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Piezoelectric thick film more than 100 miro-meters deposited by the ultrasonic assisted hydrothermal method

Research Project

Project/Area Number 23360134
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionThe University of Tokyo

Principal Investigator

MORITA Takeshi  東京大学, 新領域創成科学研究科, 准教授 (60344735)

Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥18,070,000 (Direct Cost: ¥13,900,000、Indirect Cost: ¥4,170,000)
Fiscal Year 2013: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Fiscal Year 2012: ¥9,100,000 (Direct Cost: ¥7,000,000、Indirect Cost: ¥2,100,000)
Fiscal Year 2011: ¥5,720,000 (Direct Cost: ¥4,400,000、Indirect Cost: ¥1,320,000)
Keywords厚膜 / 強誘電・圧電薄膜合成技術 / 強誘電・圧電薄膜 / 水熱合成法
Research Abstract

For medical ultrasonic devices and micro piezoelectric actuators, thick piezoelectric films are strongly demanded. In the conventional piezoelectric film deposition processes, the thickness have been limited because the crack was easily made inside the film due to high temperature crystallization process more than 600 degree C.
In this study, we focused on the hydrothermal method whose reaction temperature is 250 degree C. By developing the ultrasonic assisted hydrothermal method, we demonstrated a 172 micrometer thickness of potassium niobate film.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (45 results)

All 2014 2013 2012 2011 Other

All Journal Article (12 results) (of which Peer Reviewed: 12 results) Presentation (31 results) (of which Invited: 3 results) Remarks (2 results)

  • [Journal Article] Synthesis of lead-free piezoelectric powders by ultrasonic assisted hydrothermal method and properties of sintered (K_0.48Na_0.52)NbO_3 ceramics2014

    • Author(s)
      Gaku Isobe, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Journal Title

      IEEE Trans. on UFFC

      Volume: vol. 61 Pages: 225-230

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] The hardening of CuO-(K, Na)NbO_3 via post annealing with argon2014

    • Author(s)
      Yaoyang Liu, Takafumi Maeda, Yuriko Yokouchi and Takeshi Morita
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: vol. 53 Pages: 15503-15503

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of lead-free piezoelectric powders by ultrasonic assisted hydrothermal method and properties of sintered (K0.48Na0.52)NbO3 ceramics2014

    • Author(s)
      Gaku Isobe, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Journal Title

      IEEE Trans. on UFFC

      Volume: 61 Issue: 2 Pages: 225-230

    • DOI

      10.1109/tuffc.2014.6722608

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The hardening of CuO-(K, Na)NbO3 via post annealing with argon2014

    • Author(s)
      Yaoyang Liu, Takafumi Maeda, Yuriko Yokouchi and Takeshi Morita
    • Journal Title

      Jpn. J. Appl. Phys.

      Volume: 53 Issue: 1 Pages: 15503-15503

    • DOI

      10.7567/jjap.53.015503

    • NAID

      210000143244

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Study on optimizing ultrasonic irradiation period for thick polycrystalline PZT film by hydrothermal method2013

    • Author(s)
      Kanako Ohta, Gaku Isobe, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Journal Title

      Ultrasonics

      Volume: vol. 53 Pages: 837-841

    • Related Report
      2013 Annual Research Report 2013 Final Research Report 2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Piezoelectric properties of CuO-doped (K,Na)NbO3 lead-free ceramics synthesized with hydrothermal powders2013

    • Author(s)
      Yuriko Yokouchi, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: vol. 52

    • NAID

      210000142475

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ultrasonic-assisted hydrothermal deposition of ferroelectric PbZrO_3 thin film on NiTi-based superelastic shape memory alloys2012

    • Author(s)
      Florian Schiedeck and Takeshi Morita
    • Journal Title

      Journal of Electroceramics

      Volume: vol. 28 Pages: 45-52

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Piezoelectric properties of Li-doped (K_0.48Na_0.52)NbO_3 ceramics synthesized using hydrothermally-derived KNbO_3 and NaNbO_3 fine powders2012

    • Author(s)
      Takafumi Maeda, Tobias Hemsel, and Takeshi Morita
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: vol. 51

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Piezoelectric Properties of Li-Doped (Ko. 48Nao. 52)Nb03 Ceramics Synthesized ITgincy Hvdrothermallv-Derived KNbOs and NaNbQa Fine Powders2012

    • Author(s)
      Takafumi Maeda, Tobias Hemsel, Takeshi Morita
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 51 Issue: 9S2 Pages: 09MD08-09MD08

    • DOI

      10.1143/jjap.51.09md08

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ultrasonic-assisted hydrothermal deposition of ferroelectric PbZrO_3 thin film on NiTi-based superelastic shape memory alloys2012

    • Author(s)
      Florian Schiedeck, Takeshi Morita
    • Journal Title

      Journal of Electroceramics

      Volume: 28 Issue: 1 Pages: 45-52

    • DOI

      10.1007/s10832-011-9676-1

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improved process for the hydrothermal lead-free piezoelectric powders and the performances of sintered (K_0.48Na_0.52)NbO_3 ceramics2011

    • Author(s)
      Takafumi Maeda, Tobias Hemsel and Takeshi Morita
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: vol. 50

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Improved Process for Hydrothermal Lead-Free Piezoelectric Powders and Performances2011

    • Author(s)
      Takafumi Maeda, Tobias Hemsel, Takeshi Morita
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 50 Issue: 7S Pages: 07HC01-07HC01

    • DOI

      10.1143/jjap.50.07hc01

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] Synthesis of lead-free piezoelectric material by ultrasonic assisted hydrothermal method2014

    • Author(s)
      Gaku Isobe, Kanako Ohta, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      IWPMA2012
    • Place of Presentation
      弘前
    • Year and Date
      2014-04-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Mn-doped (K,Na)NbO3 lead-free piezoelectric ceramics fabricated with hydrothermal powders2014

    • Author(s)
      Yuriko Yokouchi, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      IWPMA 2012
    • Place of Presentation
      弘前
    • Year and Date
      2014-04-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Hydrothermal method for piezoelectric materials and their applications2013

    • Author(s)
      Takeshi Morita
    • Organizer
      SPIE Micro+Nano Materials, Devices, and Applications
    • Place of Presentation
      オーストラリア メルボルン
    • Year and Date
      2013-12-11
    • Related Report
      2013 Final Research Report
  • [Presentation] Studies on potassium niobate thick films by ultrasonic assisted hydrothermal method2013

    • Author(s)
      Ryo Kudo, Gaku Isobe, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      ICAE 2013
    • Place of Presentation
      韓国 済州島
    • Year and Date
      2013-11-13
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] Ultrasonic assisted hydrothermal method for thick piezoelectric films2013

    • Author(s)
      Takeshi Morita, Ryo Kudo and Kanako Ohta
    • Organizer
      16th US-Japan Seminar on Dielectric and Piezoelectric Materials
    • Place of Presentation
      アメリカ ノースカロライナ
    • Year and Date
      2013-11-04
    • Related Report
      2013 Final Research Report
  • [Presentation] Piezoelectric actuators using LiNbO_3 single crystals2013

    • Author(s)
      Takeshi Morita
    • Organizer
      International Workshop on Stoichiometric Lithium Niobate
    • Place of Presentation
      ドイツ ゴスラー
    • Year and Date
      2013-09-20
    • Related Report
      2013 Final Research Report
  • [Presentation] Self-sensing ultrasound transducer for cavitation monitoring2013

    • Author(s)
      Peter Bornmann, Takafumi Maeda, Tobias Hemsel, Takeshi Morita, Walter Sextro
    • Organizer
      IWPMA2013
    • Place of Presentation
      ドイツ ハノーファー
    • Year and Date
      2013-07-17
    • Related Report
      2013 Final Research Report
  • [Presentation] Piezoelectric applications of hydrothermal (K_0.48Na_0.52) NbO_3 ceramics2013

    • Author(s)
      Takafumi Maeda, Peter Bornmann, Tobias Hemsel, Takeshi Morita
    • Organizer
      IWPMA 2013
    • Place of Presentation
      ドイツハノーファー
    • Year and Date
      2013-07-16
    • Related Report
      2013 Final Research Report
  • [Presentation] Domain orientation controlled KN family piezoelectric materials with hydrothermal powders2013

    • Author(s)
      Yukiko Fujiuchi, Takajumi Maeda and Takeshi Morita
    • Organizer
      IWPMA 2013
    • Place of Presentation
      ドイツ ハノーファー
    • Year and Date
      2013-07-16
    • Related Report
      2013 Final Research Report
  • [Presentation] Ultrasonic-assisted hydrothermal method for the piezoelectric materials2013

    • Author(s)
      Takeshi Morita, Gaku Isobe, Kanako Ohta, Ryo Kudoh, Takafumi Maeda, Peter Bornmann and Tobias Hemsel
    • Organizer
      ISHA2013
    • Place of Presentation
      アメリカ テキサス
    • Year and Date
      2013-01-15
    • Related Report
      2013 Final Research Report
  • [Presentation] Ultrasonic-assisted hydrothermal method for the piezoelectric materials2013

    • Author(s)
      Takeshi MORITA
    • Organizer
      The 3rd International Solvothermal and Hydrothermal Associateion conference 2013 (ISHA2013)
    • Place of Presentation
      Austin/USA
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Polycrystaline PZT film on porous Ti substrate synthesized by ultrasonic assisted hydrothermal method2012

    • Author(s)
      Kanako Ohta, Gaku Isobe, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      Iinternational Ultrasonics Symposium 2012
    • Place of Presentation
      ドイツ ドレスデン
    • Year and Date
      2012-10-08
    • Related Report
      2013 Final Research Report
  • [Presentation] Study on PZT Film deposited by ultrasonic assisted hydrothermal method2012

    • Author(s)
      Kanako Ohta, Gaku Isobe, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      IWPMA 2012
    • Place of Presentation
      横浜
    • Year and Date
      2012-09-26
    • Related Report
      2013 Final Research Report
  • [Presentation] (K_0.48Na_0.52)NbO_3 ceramics using powders synthesized by ultrasonic assisted hydrothermal method2012

    • Author(s)
      Gaku Isobe, Takufumi Maeda, Kanako Ohta, Yuriko Yokouchi, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      IUMRS-ICEM2012
    • Place of Presentation
      横浜
    • Year and Date
      2012-09-25
    • Related Report
      2013 Final Research Report
  • [Presentation] Applications for lead-free piezoelectric materials2012

    • Author(s)
      Peter Bornmann, Tobias Hemsel, Takefumi Maeda, Takeshi Morita and Walter Sextro
    • Organizer
      IWPMA2012
    • Place of Presentation
      弘前
    • Year and Date
      2012-04-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Investigation of sound field in sonochemical reactors2012

    • Author(s)
      Peter Bornmann, Tobias Hemsel, Takeshi MORITA and Walter Sextro
    • Organizer
      IWPMA2012
    • Place of Presentation
      弘前
    • Year and Date
      2012-04-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Polycrystaline PZT film on Porous Ti substrate synthesized by Ultrasonic Assisted hydrothermal Method2012

    • Author(s)
      Kanako Ohta
    • Organizer
      InternationalUltrasonics Symposium 2012
    • Place of Presentation
      Dresden/Germany
    • Related Report
      2012 Annual Research Report
  • [Presentation] The Study on PZT film Deposited by Ultrasonic Assisted Hydrothermal Method and its Effect of Ultrasonic Irradiation2012

    • Author(s)
      Kanako Ohta
    • Organizer
      IUMRS-ICEM2012
    • Place of Presentation
      Yokohama/Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] (K0.48Na0.52)NbO3 Ceramics Using Powders Synthesized by UltrasonicAssisted Hydrothermal Method2012

    • Author(s)
      Gaku Isobe
    • Organizer
      IUMRS-ICEM2012
    • Place of Presentation
      Yokohama/Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Investigation of sound field in sonochemical reactor2012

    • Author(s)
      Peter Bornmann
    • Organizer
      IWPMA2012
    • Place of Presentation
      Hirosaki/Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Piezoelectric properties of lithium modified potassium sodium niobate ceramics synthesized by hydrothermal method2011

    • Author(s)
      Takafumi Maeda, Yuriko Yokouchi, Tobias Hemsel and Takeshi Morita
    • Organizer
      International Conference on Advanced Electromaterials2011
    • Place of Presentation
      韓国 済州島
    • Year and Date
      2011-11-10
    • Related Report
      2013 Final Research Report
  • [Presentation] 超音波アシスト水熱合成法によるPZT薄膜に関する研究2011

    • Author(s)
      太田賀奈子, 五十部学, Peter BORNMANN, Tobias HEMSEL, 森田剛
    • Organizer
      日本電子材料技術協会第48回秋季講演大会
    • Place of Presentation
      日本電子材料技術協会事務局・東京
    • Year and Date
      2011-11-10
    • Related Report
      2011 Annual Research Report
  • [Presentation] 超音波アシスト水熱合成法のための高温対応振動子の開発2011

    • Author(s)
      五十部学, ペーター・ボーンマン, トビアス・ヘムゼル, 森田剛
    • Organizer
      第32回超音波エレクトロニクスの基礎と応用に関するシンポジウム
    • Place of Presentation
      京都大学・京都
    • Year and Date
      2011-11-08
    • Related Report
      2011 Annual Research Report
  • [Presentation] Ultrasonic assisted hydrothermal method for piezoelectric thin films and powders2011

    • Author(s)
      Takeshi Morita
    • Organizer
      62nd ICAT International Smart Actuator Symposium
    • Place of Presentation
      アメリカ ペンステート
    • Year and Date
      2011-10-04
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Ultrasonic assisted hydrothermal method for piezoelectric thin films and powders2011

    • Author(s)
      Takeshi MORITA
    • Organizer
      62nd ICAT International Smart Actuator Symposium
    • Place of Presentation
      PennState, USA(招待講演)
    • Year and Date
      2011-10-04
    • Related Report
      2011 Annual Research Report
  • [Presentation] Synthesis of piezoelectric materials by ultrasonic hydrothermal method2011

    • Author(s)
      Gaku Isobe, Ryo Ageba, Takafumi Maeda, Peter Bornmann, Tobias Hemsel and Takeshi Morita
    • Organizer
      International Congress on Ultrasonics
    • Place of Presentation
      ポーランド グダンスク
    • Year and Date
      2011-09-06
    • Related Report
      2013 Final Research Report
  • [Presentation] 超音波アシスト水熱合成法による圧電材料の合成2011

    • Author(s)
      五十部学, 揚場遼, 前田孝文, ペーターボルンマン, トビアスヘムゼル, 森田剛
    • Organizer
      第23回電磁力関連のダイナミクスシンポジウム
    • Place of Presentation
      愛知県産業労働センター・名古屋
    • Year and Date
      2011-05-19
    • Related Report
      2011 Annual Research Report
  • [Presentation] Hydrothermal method for piezoelectric materials and their applications (invited)

    • Author(s)
      Takeshi Morita
    • Organizer
      SPIE Micro+Nano Materials, Devices, and Applications
    • Place of Presentation
      オーストラリア メルボルン
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Ultrasonic assisted hydrothermal method for thick piezoelectric films

    • Author(s)
      Takeshi Morita, Ryo Kudo and Kanako Ohta
    • Organizer
      16th US-Japan Seminar on Dielectric and Piezoelectric Materials
    • Place of Presentation
      アメリカ ノースカロライナ
    • Related Report
      2013 Annual Research Report
  • [Presentation] Piezoelectric actuators using LiNbO3 single crystals

    • Author(s)
      Takeshi Morita
    • Organizer
      International Workshop on Stoichiometric Lithium Niobate
    • Place of Presentation
      ドイツ ゴスラー
    • Related Report
      2013 Annual Research Report
  • [Presentation] Self-sensing ultrasound transducer for cavitation monitoring

    • Author(s)
      Peter Bornmann, Takafumi Maeda, Tobias Hemsel, Takeshi Morita, Walter Sextro
    • Organizer
      IWPMA 2013
    • Place of Presentation
      ドイツ ハノーファー
    • Related Report
      2013 Annual Research Report
  • [Remarks]

    • URL

      http://www.ems.k.u-tokyo.ac.jp/morita/

    • Related Report
      2013 Final Research Report
  • [Remarks]

    • URL

      http://www.ems.k.u-tokyo.ac.jp

    • Related Report
      2011 Annual Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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