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Development of platinum-free catalyst for fuel cells using heteroatoms

Research Project

Project/Area Number 23550057
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Organic chemistry
Research InstitutionOsaka Prefecture University

Principal Investigator

NOMOTO Akihiro  大阪府立大学, 工学(系)研究科(研究院), 講師 (60405347)

Project Period (FY) 2011 – 2013
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2013: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2012: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2011: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywords有機元素化学 / 燃料電池 / 非白金元素 / バナジウム / 錯体触媒
Research Abstract

For extensive use of fuel cells, development of efficient catalysts is indispensable. Platinum is an important catalyst in fuel cells because of its high stability and its high catalytic activity for oxygen reduction reaction (ORR). However Pt is rare in the natural resources and thereby expensive, and thus, replacement of platinum catalyst is strongly desired. In this study, vanadium is attracting much attention for ORR catalyst, and catalytic reactivities were investigated by the oxidation of fuel. As results, synthesized vanadium complexes acted as catalyst by using alcohols.

Report

(4 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Research-status Report
  • 2011 Research-status Report
  • Research Products

    (57 results)

All 2014 2013 2012 2011 Other

All Journal Article (21 results) (of which Peer Reviewed: 21 results) Presentation (28 results) (of which Invited: 5 results) Book (2 results) Remarks (6 results)

  • [Journal Article] Synthesis of Selenium Compounds by Free Radical Addition Based on Visible-Light-Activated Se-Se- Bond Cleavage2013

    • Author(s)
      A. Nomoto, Y. Higuchi, Y. Kobiki, A. Ogawa
    • Journal Title

      Mini-Rev. Med. Chem

      Volume: 13(6) Pages: 178-190

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Highly Regioselective Palladium-Catalyzed Double Hydroselenation of Terminal Alkynes with Benzeneselenol in the Presence of Acetic Acid2013

    • Author(s)
      T. Ikeda, T. Tamai, M. Daitou, Y. Minamida, T. Mitamura, H. Kusano, A. Nomoto and A. Ogawa
    • Journal Title

      Chemistry Letters

      Volume: 42 Issue: 11 Pages: 1383-1385

    • DOI

      10.1246/cl.130641

    • NAID

      130004426808

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] An Efficient and Highly Selective Carbonylative Bisthiolation of Internal Alkynes with Organic Disulfides Catalyzed by [Co2(CO)8]2013

    • Author(s)
      Y. Higuchi, S. Higashimae, T. Tamai, A. Nomoto, M. Sonoda and A. Ogawa
    • Journal Title

      Chemistry Letters

      Volume: 42 Issue: 10 Pages: 1303-1304

    • DOI

      10.1246/cl.130441

    • NAID

      10031201346

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Highly Selective Perfluoroalkylation of Unsaturated Molecules upon Photoirradiation in BTF as an Organic/Fluorous Hybrid Solvent2013

    • Author(s)
      Y. Higuchi, S. Higashimae, T. Tamai, A. Nomoto, M. Sonoda and A. Ogawa
    • Journal Title

      Journal of Applied Solution Chemistry and Modeling

      Volume: 2 Issue: 3 Pages: 178-190

    • DOI

      10.6000/1929-5030.2013.02.03.3

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of Selenium Compounds by Free Radical Addition Based on Visible-Light-Activated Se-Se Bond Cleavage2013

    • Author(s)
      A. Nomoto, H. Yoshihiro, Y. Kobiki, Y. Kobiki and A. Ogawa
    • Journal Title

      Mini-Reviews in Medicinal Chemistry

      Volume: 13 Pages: 814-823

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Highly selective introduction of heteroatom groups to isocyanides and its application to electrocyclic reactions2013

    • Author(s)
      Ogawa, Akiya; Tamai, Taichi; Mitamura, Takenori; Nomoto, Akihiro
    • Journal Title

      Pure and Applied Chemistry

      Volume: 85 Issue: 4 Pages: 785-799

    • DOI

      10.1351/pac-con-12-07-01

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Novel reducing properties of a series of lanthanoid metals in the presence of SmI22013

    • Author(s)
      Tomisaka, Yuri; Yoshimura, Aya; Nomoto, Akihiro; Sonoda, Motohiro; Ogawa, Akiya
    • Journal Title

      Research on Chemical Intermediates

      Volume: 39 Issue: 1 Pages: 43-48

    • DOI

      10.1007/s11164-012-0630-x

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Synthesis and Properties of Perfluoroalkyl Phosphine Ligands: Photoinduced Reaction of Diphosphines with Perfluoroalkyl Iodides2013

    • Author(s)
      Kawaguchi, Shin-ichi; Minamida, Yoshiaki; Ohe, Takashi; Nomoto, Akihiro; Sonoda, Motohiro; Ogawa, Akiya
    • Journal Title

      Angewandte Chemie, International Edition

      Volume: 52 Issue: 6 Pages: 1748-1752

    • DOI

      10.1002/anie.201207383

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Synthesis of selenium compounds by free radical addition based on visible-light-activated se-se bond cleavage2013

    • Author(s)
      Nomoto Akihiro; Higuchi Yoshihiro; Kobiki Yohsuke; Ogawa Akiya
    • Journal Title

      Mini reviews in medicinal chemistry

      Volume: 13 Pages: 814-823

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Highly selective perfluoro -alkylchalcogenation of alkynes by the combination of iodoperfluoroalkanes and organic dichalcogenides upon photo-irradiation2012

    • Author(s)
      T. Tamai, A. Nomoto, K. Tsuchii, Y. Minamida, T. Mitamura, M. Sonoda, A. Ogawa
    • Journal Title

      Tetrahedron

      Volume: 68(51) Pages: 10516-10522

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Highly selective perfluoroalkylchalcogenation of alkynes by the combination of iodoperfluoroalkanes and organic dichalcogenides upon photoirradiation2012

    • Author(s)
      Tamai, Taichi; Nomoto, Akihiro; Tsuchii, Kaname; Minamida, Yoshiaki; Mitamura, Takenori; Sonoda, Motohiro; Ogawa, Akiya
    • Journal Title

      Tetrahedron

      Volume: 68 Issue: 51 Pages: 10516-10522

    • DOI

      10.1016/j.tet.2012.09.026

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Novel Heterotetranuclear V2Mo2 or V2W2 Complexes with 4, 4'-Di-tert-butyl -2, 2'-bipyridine : Syntheses, Crystal Structures, and Catalytic Activities2011

    • Author(s)
      S. Kodama, A. Nomoto, S. Yano, M. Ueshima, A. Ogawa
    • Journal Title

      Inorg. Chem

      Volume: 50(20) Pages: 9942-9947

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Vanadium-catalyzed atmospheric oxidation of benzyl alcohols using water as solvent2011

    • Author(s)
      A. Nomoto, S. Yano, M. Ueshima, A. Ogawa, S. Kodama, S. Hashidate
    • Journal Title

      Chem. Lett

      Volume: 40(5) Pages: 495-497

    • NAID

      10028242808

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Crystal structures of β-chalcogeno-α, β-saturated chalcogenoesthers synthesized by regioand stereoselective addition and carbonylation reactions of terminal alkynes catalyzed by Pd(PPh_3)_42011

    • Author(s)
      T. Ozaki, A. Nomoto, A. Ogawa
    • Journal Title

      Hetreoatom. Chem. (Special Issue)

      Volume: 22(3-4) Pages: 579-585

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Cobalt-Catalyzed Thiolative Lactonization of Alkynes with Double CO Incorporation2011

    • Author(s)
      Higuchi Yoshihiro
    • Journal Title

      Organometallics

      Volume: 30 Issue: 17 Pages: 4539-4543

    • DOI

      10.1021/om200248f

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Crystal structures of β-chalcogeno-α, β-unsaturated chalcogenoesters: Novel intramolecular interaction between the carbonyl oxygen and the chalcogen atom at the β-position2011

    • Author(s)
      Ozaki Toshiya
    • Journal Title

      Heteroatom Chemistry

      Volume: 22 Issue: 3-4 Pages: 579-585

    • DOI

      10.1002/hc.20690

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Highly regioselective double hydrothiolation of terminal acetylenes with thiols catalyzed by palladium diacetate2011

    • Author(s)
      Mitamura Takenori
    • Journal Title

      Bulletin of the Chemical Society of Japan

      Volume: 84 Issue: 4 Pages: 413-415

    • DOI

      10.1246/bcsj.20100311

    • NAID

      10028046952

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Novel Heterotetranuclear V2Mo2 or V2W2 Complexes with 4,4'-Di-tert-butyl-2,2'-bipyridine: Syntheses, Crystal Structures, and Catalytic Activities2011

    • Author(s)
      Kodama Shintaro
    • Journal Title

      Inorganic Chemistry

      Volume: 50 Issue: 20 Pages: 9942-9947

    • DOI

      10.1021/ic2009094

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Photochemical intramolecular cyclization of o-alkynylaryl isocyanides with organic dichalcogenides leading to 2,4-bischalcogenated quinolines2011

    • Author(s)
      Mitamura Takenori
    • Journal Title

      Organic & Biomolecular Chemistry

      Volume: 9 Issue: 10 Pages: 3768-3775

    • DOI

      10.1039/c0ob01168a

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Rhodium-Catalyzed Highly Stereoselective Hydroselenation of Internal Alkynes Bearing an Electron-withdrawing Group2011

    • Author(s)
      S.Kawaguchi, A.Ogawa, 他4名
    • Journal Title

      Organometallics

      Volume: 30 Issue: 24 Pages: 6766-6769

    • DOI

      10.1021/om200663k

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Journal Article] Vanadium-catalyzed atmospheric oxidation of benzyl alcohols using water as solvent2011

    • Author(s)
      Kodama Shintaro
    • Journal Title

      Chemistry Letters

      Volume: 40 Issue: 5 Pages: 495-497

    • DOI

      10.1246/cl.2011.495

    • NAID

      130004426216

    • Related Report
      2011 Research-status Report
    • Peer Reviewed
  • [Presentation] 銅塩を触媒とする水溶媒中でのベンジルアミン誘導体の過酸化水素酸化反応2014

    • Author(s)
      圎井邦昌, 東浦祐樹, 野元昭宏, 植嶌陸男, 小川昭弥
    • Organizer
      日本化学会第94春季年会
    • Place of Presentation
      名古屋
    • Related Report
      2013 Final Research Report
  • [Presentation] 銅塩を触媒とする水溶媒中でのベンジルアミン誘導体の過酸化水素酸化反応2014

    • Author(s)
      圓井 邦昌・東浦 祐樹・野元 昭宏・植嶌 陸男・小川 昭弥
    • Organizer
      日本化学会第94春季年会
    • Place of Presentation
      名古屋大学(愛知県名古屋市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] ヘテロ元素を有する共役系化合物の合成と錯体化学への応用2013

    • Author(s)
      野元昭宏
    • Organizer
      ヘテロ原子部会第2回懇話会
    • Place of Presentation
      神戸
    • Year and Date
      2013-10-13
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Development of Vanadium Complex Catalysts for Environmentally Benign Oxidation2013

    • Author(s)
      A. Nomoto
    • Organizer
      20-th International The Society of Pure and Applied Coordination Chemistry Symposium (SPACC-20)
    • Place of Presentation
      Changchun, China
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] ベンジルアルコール誘導体のグリーン酸化反応 : バナジウム錯体触媒による水溶媒中での常圧空気酸化法の開発2013

    • Author(s)
      圎井邦昌, 東浦祐樹, 野元昭宏, 植嶌陸男, 矢野重信, 小川昭弥
    • Organizer
      錯体化学会第63回討論会
    • Place of Presentation
      沖縄
    • Related Report
      2013 Final Research Report
  • [Presentation] Development of Vanadium Complex Catalysts for Environmentally Benign Oxidation2013

    • Author(s)
      A. Nomoto
    • Organizer
      20-th International The Society of Pure and Applied Coordination Chemistry Symposium (SPACC-20)
    • Place of Presentation
      Changchun University of Science and Technology (Changchun, China)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Synthesis and Characterization of New Sulpher Rich Platinum Arylalkenylacetylide Complex2013

    • Author(s)
      M. M. Rahman, A. Nomoto, and A. Ogawa
    • Organizer
      10th-International Symposia on Advancing the Chemical Sciences (ISACS10)
    • Place of Presentation
      京都大学(京都府京都市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Synthesis of Hydrophilic Polymer-Supported Lanthanide Nanoparticles2013

    • Author(s)
      A. Nomoto, A. Kido, K. Kakiuchi, M. Ueshima, and A, Ogawa
    • Organizer
      20-th International The Society of Pure and Applied Coordination Chemistry Symposium (SPACC-20)
    • Place of Presentation
      Changchun University of Science and Technology (Changchun, China)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Stereo- and Regioselective Introduction of Phenylchalcogeno Moieties into Ethynylferrocene2013

    • Author(s)
      A. Nomoto, T. Fujiyama, N. Nakaga, and A, Ogawa
    • Organizer
      20-th International The Society of Pure and Applied Coordination Chemistry Symposium (SPACC-20)
    • Place of Presentation
      Changchun University of Science and Technology (Changchun, China)
    • Related Report
      2013 Annual Research Report
  • [Presentation] ベンジルアルコール誘導体のグリーン酸化反応:バナジウム錯体触媒による水溶媒中での常圧空気酸化法の開発2013

    • Author(s)
      圎井邦昌, 東浦祐樹, 野元昭宏, 植嶌陸男, 矢野 重信, 小川昭弥
    • Organizer
      錯体化学会第63回討論会
    • Place of Presentation
      琉球大学(沖縄県)
    • Related Report
      2013 Annual Research Report
  • [Presentation] バナジウム触媒を用いた水溶媒中でのアルコール類のグリーンな酸素酸化反応2013

    • Author(s)
      東前信也・樋口嘉博・玉井太一・野元昭宏・園田素啓・小川昭弥
    • Organizer
      日本化学会第93春季年会
    • Place of Presentation
      滋賀
    • Related Report
      2012 Research-status Report
  • [Presentation] Crystal Structure of・-Unsaturated Chalcogenoethers and Interactions between the O-Ch Atoms2012

    • Author(s)
      A. Nomoto, T. Ozaki, S. Hayashi, W. Nakanishi, A. Ogawa
    • Organizer
      The 10th International Conference on Heteroatom Chemistry (ICHAC-10)
    • Place of Presentation
      Kyoto, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] Synthesis and X-ray Crystal Analysis of Heterotetranuclear V_2Mo_3 or V_2W_2 Complexes2012

    • Author(s)
      A. Nomoto, S. Kodama, S. Yano, M. Ueshima, A. Ogawa
    • Organizer
      19th International SPACC Symposium
    • Place of Presentation
      Sapporo, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] Synthesis and X-ray Crystal Analysis of Heterotetranuclear V2Mo2 or V2W2 Complexes2012

    • Author(s)
      Nomoto, Akihiro; Kodama, Shintaro; Yano, Shigenobu; Ueshima, Michio; Ogawa, Akiya
    • Organizer
      Proc. of 19th International the Society of Pure and Applied Coordination Chemistry Symposium
    • Place of Presentation
      札幌
    • Related Report
      2012 Research-status Report
  • [Presentation] Application of LnI2/Ln Reduction Systems to Si-Si Bond Formation2012

    • Author(s)
      Yoshimura, Aya; Li, Zhifang ; Nomoto, Akihiro; Ogawa, Akiya
    • Organizer
      Proc. of 19th International the Society of Pure and Applied Coordination Chemistry Symposium
    • Place of Presentation
      札幌
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] 15. Crystal Structure of b-Chalcogeno-a,b-Unsaturated Chalcogenoesthers and Interactions between the O-Ch Atoms2012

    • Author(s)
      Nomoto, Akihiro; Ozaki, Toshiya; Hayashi, Satoko; Nakanishi, Waro; Ogawa, Akiya
    • Organizer
      Proc. of 10th International Conference on Heteroatom Chemistry
    • Place of Presentation
      京都
    • Related Report
      2012 Research-status Report
  • [Presentation] 含カルコゲンアミノ酸を導入したアントラキノン誘導体の配位挙動2012

    • Author(s)
      野元昭宏
    • Organizer
      日本化学会第92回春季年会
    • Place of Presentation
      慶応大学(神奈川県)
    • Related Report
      2011 Research-status Report
  • [Presentation] 異種金属四核錯体を触媒とする水溶媒中での酸化反応の開発2012

    • Author(s)
      圓井邦昌
    • Organizer
      日本化学会第92回春季年会
    • Place of Presentation
      慶応大学(神奈川県)
    • Related Report
      2011 Research-status Report
  • [Presentation] 水溶媒におけるアルコール酸化のためのバナジウム錯体触媒の合成と分子構造2011

    • Author(s)
      野元昭宏, 小玉晋太朗, 白井正充, 小川昭弥
    • Organizer
      第62回有機合成化学協会関東支部シンポジウム
    • Place of Presentation
      新潟
    • Year and Date
      2011-11-26
    • Related Report
      2013 Final Research Report
  • [Presentation] Oxidation of Benzyl Alcohols Using Vanadium Catalysts in Water under the Atmosphere of Oxygen2011

    • Author(s)
      K. Marui, S. Kodama, S. Hashidate, A. Nomoto, S. Yano, M. Ueshima, A. Ogawa
    • Organizer
      5th Pacific Symposium on Radical Chemistry (PSRC-5)
    • Place of Presentation
      Shirahama, Japan
    • Related Report
      2013 Final Research Report
  • [Presentation] Photoinduced Reductive Carboxylation of Alkyl Halides with Carbon Dioxide2011

    • Author(s)
      Akihiro Nomoto
    • Organizer
      5th Pacific Symposium on Radical Chemistry
    • Place of Presentation
      シーモア(和歌山県)
    • Related Report
      2011 Research-status Report
  • [Presentation] アントラキノン誘導体への含硫黄および含セレンアミノ酸の導入とその錯形成挙動2011

    • Author(s)
      常田義真
    • Organizer
      錯体化学会第61回討論会
    • Place of Presentation
      岡山理科大学(岡山県)
    • Related Report
      2011 Research-status Report
  • [Presentation] ヨウ化サマリウムと二酸化炭素の光励起還元的カルボキシル化反応による複素環化合物の合成2011

    • Author(s)
      野元昭宏
    • Organizer
      第41回複素環化学討論会
    • Place of Presentation
      熊本市民会館(熊本県)
    • Related Report
      2011 Research-status Report
  • [Presentation] 水溶媒におけるアルコール酸化のためのバナジウム錯体触媒の合成と分子構造2011

    • Author(s)
      野元昭宏
    • Organizer
      第62回有機合成化学協会関東支部シンポジウム
    • Place of Presentation
      新潟大学工学部(新潟県)
    • Related Report
      2011 Research-status Report
  • [Presentation] Liquid-phase Synthesis of Lanthanide Nanoparticles Supported by Hydrophilic Polymer2011

    • Author(s)
      Akihiro Nomoto
    • Organizer
      International Symposium on Catalysis and Fine Chemicals 2011
    • Place of Presentation
      奈良新公会堂(奈良県)
    • Related Report
      2011 Research-status Report
  • [Presentation] β-カルコゲノ-α,β-不飽和カルコゲノエステルの位置および立体選択的な合成と結晶構造2011

    • Author(s)
      野元昭宏
    • Organizer
      第38回有機典型元素化学討論会
    • Place of Presentation
      石川県立音楽堂(石川県)
    • Related Report
      2011 Research-status Report
  • [Presentation] ヘテロ元素を有する共役系化合物の合成と錯体化学への応用

    • Author(s)
      野元昭宏
    • Organizer
      ヘテロ原子部会第2回懇話会
    • Place of Presentation
      アスビオファーマ(株)(兵庫県神戸市)
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] ヨウ化アルキルおよびヨウ化サマリウムを用いた光照射CO2固定化反応の開発

    • Author(s)
      野元昭宏・藤山卓也・小川昭弥
    • Organizer
      第15回ヨウ素学会シンポジウム
    • Place of Presentation
      千葉
    • Related Report
      2012 Research-status Report
  • [Book] "Preparative Uses of Organoselenium and Organotellurium Compounds", In Organic Selenium and Tellurium Compounds2012

    • Author(s)
      A. Nomoto, A. Ogawa
    • Publisher
      Ed by Z. Rappoport, Wiley-VCH
    • Related Report
      2013 Final Research Report
  • [Book] Organic Selenium and Tellurium Compounds2011

    • Author(s)
      Akihiro Nomoto
    • Publisher
      Wiley
    • Related Report
      2011 Research-status Report
  • [Remarks]

    • URL

      http://jstshingi.jp/abst/2007/osakfu1025/program.html#609

    • Related Report
      2013 Final Research Report
  • [Remarks]

    • URL

      http://www.chem.osakafu-u.ac.jp/ohka/ohka8/index.html

    • Related Report
      2013 Final Research Report
  • [Remarks] 大阪府立大学工学研究科物質・化学系専攻小川研究室

    • URL

      http://www.chem.osakafu-u.ac.jp/ohka/ohka8/index.html

    • Related Report
      2013 Annual Research Report
  • [Remarks]

    • URL

      http://jstshingi.jp/osakafu/program.html,

    • Related Report
      2011 Research-status Report
  • [Remarks]

    • URL

      http://deainoba.jp/meeting/081119/list.html,

    • Related Report
      2011 Research-status Report
  • [Remarks]

    • URL

      http://www.kansai.meti.go.jp/2giki/kansai-seeds/seedsfils/seedsfiles2009/opu/opu026nomoto-opu.pdf

    • Related Report
      2011 Research-status Report

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Published: 2011-08-05   Modified: 2019-07-29  

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