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Develpment of Biomedical Ti-based Shape Memory and Superelastic Alloys

Research Project

Project/Area Number 23360300
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionUniversity of Tsukuba

Principal Investigator

MIYAZAKI Shuichi  筑波大学, 数理物質系, 教授 (50133038)

Research Collaborator KIM Hee Young  筑波大学, 数理物質系, 准教授 (20333841)
Project Period (FY) 2011-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥19,240,000 (Direct Cost: ¥14,800,000、Indirect Cost: ¥4,440,000)
Fiscal Year 2013: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2012: ¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2011: ¥10,660,000 (Direct Cost: ¥8,200,000、Indirect Cost: ¥2,460,000)
Keywords新機能材料 / 形状記憶合金 / チタン合金 / 超弾性合金 / マルテンサイト変態 / 形状記憶効果
Research Abstract

In order to develop novel biomedical shape memory alloys, the effects of composi-
tion and microstructure on martensitic transformation temperatures, shape memory and superelastic proper- ties and mechanical properties of Ti-base alloys were systematically investigated. Through the optimiza- tion of composition and microstructures by thermo-mechanical treatment, a larger superelastic recovery strain larger than 5% was obtained in Ti-Nb-Zr-Sn and Ti-Nb-Zr-Al alloys. The suppression of omega phase was very useful to decrease the stress hysteresis and to increase superelastic recovery strain in Ti-basedsuperelastic alloys.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Research Products

    (32 results)

All 2014 2013 2012 2011 Other

All Journal Article (13 results) (of which Peer Reviewed: 11 results) Presentation (16 results) (of which Invited: 5 results) Remarks (1 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Effect of Sn addition on stress hysteresis and superelastic properties of a Ti-15Nb-3Mo alloy2014

    • Author(s)
      M.F. Ijaz, H.Y. Kim, H. Hosoda, S. Miyazaki
    • Journal Title

      Scripta Materialia

      Volume: Vol.72-73 Pages: 29-32

    • DOI

      10.1016/j.scriptamat.2013.10.007

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Origin of {332} twinning in metastable β-Ti alloys2014

    • Author(s)
      H. Tobe, H.Y. Kim, T. Inamura, H. Hosoda, S. Miyazaki
    • Journal Title

      Acta Materialia

      Volume: Vol.64 Pages: 345-355

    • DOI

      10.1016/j.actamat.2013.10.048

    • NAID

      120007136186

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] 生体用形状記憶合金2014

    • Author(s)
      金 熙榮、宮崎修一
    • Journal Title

      日本材料科学会誌

      Volume: 51 Pages: 6-9

    • Related Report
      2013 Annual Research Report
  • [Journal Article] Nanodomain structure and its effect on abnormal thermal expansion behavior of a Ti-23Nb-2Zr-0.7Ta-1.2O alloy2013

    • Author(s)
      H.Y. Kim, L. Wei, S. Kobayashi, M. Tahara, S. Miyazaki
    • Journal Title

      Acta Materialia

      Volume: Vol.61 Issue: 13 Pages: 4874-4886

    • DOI

      10.1016/j.actamat.2013.04.060

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Nb content on deformation behavior and shape memory properties of Ti-Nb alloys2012

    • Author(s)
      Hirobumi Tobe
    • Journal Title

      Journal of Alloys and Compounds

      Volume: (印刷中) Pages: 435-438

    • DOI

      10.1016/j.jallcom.2012.02.023

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Room temperature aging behavior of Ti-Nb-Mo-based superelastic alloys2012

    • Author(s)
      Y. Al-Zain, H.Y. Kim, T. Koyano, H. Hosod, T.H. Nam, S. Miyazaki
    • Journal Title

      Acta Materialia

      Volume: Vol.59 Issue: 5 Pages: 1464-1473

    • DOI

      10.1016/j.actamat.2011.12.033

    • ISSN
      1359-6454
    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ti-Ni基およびTi基新規形状記憶合金の開発2012

    • Author(s)
      金 熙榮、宮崎修一
    • Journal Title

      金属

      Volume: 82 Pages: 466-472

    • Related Report
      2012 Annual Research Report
  • [Journal Article] Formation of nanoscaled precipitates and their effects on the high-temperature shape-memory characteristics of a Ti50Ni15Pd25Cu10 alloy2012

    • Author(s)
      M.I.Khan, H.Y.Kim, T.H.Nam, S.Miyazaki
    • Journal Title

      Acta Materialia

      Volume: 60 Issue: 16 Pages: 5900-5913

    • DOI

      10.1016/j.actamat.2012.07.032

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Stability of Ti-Ta Base High Temperature Shape Memory Alloys2012

    • Author(s)
      H.Y.Kim, T.Kanaya, T.Fukushima, P.J.S. Buenconsejo, S.Miyazaki
    • Journal Title

      Materials Science Forum

      Volume: 706-709 Pages: 1921-1924

    • DOI

      10.4028/www.scientific.net/msf.706-709.1921

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Omega Phase on Shape Memory Properties of Ti-base Alloys2012

    • Author(s)
      H.Y.Kim, Y.Al-Zain, T.Inamura, H.Hosoda, S.Miyazaki
    • Journal Title

      Proc. of 12th World Conference on Titanium

      Volume: - Pages: 680-682

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Room temperature aging behavior of Ti-Nb-Mo-based superelastic alloys2012

    • Author(s)
      Y.Al-Zain,H.Y.Kim, T.Koyano, H.Hosoda, T.H.Nam, S.Miyazaki
    • Journal Title

      Acta Materialia

      Volume: 59 Pages: 1464-1473

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Lattice modulation and superelasticity in oxygen-added beta-Ti alloys2011

    • Author(s)
      M.Tahara, H.Y.Kim, T.Inamura, H.Hosoda, S.Miyazaki
    • Journal Title

      Acta Materialia

      Volume: 59 Pages: 6208-6218

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Role of interstitial atoms in the microstructure and non-linear elastic deformation behavior of Ti-Nb alloy2011

    • Author(s)
      M.Tahara, H.Y.Kim, T.Inamura, H.Hosoda, S.Miyazaki
    • Journal Title

      Journal of Alloys and Compounds

      Volume: (印刷中) Pages: S404-S407

    • DOI

      10.1016/j.jallcom.2011.12.113

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] Ti-Zr-Nb 合金の超弾性特性に及ぼすω相の影響2014

    • Author(s)
      中井 啓介, 金 熙榮, 細田 秀樹, 宮崎 修一
    • Place of Presentation
      東京工業大学
    • Year and Date
      2014-03-23
    • Related Report
      2013 Final Research Report
  • [Presentation] 形状記憶合金の基礎研究と材料開発2014

    • Author(s)
      宮崎修一
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2014-03-21
    • Related Report
      2013 Final Research Report
  • [Presentation] 生体用チタン基形状記憶・超弾性合金の開発2012

    • Author(s)
      宮崎修一
    • Organizer
      日本金属学会2012年秋期大会
    • Place of Presentation
      愛媛大学
    • Year and Date
      2012-09-19
    • Related Report
      2013 Final Research Report
  • [Presentation] Ti-18Zr-Nb 合金の超弾性特性に及ぼすSn 添加の影響2012

    • Author(s)
      伏 傑, 金 熙榮, 細田 秀樹, 宮崎 修一
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2013 Final Research Report
  • [Presentation] Effect of Sn Addition on the Superelastic Properties of Ti-15Nb-3Mo Alloy2012

    • Author(s)
      M.F. Ijaz, H.Y. Kim, H. Hosoda, S. Miyazaki
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2013 Final Research Report
  • [Presentation] Ti-18Zr-Nb合金の超弾性特性に及ぼすSn添加の影響2012

    • Author(s)
      伏傑、金煕榮、細田秀樹、宮崎修一
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] Sn添加によるTi-Zr-Nb合金の再結晶集合組織制御2012

    • Author(s)
      片伯部信之、田原正樹、金煕榮、細田秀樹、宮崎修一
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] Effect of Sn Addition on the Superelastic Properties of Ti-15Nb-3Mo Alloy2012

    • Author(s)
      M.F.Ijaz. H.Y.Kim, H.Hosoda, S.Miyazaki
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2012-03-29
    • Related Report
      2011 Annual Research Report
  • [Presentation] Ti-Zr-Nb合金の超弾性特性・集合組織形成に及ぼすAl添加の影響2011

    • Author(s)
      中井啓介、金煕榮、細田秀樹、宮崎修一
    • Organizer
      日本金属学会2011年秋期大会
    • Place of Presentation
      沖縄コンベンションセンター
    • Year and Date
      2011-11-09
    • Related Report
      2011 Annual Research Report
  • [Presentation] Superelastic properties of (Ti-50Zr)-Mo-Sn alloys

    • Author(s)
      Muhammad Farzik Ijaz,、金 熙榮、細田 秀樹、宮崎 修一
    • Organizer
      日本金属学会2013年秋期講演大会
    • Place of Presentation
      金沢大学(金沢市)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] (Ti-Zr)-Nb合金の再結晶集合組織に及ぼすNb濃度の影響

    • Author(s)
      植松 健斗、金 熙榮、細田 秀樹、宮崎 修一
    • Organizer
      日本金属学会2013年秋期講演大会
    • Place of Presentation
      金沢大学(金沢市)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Ti-Zr-Nb合金の超弾性特性に及ぼすω相の影響

    • Author(s)
      中井 啓介、金 熙榮、細田 秀樹、宮崎 修一
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京工業大学(東京都)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 形状記憶合金の基礎研究と材料開発

    • Author(s)
      宮崎 修一
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京工業大学(東京都)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 生体用チタン基形状記憶・超弾性合金の開発

    • Author(s)
      宮崎修一
    • Organizer
      日本金属学会2012年秋期大会
    • Place of Presentation
      愛媛大学(松山市)
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Ti-Nb系合金のナノ組織化および集合組織

    • Author(s)
      金 熙榮、戸部 裕史、宮崎 修一
    • Organizer
      日本金属学会2012年秋期大会
    • Place of Presentation
      愛媛大学(松山市)
    • Related Report
      2012 Annual Research Report
  • [Presentation] Ti-Zr基合金の圧延集合組織に及ぼすNb濃度の影響

    • Author(s)
      植松 健斗, 金 熙榮, 細田 秀樹, 宮崎 修一
    • Organizer
      日本金属学会2013年春期大会
    • Place of Presentation
      東京理科大(東京都)
    • Related Report
      2012 Annual Research Report
  • [Remarks]

    • URL

      http://sma.ims.tsukuba.ac.jp/index.html

    • Related Report
      2013 Final Research Report
  • [Patent(Industrial Property Rights)] 生体用超弾性ジルコニウム合金, 歯列矯正用ワイヤ, 医療用ステントおよび眼鏡2011

    • Inventor(s)
      宮崎 修一, 金 熙榮, 佐藤 陽祐
    • Industrial Property Rights Holder
      筑波大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2011-192977
    • Filing Date
      2011-09-05
    • Related Report
      2013 Final Research Report
  • [Patent(Industrial Property Rights)] 生体用超弾性ジルコニウム合金、歯列矯正用ワイヤ、医療用ステントおよび眼鏡2011

    • Inventor(s)
      宮崎修一、金煕榮、佐藤陽祐
    • Industrial Property Rights Holder
      筑波大学
    • Industrial Property Number
      2011-192977
    • Filing Date
      2011-09-05
    • Related Report
      2011 Annual Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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