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In-situ TEM observation of silicon fatigue process using resonance compressive fatigue test

Research Project

Project/Area Number 23360054
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionNagoya Institute of Technology

Principal Investigator

KAMIYA Shoji  名古屋工業大学, 工学(系)研究科(研究院), 教授 (00204628)

Co-Investigator(Renkei-kenkyūsha) SATO Kazuo  愛知工業大学, 工学研究科, 教授 (30262851)
NAKAJIMA Masahiro  名古屋大学, 工学研究科, 助教 (80377837)
IZUMI Hayato  名古屋工業大学, 工学研究科, 助教 (90578337)
MORITANI Tomokazu  名古屋工業大学, 工学研究科, 助教 (50362322)
Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥18,590,000 (Direct Cost: ¥14,300,000、Indirect Cost: ¥4,290,000)
Fiscal Year 2013: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2012: ¥6,500,000 (Direct Cost: ¥5,000,000、Indirect Cost: ¥1,500,000)
Fiscal Year 2011: ¥8,320,000 (Direct Cost: ¥6,400,000、Indirect Cost: ¥1,920,000)
Keywordsシリコン / MEMS / 疲労試験 / 圧縮応力 / TEM / その場観察 / 透過型電子顕微鏡 / EBIC / 再結合欠陥 / 透過電子顕微鏡 / 共振デバイス
Research Abstract

The purpose of this study is to observe directly silicon fatigue process from initial defect to fatigue fracture by in-situ TEM fatigue test for surveying the fatigue mechanism. Compressive-tensile test device with comb drive actuator was fabricated using SOI-MEMS technologies. TEG (test element group) device was electrically actuated by applying voltage under vacuum environment. For fatigue test with controlled stress ratio, TEM holder was developed by assembling a load cell, piezo actuator, and electrostatic probe. Under cyclic compressive load, accumulation of recombination defect was observed using electron beam induced current imaging. It was found that this defect was deeply related with decrease in fracture strength of silicon.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (40 results)

All 2014 2013 2012 2011 Other

All Journal Article (8 results) (of which Peer Reviewed: 8 results) Presentation (31 results) Remarks (1 results)

  • [Journal Article] Defect accumulation and strength reduction in single crystalline silicon induced by cyclic compressive stress2014

    • Author(s)
      S.Kamiya, T.Kita, H.Izumi
    • Journal Title

      Sensors and Actuators A

      Volume: 208 Pages: 30-36

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Defect accumulation and strength reduction in single crystalline silicon induced by cyclic compressive stress2014

    • Author(s)
      Shoji Kamiya, Toshifumi Kita, Hayato Izumi
    • Journal Title

      Sensors and Actuators A

      Volume: 208 Pages: 3036-3036

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A prediction scheme of the static fracture strength of MEMS structures based on the characterization of damage distribution on a processed surface2013

    • Author(s)
      V.L.Huy, S.Kamiya, K.Nagayoshi, H.Izumi, J.Gaspar, O.Paul
    • Journal Title

      Journal of Micromechanics and Microengineering

      Volume: 23

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] A prediction scheme of the static fracture strength of MEMS structures based on the characterization of damage distribution on a processed surface2013

    • Author(s)
      Vu Le Huy, Shoji, Kamiya, Kei Nagayoshi, Hayato Izumi, Joao Gaspar, Oliver Paul
    • Journal Title

      Journal of Micromechanics and Microengineering

      Volume: 23 Pages: 45008-45008

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Statistical characterization of fracture strength and fatigue lifetime of polysilicon thin films with different stress concentration fields2012

    • Author(s)
      V.L.Huy, S.Kamiya, J.Gaspar, O.Paul
    • Journal Title

      Journal of Solid Mechanics and Materials Engineering

      Volume: 6 Pages: 1013-1029

    • NAID

      130003323429

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Statistical characterization of fatigue lifetime of polysiliocn thin films2012

    • Author(s)
      V.L.Huy, J.Gaspar, O.Paul, S.Kamiya
    • Journal Title

      Sensors and Actuators A

      Volume: 179 Pages: 251-262

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Statistical characterization of fracture strength and fatigue lifetime of polysilicon thin films with different stress concentration fields2012

    • Author(s)
      Vu Le Huy, Shoji, Kamiya, Joao Gaspar, Oliver Paul
    • Journal Title

      Journal of Solid Mechanics and Materials Engineering

      Volume: 6 Pages: 10131029-10131029

    • NAID

      130003323429

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Statistical characterization of fatigue lifetime of polysilicon thin films2012

    • Author(s)
      Vu Le Huy, Joao Gaspar, Oliver Paul, Shoji Kamiya
    • Journal Title

      Sensors and Actuators A

      Volume: 179 Pages: 251-262

    • DOI

      10.1016/j.sna.2012.03.011

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] 繰り返し荷重によるシリコンの疲労損傷集積の観察2014

    • Author(s)
      泉隼人、喜多俊文、田中健太郎、神谷庄司
    • Organizer
      日本機械学会東海支部第63会総会講演会
    • Place of Presentation
      名古屋市
    • Related Report
      2013 Final Research Report
  • [Presentation] 繰り返し荷重によるシリコンの疲労損傷集積の観察2014

    • Author(s)
      泉隼人、喜多俊文、田中健太郎、神谷庄司
    • Organizer
      日本機械学会東海支部第63期総会
    • Place of Presentation
      大同大学、愛知県
    • Related Report
      2013 Annual Research Report
  • [Presentation] 繰り返し圧縮応力によるシリコン単結晶中の欠陥形成と残存引張強度2013

    • Author(s)
      喜多俊文、神谷庄司、泉隼人
    • Organizer
      日本機械学会2013年度年次大会
    • Place of Presentation
      岡山市
    • Related Report
      2013 Final Research Report
  • [Presentation] EBIC observation of the defects in single crystalline silicon induced by mechanical compressive stress2013

    • Author(s)
      T.Kita, S.Kamiya, H.Izumi
    • Organizer
      The 27th International Conference on Defects in Semiconductors 2013 (ICDS2013)
    • Place of Presentation
      Bologna, Italy
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] Direct observation of damage accumulation process inside silicon under mechanical fatigue loading2013

    • Author(s)
      S.Kamiya, R.Hirai, H.Izumi, N.Umehara, T.Tokoroyama
    • Organizer
      The 17th International Conference on Solid-State Sensors, Actuators, and Microsystems (Transducers2013&EurosensorsXXXVII)
    • Place of Presentation
      Barcelona, Spain
    • Related Report
      2013 Final Research Report
  • [Presentation] 単結晶シリコンの塑性特性における吸蔵水素の影響2013

    • Author(s)
      向山諒太、泉隼人、宍戸信之、神谷庄司
    • Organizer
      日本機械学会東海支部第62会総会講演会
    • Place of Presentation
      津市
    • Related Report
      2013 Final Research Report
  • [Presentation] 電子線誘起電流を用いた圧縮応力下におけるシリコン疲労損傷の観察2013

    • Author(s)
      喜多俊文、神谷庄司、泉隼人、梅原徳次、野老山貴行、Vu Le Huy、小川将史
    • Organizer
      日本機械学会東海支部第62会総会講演会
    • Place of Presentation
      津市
    • Related Report
      2013 Final Research Report
  • [Presentation] Direct observation of damage accumulation process inside silicon under mechanical fatigue loading2013

    • Author(s)
      Shoji Kamiya, Ryutaro Hirai, Hayato Izumi, Noritsugu Umehara, Takayuki Tokoroyama
    • Organizer
      Technical Digest of the 17th International Conference on Solid-State Sensors, Actuators, and Microsystems (Transducers2013&Eurosensors XXVII)
    • Place of Presentation
      Barcelona, Spain
    • Related Report
      2013 Annual Research Report
  • [Presentation] 繰り返し圧縮応力によるシリコン単結晶中の欠陥形成と残存引張強度2013

    • Author(s)
      喜多俊文、神谷庄司、泉隼人
    • Organizer
      日本機械学会2013年度年次大会
    • Place of Presentation
      岡山大学、岡山県
    • Related Report
      2013 Annual Research Report
  • [Presentation] 単結晶シリコンの塑性特性における吸蔵水素の影響2013

    • Author(s)
      向山諒太、泉隼人、宍戸信之、神谷庄司
    • Organizer
      日本機械学会東海支部第62期総会
    • Place of Presentation
      三重大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 電子線誘起電流を用いた圧縮応力下におけるシリコンの疲労損傷の観察2013

    • Author(s)
      喜多俊文、神谷庄司、泉隼人、梅原徳次、野老山貴行、Vu Le Huy、小川将史
    • Organizer
      日本機械学会東海支部第62期総会
    • Place of Presentation
      三重大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Mysteries in fracture behavior of silicon and polysilicon micro-scale structures in various environments and under repeated loading2012

    • Author(s)
      S.Kamiya
    • Organizer
      OKMETIC-Nagoya seminar 2012
    • Place of Presentation
      Nagoya
    • Year and Date
      2012-03-02
    • Related Report
      2013 Final Research Report
  • [Presentation] Mysteries in fracture behavior of silicon and polysilicon micro-scale structures in various environments and under repeated loading2012

    • Author(s)
      Shoji Kamiya
    • Organizer
      OKMETIC-Nagoya seminar 2012
    • Place of Presentation
      Nagoya, Japan(招待講演)
    • Year and Date
      2012-03-02
    • Related Report
      2011 Annual Research Report
  • [Presentation] IDENTIFICATION OF FATIGUE CRACK EXTENSION PROCESS INZERO-TENSION CYCLIC STRESS TEST OF POLYSILICON FILMS2012

    • Author(s)
      Vu Le Huy, Shoji Kamiya, Joao Gaspar, Oliver Paul
    • Organizer
      25th IEEE International Conference on Micro Electro Mechanical Systems
    • Place of Presentation
      Paris, France
    • Year and Date
      2012-01-30
    • Related Report
      2011 Annual Research Report
  • [Presentation] 繰返し応力に対するシリコンMEMS構造体の疲労寿命と長期信頼性評価2012

    • Author(s)
      神谷庄司
    • Organizer
      平成23年度第10回九州地区ナノテクノロジー拠点ネットワーク講演会
    • Place of Presentation
      北九州産業学術研究都市早稲田大学講義室(招待講演)
    • Year and Date
      2012-01-26
    • Related Report
      2011 Annual Research Report
  • [Presentation] 繰返し応力に対するシリコンMEMS 構造体の疲労寿命と信頼性評価2012

    • Author(s)
      神谷庄司
    • Organizer
      平成13年度第10回九州地区ナノテクノロジー拠点ネットワーク講演会
    • Place of Presentation
      北九州市
    • Year and Date
      2012-01-16
    • Related Report
      2013 Final Research Report
  • [Presentation] 異なる疲労機構に基づくシリコン微小構造物の寿命評価モデルの比較2012

    • Author(s)
      平川創、泉隼人、生津資大、神谷庄司
    • Organizer
      日本機械学会M&M2012材料力学カンファレンス
    • Place of Presentation
      松山市
    • Related Report
      2013 Final Research Report
  • [Presentation] TEM 内疲労試験その場観察を目的としたMEMS 共振デバイスの開発2012

    • Author(s)
      Lam Hoanson、泉隼人、神谷庄司
    • Organizer
      日本機械学会2012年度年次大会
    • Place of Presentation
      金沢市
    • Related Report
      2013 Final Research Report
  • [Presentation] 単結晶シリコン薄膜の破壊挙動に及ぼす水と温度の影響の評価2012

    • Author(s)
      Isram Md. Wahedul、泉隼人、小川将史、神谷庄司
    • Organizer
      日本機械学会2012年度年次大会
    • Place of Presentation
      金沢市
    • Related Report
      2013 Final Research Report
  • [Presentation] Identification of fatigue crack extension process inzero-tension cyclic stress test of polysilicon films2012

    • Author(s)
      V.L.Huy, S.Kamiya, J.Gaspar, O.Paul
    • Organizer
      25th IEEE International Conference on Micro Electro Mechanical Systems (MEMS2012)
    • Place of Presentation
      Paris, France
    • Related Report
      2013 Final Research Report
  • [Presentation] 異なる疲労機構に基づくシリコン微小構造物の寿命評価モデルの比較2012

    • Author(s)
      平川創、泉隼人、生津資大、神谷庄司
    • Organizer
      日本機械学会M&M2012材料力学カンファレンス
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] TEM内疲労試験その場観察を目的としたMEMS共振デバイスの開発2012

    • Author(s)
      Lam Hoanson、泉隼人、神谷庄司
    • Organizer
      日本機械学会2012年度年次大会
    • Place of Presentation
      金沢大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 単結晶シリコン薄膜の破壊挙動に及ぼす水と温度の影響の評価2012

    • Author(s)
      Isram Md. Wahedul、泉隼人、小川将史、神谷庄司
    • Organizer
      日本機械学会2012年度年次大会
    • Place of Presentation
      金沢大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Fracture Behavior of Silicon Thin Film under Liquid Water2011

    • Author(s)
      Hayato Izumi, Ya-Chi Cheng, Masayoshi Ishikawa, Shoji Kamiya, Ming-Tzer Lin
    • Organizer
      13th International Conference on Electronics Materials and Packaging
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2011-12-14
    • Related Report
      2011 Annual Research Report
  • [Presentation] 異なる試験手法により得られたシリコンの疲労挙動の相互比較2011

    • Author(s)
      神谷庄司、土屋智由、池原毅、佐藤一雄、安藤妙子、生津資大、高島和希
    • Organizer
      第3回マイクロ・ナノ工学シンポジウム
    • Place of Presentation
      船堀、東京
    • Year and Date
      2011-09-27
    • Related Report
      2011 Annual Research Report
  • [Presentation] 単結晶シリコンの疲労挙動とその環境依存性2011

    • Author(s)
      石川正芳、神谷庄司、泉隼人、宍戸信之
    • Organizer
      日本機械学会M&M 2011
    • Place of Presentation
      北九州、福岡
    • Year and Date
      2011-07-16
    • Related Report
      2011 Annual Research Report
  • [Presentation] ESTIMATION OF THE PARAMETERS DETERMINING STRENGTH AND FATIGUE BEHAVIORS OF ARBITRARILY-SHAPED POLYSILICON THIN FILMS2011

    • Author(s)
      Vu Le Huy, Joao Gaspar, Oliver Paul, Shoji Kamiya
    • Organizer
      ASME 2011 Pacific Rim Technical Conference & Exposition on Packaging and Integration of Electronic and Photonic Systems
    • Place of Presentation
      Portland, OR, USA
    • Year and Date
      2011-07-07
    • Related Report
      2011 Annual Research Report
  • [Presentation] Estimation of the parameters determining strength and fatigue behaviors of arbitrarily-shaped polysilicon thin films2011

    • Author(s)
      V.L.Huy, J.Gaspar, O.Paul, S.Kamiya
    • Organizer
      ASME2011 Pacific Rim Technical Conference & Exposition on Packaging and Integration of Electronic and Photonic Systems (InterPACK2011)
    • Place of Presentation
      Portland, USA
    • Related Report
      2013 Final Research Report
  • [Presentation] 単結晶シリコンの疲労挙動とその環境依存性2011

    • Author(s)
      石川正芳、神谷庄司、泉隼人、宍戸信之
    • Organizer
      日本機械学会M&M2011材料力学カンファレンス
    • Place of Presentation
      北九州市
    • Related Report
      2013 Final Research Report
  • [Presentation] 異なる試験手法により得られたシリコンの疲労挙動の相互比較2011

    • Author(s)
      神谷庄司、土屋智由、池原毅、佐藤一雄、安藤妙子、生津資大、高島和希
    • Organizer
      第3回マイクロ・ナノ工学シンポジウム
    • Place of Presentation
      船掘
    • Related Report
      2013 Final Research Report
  • [Presentation] Fracture behavior of silicon thin film under liquid water2011

    • Author(s)
      H.Izumi, Y.Cheng, M.Ishikawa, S.Kamiya, M-T.Lin
    • Organizer
      13th International Conference on Electronics Materials and Packaging (EMAP2011)
    • Place of Presentation
      Kyoto
    • Related Report
      2013 Final Research Report
  • [Remarks]

    • URL

      http://microsystemreliability.web.nitech.ac.jp

    • Related Report
      2013 Final Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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