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Fabrication of microscopic infrared spectrum analysis system for in-situ observation of chemical reaction in the water

Research Project

Project/Area Number 23360282
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionTokyo University of Science

Principal Investigator

ISHIGURO Takashi  東京理科大学, 基礎工学部, 教授 (10183162)

Co-Investigator(Kenkyū-buntansha) TAMURA Kouji  東京理科大学, 基礎工学部, 教授 (30271547)
HYASE Masanori  東京理科大学, 理工学部, 准教授 (70293058)
NAKAMURA Yoshio  東京工業大学, 理工学研究科, 教授 (00164351)
Co-Investigator(Renkei-kenkyūsha) TAMURA Kouji  東京理科大学, 基礎工学部, 教授 (30271547)
HAYASE Masanori  東京理科大学, 理工学部, 准教授 (70293058)
Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥19,760,000 (Direct Cost: ¥15,200,000、Indirect Cost: ¥4,560,000)
Fiscal Year 2013: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Fiscal Year 2012: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Fiscal Year 2011: ¥14,560,000 (Direct Cost: ¥11,200,000、Indirect Cost: ¥3,360,000)
Keywords透過赤外分光 / 水熱反応 / バイオ・ソフトマター / 水 / 赤外顕微分光 / ATP / FT-IR / ADP / MEMS
Research Abstract

A stable and high-speed transmission infrared spectroscopy system for in-situ observation of chemical reaction in the water was fabricated. In-situ transmission infrared spectroscopy of hydroxylation of metallic film and subsequent dehydration processes were observed. Systematic change of absorbance in the three phases and the supercritical phase of the water were also observed and evaluated their states of the hydrogen bond. Furthermore, absorbance spectra of the adenosine triphosphate solution were observed and identification of the decomposed components was achieved. As a result, it was confirmed that transmission infrared spectroscopy was useful for the evaluation of chemical reaction in the aqueous solution.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (31 results)

All 2014 2013 2012 2011 Other

All Journal Article (4 results) (of which Peer Reviewed: 2 results) Presentation (27 results)

  • [Journal Article] In-situ Transmission Infrared Spectroscopy of Hydroxylation of Aluminum Thin Film and Subsequent Dehydration Processes2014

    • Author(s)
      Takuji Ube, Takashi Harumoto, Takashi Ishiguro
    • Journal Title

      Jap. J. Appl. Phys.

      Volume: 53 Issue: 6 Pages: 066701-066701

    • DOI

      10.7567/jjap.53.066701

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of liposome reinforced with cholesterol and application to transmission electron microscopy observation2013

    • Author(s)
      Marina Kamogawa, Takuji Ube, Junichi Shimanuki, Takashi Harumoto, Makoto Yuasa, and Takashi Ishiguro
    • Journal Title

      MRS Online Proceedings Library

      Volume: vol.1498

    • DOI

      10.1557/opl.2013.390

    • Related Report
      2013 Final Research Report 2012 Annual Research Report
  • [Journal Article] Formation of Anti-Reflection Coating by Hydrothermal Treatment of Aluminum Films and Their Stabilization by Dehydration2013

    • Author(s)
      Aki Egashira, Takuji Ube, Yusuke Hosoki, Takashi Harumoto and Takashi Ishiguro
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 54 Issue: 6 Pages: 1025-1028

    • DOI

      10.2320/matertrans.M2013026

    • NAID

      10031176428

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Transmission Electron Microscopy Observation of Antibody2012

    • Author(s)
      Marina Kamogawa, Junichi Shimanuki, Takachika Azuma, Akikazu Murakami, Takashi Ishiguro
    • Journal Title

      Procedia Engineering

      Volume: vol.36 Pages: 150-153

    • DOI

      10.1016/j.proeng.2012.03.023

    • Related Report
      2013 Final Research Report 2012 Annual Research Report
  • [Presentation] In-situ Transmission Infrared Spectroscopy of ATP in Aqueous Solutions2014

    • Author(s)
      Masayuki Watanabe, Toru Ishizuka, Takuji Ube, Takashi Harumoto, Koji Tamura, Shin Aoki, and Takashi Ishiguro
    • Organizer
      International Symposium on Technologies against Cancer 2014
    • Place of Presentation
      Katsushika Campus, Tokyo University of Science, Tokyo, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] エタノール水溶液の透過赤外吸収スペクトルその場観察2014

    • Author(s)
      宇部卓司, 中山璃子, 春本高志, 石黒孝
    • Organizer
      2014年日本金属学会春期大会
    • Place of Presentation
      東京工業大学(大岡山キャンパス)
    • Related Report
      2013 Final Research Report
  • [Presentation] In-situ Transmission Infrared Spectroscopy of ATP in Aqueous Solutionv2014

    • Author(s)
      Masayuki Watanabe, Toru Ishizuka, Takuji Ube, Takashi Harumoto, Koji Tamura, Shin Aoki, and Takashi Ishiguro
    • Organizer
      International Symposium on Technologies against Cancer 2014
    • Place of Presentation
      Katsushika Campus, Tokyo University of Science, Tokyo, Japan
    • Related Report
      2013 Annual Research Report
  • [Presentation] エタノール水溶液の透過赤外吸収スペクトルその場観察2014

    • Author(s)
      宇部卓司、中山璃子、春本高志、石黒孝
    • Organizer
      2014年日本金属学会春期大会
    • Place of Presentation
      東京工業大学(大岡山キャンパス)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fe, Co, Ni 遷移金属膜の高温高圧水熱反応2013

    • Author(s)
      冨永知宏, 石塚徹, 春本高志, 石黒孝
    • Organizer
      2013年日本金属学会春期大会
    • Place of Presentation
      東京理科大学(神楽坂キャンパス)
    • Related Report
      2013 Final Research Report
  • [Presentation] メゾスコピック凹凸アルミナ表面形成によるガラスの高透過率化2013

    • Author(s)
      阿曽亮介, 春本高志, 石黒孝
    • Organizer
      2013年日本金属学会春期大会
    • Place of Presentation
      東京理科大学(神楽坂キャンパス)
    • Related Report
      2013 Final Research Report
  • [Presentation] Development of In-situ Transmission FT-IR Measurement of Supercritical Water2013

    • Author(s)
      Takuji Ube, Takashi Harumoto and Takashi Ishiguro
    • Organizer
      Materials Research Society Spring Meeting 2013
    • Place of Presentation
      San Francisco, CA USA
    • Related Report
      2013 Final Research Report
  • [Presentation] Transmission Infrared Absorption Spectroscopy of ATP in Aqueous Solution2013

    • Author(s)
      Masayuki Watanabe, Toru Ishizuka, Takuji Ube, Takashi Harumoto, Koji Tamura, Shin Aoki, and Takashi Ishiguro
    • Organizer
      2013 Taiwan-Japan Symposium on Polyscale Technologies for Biomedical Engineering and Environmental Sciences (PT-BMES 2013)
    • Place of Presentation
      Tokyo University of Science, Oshamambe, Hokkaido, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] 第一原理計算による水の赤外吸収スペクトルのシミュレーション2013

    • Author(s)
      石塚徹, 宇部卓司, 春本高志, 中村吉男, 石黒孝
    • Organizer
      2013年第74回応用物理学会秋季学術講演会
    • Place of Presentation
      同志社大学
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] Development of In-situ Transmission FT-IR Measurement of Supercritical Water2013

    • Author(s)
      Takuji Ube, Takashi Harumoto and Takashi Ishiguro
    • Organizer
      Materials Research Society Fall Meeting 2013
    • Place of Presentation
      San Francisco, CA USA
    • Related Report
      2013 Annual Research Report
  • [Presentation] Infrared Microscopy Study on Hydrogen Bonding State of Aqueous Acetone Solution2013

    • Author(s)
      Takuji Ube, Toru Ishizuka, Takashi Harumoto, and Takashi Ishiguro
    • Organizer
      2013 JAPAN-TAIWAN SYMPOSIUM ON POLYSCALE TECHNOLOGIES FOR BIOMEDICAL ENGINEERING AND ENVIRONMENTAL SCIENCES (PT-BMES 2013)
    • Place of Presentation
      Tokyo University of Science, Oshamambe, Hokkaido, Japan
    • Related Report
      2013 Annual Research Report
  • [Presentation] Transmission Infrared Absorption Spectroscopy of ATP in Aqueous Solution2013

    • Author(s)
      Masayuki Watanabe, Toru Ishizuka, Takuji Ube, Takashi Harumoto, Koji Tamura, Shin Aoki, and Takashi Ishiguro
    • Organizer
      2013 JAPAN-TAIWAN SYMPOSIUM ON POLYSCALE TECHNOLOGIES FOR BIOMEDICAL ENGINEERING AND ENVIRONMENTAL SCIENCES (PT-BMES 2013)
    • Place of Presentation
      Tokyo University of Science, Oshamambe, Hokkaido, Japan
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fe, Co, Ni遷移金属膜の高温高圧水熱反応2013

    • Author(s)
      冨永知宏、石塚徹、春本高志、石黒孝
    • Organizer
      2013年日本金属学会春期大会
    • Place of Presentation
      東京理科大学(神楽坂キャンパス)
    • Related Report
      2012 Annual Research Report
  • [Presentation] メゾスコピック凹凸アルミナ表面形成によるガラスの高透過率化2013

    • Author(s)
      阿曽亮介、春本高志、石黒孝
    • Organizer
      2013年日本金属学会春期大会
    • Place of Presentation
      東京理科大学(神楽坂キャンパス)
    • Related Report
      2012 Annual Research Report
  • [Presentation] In-situ Infrared Spectroscopic Study of Hydrogen Bonds in Supercritical Water and Methanol2012

    • Author(s)
      Takuji Ube, Takashi Harumoto, and Takashi Ishiguro
    • Organizer
      2012 Taiwan-Japan Symposium on Polyscale Technologies for Biomedical Engineering and Environmental Sciences (PT-BMES 2012)
    • Place of Presentation
      National Tsing Hua University, Hsinchu, Taiwan
    • Year and Date
      2012-09-05
    • Related Report
      2013 Final Research Report
  • [Presentation] Transmission FT-IR Spectroscopy of ATP-Mg Complex in Aqueous Solution2012

    • Author(s)
      Masayuki Watanabe, Takuji Ube, Koji Tamura, Shin Aoki, Takashi Harumoto, and Takashi Ishiguro
    • Organizer
      2012 Taiwan-Japan Symposium on Polyscale Technologies for Biomedical Engineering and Environmental Sciences (PT-BMES 2012)
    • Place of Presentation
      National Tsing Hua University, Hsinchu, Taiwan
    • Year and Date
      2012-09-05
    • Related Report
      2013 Final Research Report
  • [Presentation] 水熱・脱水反応過程のその場・透過赤外吸収スペクトル測定2012

    • Author(s)
      宇部卓司, 石黒 孝
    • Organizer
      2012年日本金属学会春期大会
    • Place of Presentation
      横浜国立大学
    • Related Report
      2013 Final Research Report 2011 Annual Research Report
  • [Presentation] 過冷却水中Mg 水和反応その場・透過赤外吸収スペクトル測定2012

    • Author(s)
      宇部卓司, 佐藤和裕, 春本高志, 石黒孝
    • Organizer
      2012年日本金属学会秋期大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2013 Final Research Report
  • [Presentation] Mg 膜の低温水による膜改質2012

    • Author(s)
      佐藤和裕, 宇部卓司, 春本高志, 石黒孝
    • Organizer
      2012年日本金属学会秋期大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2013 Final Research Report
  • [Presentation] 過冷却水中Mg水和反応その場・透過赤外吸収スペクトル測定2012

    • Author(s)
      宇部卓司, 佐藤和裕, 春本高志, 石黒孝
    • Organizer
      2012年日本金属学会秋期(第151回)大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Mg膜の低温水による膜改質2012

    • Author(s)
      佐藤和裕, 宇部卓司, 春本高志, 石黒孝
    • Organizer
      2012年日本金属学会秋期(第151回)大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Antireflection Coating of γ-alumina with Gradient-refractive Index Structure2011

    • Author(s)
      Yusyke Hosoki, Takuji Ube, and Takashi Ishiguro
    • Organizer
      ISES Solar World Congress 2011
    • Place of Presentation
      Congress Palais in Kassel, Germany
    • Related Report
      2013 Final Research Report 2011 Annual Research Report
  • [Presentation] In-situ Infrared Spectroscopy of Reaction between Aluminum Thin Film and Ultrapure Water2011

    • Author(s)
      Takuji Ube and Takashi Ishiguro
    • Organizer
      12th International Union of Materials Reserch Soc ieties International Conference in Asia 2011
    • Place of Presentation
      Taipei World Trade Center Nangang Exhibition Hall, Taiwan
    • Related Report
      2013 Final Research Report
  • [Presentation] In-situ Infrared Spectroscopy of Reaction between Aluminum Thin Film and Ultrapure Water2011

    • Author(s)
      Takuji Ube, Takashi Ishiguro
    • Organizer
      12^<th> International Union of Materials Reserch Societies International Conference in Asia 2011
    • Place of Presentation
      Taipei World Trade Center Nangang Exhibition Hall, Taiwan
    • Related Report
      2011 Annual Research Report
  • [Presentation] In-situ Infrared Spectroscopic Study of Hydrogen Bonds in Supercritical Water and Methanol

    • Author(s)
      Takuji Ube, Takashi Harumoto, and Takashi Ishiguro
    • Organizer
      2012 TAIWAN-JAPAN SYMPOSIUM ON POLYSCALE TECHNOLOGIES FOR BIOMEDICAL ENGINEERING AND ENVIRONMENTAL SCIENCES (PT-BMES 2012)
    • Place of Presentation
      National Tsing Hua University, Hsinchu, Taiwan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Transmission FT-IR Spectroscopy of ATP-Mg Complex in Aqueous Solution

    • Author(s)
      Masayuki Watanabe, Takuji Ube, Koji Tamura, Shin Aoki, Takashi Harumoto, and Takashi Ishiguro
    • Organizer
      2012 TAIWAN-JAPAN SYMPOSIUM ON POLYSCALE TECHNOLOGIES FOR BIOMEDICAL ENGINEERING AND ENVIRONMENTAL SCIENCES (PT-BMES 2012)
    • Place of Presentation
      National Tsing Hua University, Hsinchu, Taiwan
    • Related Report
      2012 Annual Research Report
  • [Presentation] バイオ・ソフトマターの透過電子顕微鏡観察

    • Author(s)
      加茂川まりな、島貫純一、宇部卓司、春本高志、湯浅真、浜田典昭、石黒孝
    • Organizer
      日本顕微鏡学会関東支部 第37回講演会
    • Place of Presentation
      東京大学本郷キャンパス 山上会館(東京)
    • Related Report
      2012 Annual Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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