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In-situ observation of electrochemical deposited thin films by diffraction method

Research Project

Project/Area Number 23656080
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Research InstitutionYokohama National University

Principal Investigator

AKINIWA Yoshiaki  横浜国立大学, 大学院・工学研究院, 教授 (00212431)

Co-Investigator(Renkei-kenkyūsha) SHOBU Takahisa  独立行政法人日本原子力研究開発機構, 量子ビーム応用研究部門, 研究員 (90425562)
Project Period (FY) 2011 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2012: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2011: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords薄膜 / 残留応力 / 結晶配向 / X線 / 電子線後方散乱 / 放射光 / 電着薄膜 / その場測定
Research Abstract

The formation mechanism of the electrochemical deposited thin films was examined by observing the change of the crystalline orientation and residual stress during deposition by the X-ray method and the electron backscatter diffraction method. For the copper thin films deposited by both the direct current method and the pulse method, there were few changes of the crystalline orientation during deposition. On the other hand, the residual stress varied from tensile to compression. It was suggested that the formation mechanism of copper thin films was except the Volmer-Weber type.

Report

(3 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Research-status Report
  • Research Products

    (13 results)

All 2013 2012 2011

All Presentation (13 results)

  • [Presentation] X線回折法による金属材料の非破壊応力評価2013

    • Author(s)
      秋庭義明
    • Organizer
      日本鉄鋼協会,非線形現象を利用した非破壊的損傷評価シンポジウム
    • Place of Presentation
      東京
    • Year and Date
      2013-03-28
    • Related Report
      2012 Final Research Report
  • [Presentation] X線回折法による金属材料の非破壊応力評価2013

    • Author(s)
      秋庭義明
    • Organizer
      日本鉄鋼協会,非線形現象を利用した非破壊的損傷評価シンポジウム
    • Place of Presentation
      東京
    • Related Report
      2012 Annual Research Report
  • [Presentation] 二次元検出器走査システムを利用した応力測定法開発2012

    • Author(s)
      張朔源,城鮎美,菖蒲敬久
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 電着ニッケル薄膜のX線回折法による粒径と転位密度の評価2012

    • Author(s)
      田中浩人,田中啓介,來海博央,鈴木賢治,菖蒲敬久
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] オーステナイト系ステンレス鋼のWJPによる残留応力2012

    • Author(s)
      鈴木賢治,菖蒲敬久,城鮎美
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 浸炭焼入したクロムモリブデン鋼の残留応力と硬化層の評価2012

    • Author(s)
      坂井田喜久,山下翔平,矢代茂樹,菖蒲敬久
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] フロントエンド機器用母材無酸素銅の残留ひずみ2012

    • Author(s)
      佐野睦,高橋直,渡辺篤雄,北村英男,城鮎美,菖蒲敬久
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 高エネルギ放射光X線回折法によるNi基超合金の材料評価2012

    • Author(s)
      菖蒲敬久,近藤義宏,三浦信祐,村田純教,石山新太郎
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 放射光白色X線によるアルミ単結晶延性損傷進展挙動の検証2012

    • Author(s)
      柴野純一,木曽稔,梶原堅太郎,菖蒲敬久,三浦節男,小林道明
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] 金属ガラスの引張変形下での高エネルギー放射光ひずみ解析2012

    • Author(s)
      清水健太,松田卓弥,菊地拓哉,今福宗行,才田淳,菖蒲敬久,大谷眞一
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] アルミニウム単結晶における残留応力と再結晶挙動に関する研究2012

    • Author(s)
      城鮎美,岡田達也,菖蒲敬久,河野智也,文屋宏友
    • Organizer
      日本材料学会,第46回X線材料強度に関するシンポジウム
    • Place of Presentation
      京都
    • Year and Date
      2012-07-06
    • Related Report
      2012 Final Research Report
  • [Presentation] X-Ray Measurement of Residual Stress Distribution in Sputtered Cu Thin Films2011

    • Author(s)
      Y. Akiniwa, T. Sakaue
    • Organizer
      Thermec 2011
    • Place of Presentation
      Quebec, Canada
    • Year and Date
      2011-08-04
    • Related Report
      2012 Final Research Report
  • [Presentation] X-Ray Measurement of Residual Stress Distribution in Sputtered Cu Thin Films2011

    • Author(s)
      Y. Akiniwa, T. Sakaue
    • Organizer
      Thermec 2011(招待講演)
    • Place of Presentation
      Quebec, Canada
    • Related Report
      2011 Research-status Report

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Published: 2011-08-05   Modified: 2019-07-29  

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