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Creation of super hard coatings with excellent oxidation resistance made from ubiquitous elements

Research Project

Project/Area Number 23656456
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Material processing/treatments
Research InstitutionUniversity of Toyama

Principal Investigator

NOSE Masateru  富山大学, 芸術文化学部, 教授 (70269570)

Co-Investigator(Renkei-kenkyūsha) MATSUDA Kenji  富山大学, 大学院・理工学研究部, 教授 (00209553)
Project Period (FY) 2011 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2012: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2011: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords薄膜プロセス / 硬質保護膜 / ナノコンポジット膜 / ユビキタス元素 / 硬質膜 / 差動排気同時成膜法 / 反応スパッタ法
Research Abstract

We prepared composite films consisting of nitride and oxide in order to obtain new protective coatings having super high hardness and excellent oxidationresistance, which were made from ubiquitous elements. The new nanocomposite coatings consisting of AlN and oxide (SiOx or AlxOy) were deposited with the differential pumping co-sputtering system. The indentation hardness of AlN and the oxide were 24GPa and 11~ 13GPa, respectively. Regardless of the lower hardness of single phase films, the AlN/SiOx or AlN/AxOy nanocomposite coatings showed an increase of ~50% in indentation hardness from that of the AlN film and achieved a maximum hardness of 34 GPa by co-deposition of oxide and nitride. The indentation hardness of some composite coatings barely changed when the coating samples were annealed at 800 ℃×1 hour in air

Report

(3 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Research-status Report
  • Research Products

    (24 results)

All 2013 2012 2011

All Presentation (24 results)

  • [Presentation] AlN/AlxOyナノ複相構造膜の微細構造と機械的性質2013

    • Author(s)
      佐藤誉将,前田晃広,松田健二,Wen-An Chiou,野瀬正照
    • Organizer
      AlN/AlxOyナノ複相構造膜の微細構造と機械的性質
    • Place of Presentation
      東京理科大学(東京都新宿区
    • Year and Date
      2013-03-28
    • Related Report
      2012 Final Research Report
  • [Presentation] AlN/AlxOyナノ複相構造膜の微細構造と機械的性質2013

    • Author(s)
      佐藤誉将、前田晃広、松田健二、Wen-An Chiou、野瀬正照
    • Organizer
      日本金属学会2013年春期大会
    • Place of Presentation
      東京理科大学(東京都新宿区)
    • Related Report
      2012 Annual Research Report
  • [Presentation] RF反応スパッタ法で作製したSiAlON薄膜の構造と機械的性質2012

    • Author(s)
      松本和晃,橋爪 隆,佐伯 淳,野瀬正照
    • Organizer
      日本金属学会・日本鉄鋼協会北信越支部連合講演会
    • Place of Presentation
      福井工業大学(福井県福井市)
    • Year and Date
      2012-12-08
    • Related Report
      2012 Final Research Report
  • [Presentation] 差動排気同時成膜法により作製した窒化物/酸化物ナノ複相構造膜の機械的特性と微細組織2012

    • Author(s)
      佐藤誉将,前田晃広,松田健二,塩尻 詢,Wen- An Chiou,野瀬正照
    • Organizer
      日本金属学会・日本鉄鋼協会北信越支部連合講演会
    • Place of Presentation
      福井工業大学(福井県福井市)
    • Year and Date
      2012-12-08
    • Related Report
      2012 Final Research Report
  • [Presentation] AlN/SiOxナノコンポジット膜の微細構造2012

    • Author(s)
      佐藤誉将, 高畠浩史,川畑常眞,松田健二,Wen-An Chiou,塩尻 詢,野瀬正照
    • Organizer
      日本金属学会2012年秋期大会
    • Place of Presentation
      愛媛大学(愛媛県松山市)
    • Year and Date
      2012-09-19
    • Related Report
      2012 Final Research Report
  • [Presentation] A Novel Technique of Fabricating Nitride/Oxide Nanocomposite Coatings - Using Differential Pumping Co-sputtering System-2012

    • Author(s)
      Masateru Nose, Wen-An Chiou, TokimasaKawabata, Yuji Hatano, Kenji Matsuda
    • Organizer
      3th International Conference on Plasma Surface Engineering (PSE2012)
    • Place of Presentation
      Garmish-Partenkirchen,Germany
    • Year and Date
      2012-09-11
    • Related Report
      2012 Final Research Report
  • [Presentation] Microstructure and properties of AlN/SiOx nanocomposite films preparedby differential pumping co-sputtering system2012

    • Author(s)
      T. Sato, H. Takabatake, T. Kawabata, K.Matsuda, W-A. Chiou, M. Shiojiri, M. Nose
    • Organizer
      Polish-Japanese Joint Seminar on Micro and Nano Analysis
    • Place of Presentation
      Sieniawa,Poland
    • Year and Date
      2012-09-11
    • Related Report
      2012 Final Research Report
  • [Presentation] TEM Study of AlN/Oxides (SiOx and AlxOy) Nanocomposite Films Prepared by Differential Pumping Co-Sputtering System2012

    • Author(s)
      Masateru Nose, Wen-An Chiou, Takamasa Satho, Hiroshi Takabatake, Tokimasa Kawabata and Kenji Matsuda
    • Organizer
      Microscopy and Microanalysis Meeting2012,Microscopy Society of America
    • Place of Presentation
      Phenix, USA
    • Year and Date
      2012-08-01
    • Related Report
      2012 Final Research Report
  • [Presentation] 差動排気型2元同時成膜装置を用いたAlN/SiOxナノコンポジット膜の作製2012

    • Author(s)
      佐藤誉将, 野瀬正照,松田健二,他3名
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学(神奈川県横浜市
    • Year and Date
      2012-03-29
    • Related Report
      2012 Final Research Report
  • [Presentation] TEM Study of AlN/Oxides (SiOx and AlxOy) Nanocomposite Films Prepared by Differential Pumping Co-Sputtering System2012

    • Author(s)
      Masateru Nose, Wen-An Chiou, Takamasa Satho, Hiroshi Takabatake, Tokimasa Kawabata and Kenji Matsuda
    • Organizer
      Microscopy and Microanalysis Meeting, Microscopy Society of America
    • Place of Presentation
      Phenix AZ, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] Microstructure and properties of AlN/SiOx nanocomposite films prepared by differential pumping co-sputtering system2012

    • Author(s)
      T. Sato, H. Takabatake, T. Kawabata, K. Matsuda, W-A. Chiou, M. Shiojiri, M. Nose
    • Organizer
      Polish-Japanese Joint Seminar on Micro and Nano Analysis
    • Place of Presentation
      Sieniawa, Poland
    • Related Report
      2012 Annual Research Report
  • [Presentation] A Novel Technique of Fabricating Nitride/Oxide Nanocomposite Coatings –Using Differential Pumping Co-sputtering System –2012

    • Author(s)
      Masateru Nose, Wen-An Chiou, Tokimasa Kawabata, Yuji Hatano, Kenji Matsuda
    • Organizer
      13th International Conference on Plasma Surface Engineering (PSE2012)
    • Place of Presentation
      Garmish-Partenkirchen, Germany
    • Related Report
      2012 Annual Research Report
  • [Presentation] AlN/SiOxナノコンポジット膜の微細構造2012

    • Author(s)
      佐藤誉将, 高畠浩史、川畑常眞、松田健二、Wen-An Chiou、塩尻 詢、野瀬正照
    • Organizer
      日本金属学会2012年秋期大会
    • Place of Presentation
      愛媛大学(愛媛県松山市)
    • Related Report
      2012 Annual Research Report
  • [Presentation] 差動排気同時製膜法により作製した窒化物/酸化物ナノ複相構造膜の機械的特性と微細組織2012

    • Author(s)
      佐藤誉将、前田晃広、松田健二、塩尻 詢、Wen-An Chiou、野瀬正照
    • Organizer
      日本金属学会・日本鉄鋼協会北信越支部連合講演会
    • Place of Presentation
      福井工業大学(福井県福井市)
    • Related Report
      2012 Annual Research Report
  • [Presentation] RF反応スパッタ法で作製したSiAlON薄膜の構造と機械的性質2012

    • Author(s)
      松本和晃、橋爪 隆、佐伯 淳、野瀬正照
    • Organizer
      日本金属学会・日本鉄鋼協会北信越支部連合講演会
    • Place of Presentation
      福井工業大学(福井県福井市)
    • Related Report
      2012 Annual Research Report
  • [Presentation] 差動排気型2元同時成膜装置を用いたAlN/SiOxナノコンポジット膜の作製2012

    • Author(s)
      佐藤誉将, 野瀬正照,松田健二,他3名
    • Organizer
      日本金属学会2012年春期大会
    • Place of Presentation
      横浜国立大学(神奈川県横浜市)
    • Related Report
      2011 Research-status Report
  • [Presentation] 差動排気型同時成膜装置を用いたAlN/酸化物ナノコンポジット膜の機械的性質2011

    • Author(s)
      佐藤誉将,松田健二,野瀬正照,他4名
    • Organizer
      日本金属学会北陸信越支部・日本鉄鋼協会北陸信越支部平成23年度 連合講演会
    • Place of Presentation
      金沢工業大学(石川県野々市市)
    • Year and Date
      2011-12-03
    • Related Report
      2012 Final Research Report
  • [Presentation] RF反応スパッタ法によるSiAlON膜の作製2011

    • Author(s)
      松本和晃,佐伯淳,橋爪隆,野瀬正照
    • Organizer
      日本金属学会北陸信越支部・日本鉄鋼協会北陸信越支部 平成23年度連合講演会
    • Place of Presentation
      金沢工業大学(石川県野々市市)
    • Year and Date
      2011-12-03
    • Related Report
      2012 Final Research Report
  • [Presentation] 差動排気型2元同時成膜装置を用いた窒化物/酸化物ナノコンポジット膜作製2011

    • Author(s)
      佐藤誉将, 野瀬正照,松田健二,他4名
    • Organizer
      日本金属学会2011年秋期大会
    • Place of Presentation
      沖縄コンベンションセンター(沖縄県宜野湾市)
    • Year and Date
      2011-11-08
    • Related Report
      2012 Final Research Report
  • [Presentation] TEM Study of Aluminium Oxynitride Films Prepared by Reactive R. F.-Sputteirng2011

    • Author(s)
      L-C. Lai, M. Nose, W-A. Chiou and A. Saiki
    • Organizer
      Microscopy and Microanalysis Meeting 2011
    • Place of Presentation
      Microscopy Society of America,Nashville,USA
    • Year and Date
      2011-08-11
    • Related Report
      2012 Final Research Report
  • [Presentation] TEM Study of Aluminium Oxynitride Films Prepared by Reactive R. F.-Sputteirng2011

    • Author(s)
      L-C. Lai, M. Nose, W-A. Chiou and A. Saiki
    • Organizer
      Microscopy and Microanalysis 2011
    • Place of Presentation
      Nashville 国際会議場 (USA)
    • Related Report
      2011 Research-status Report
  • [Presentation] 差動排気型2元同時成膜装置を用いた窒化物/酸化物ナノコンポジット膜作製2011

    • Author(s)
      佐藤誉将, 野瀬正照,松田健二,他4名
    • Organizer
      日本金属学会2011年秋期大会
    • Place of Presentation
      沖縄コンベンションセンター(沖縄県宜野湾市)
    • Related Report
      2011 Research-status Report
  • [Presentation] RF反応スパッタ法によるSiAlON膜の作製2011

    • Author(s)
      松本和晃、佐伯淳、橋爪隆、野瀬正照
    • Organizer
      日本金属学会北陸信越支部・日本鉄鋼協会北陸信越支部 平成23年度 連合講演会
    • Place of Presentation
      金沢工業大学(石川県野々市市)
    • Related Report
      2011 Research-status Report
  • [Presentation] 差動排気型同時成膜装置を用いたAlN/酸化物ナノコンポジット膜の機械的性質2011

    • Author(s)
      佐藤誉将、松田健二、野瀬正照、他4名
    • Organizer
      日本金属学会北陸信越支部・日本鉄鋼協会北陸信越支部 平成23年度 連合講演会
    • Place of Presentation
      金沢工業大学(石川県野々市市)
    • Related Report
      2011 Research-status Report

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Published: 2011-08-05   Modified: 2019-07-29  

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