美和
    • Organizer
      応用物理学会結晶工学分科会主催2011年・年末講演会、17
    • Place of Presentation
      学習院大学創立100周年記念会館
    • Year and Date
      2011-12-15
    • Related Report
      2013 Final Research Report
  • [Presentation] 蛍光収量法によるNEA 表面作製中のGaAs上へのCs 吸着量の測定2011

    • Author(s)
      坪田光治、恵良淳史、田渕雅夫、竹田美和、西谷智博
    • Organizer
      応用物理学会結晶工学分科会主催2011年・年末講演会、18
    • Place of Presentation
      学習院大学創立100周年記念会館
    • Year and Date
      2011-12-15
    • Related Report
      2013 Final Research Report
  • [Presentation] 可視光およびX線を用いた窒化物半導体結晶成長原子レベルその場観察

    • Author(s)
      鞠光旭, 渕真悟, 田渕雅夫, 竹田美和, 本田善央, 山口雅史, 天野浩
    • Organizer
      第74回応用物理学会秋季学術講演会
    • Place of Presentation
      同志社大学
    • Related Report
      2013 Annual Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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