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Development of microdevices for exact evaluation of nucleation and growth processes to produce high-quality metal oxide nanoparticles

Research Project

Project/Area Number 23686113
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypeSingle-year Grants
Research Field Reaction engineering/Process system
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

Sue Kiwamu  国立研究開発法人産業技術総合研究所, 化学プロセス研究部門, 主任研究員 (60333845)

Research Collaborator AOKI Mitsuko  
ONO Takeshi  
SATO Takafumi  
HAMANE Daisuke  
KAWASAKI Shin-ichiro  
HAKUTA Yukiya  
TAKASHIMA Hiroshi  
OHARA Motohiro  
TAKEBAYASHI Yoshihiro  
YODA Satoshi  
FURUYA Takeshi  
SATO Toshiyuki  
HIAKI Toshihiko  
HATAKEDA Kiyotaka  
KÖLBL Andreas  
KRAUT Manfred  
DITTMEYER Roland  
Project Period (FY) 2011-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥27,430,000 (Direct Cost: ¥21,100,000、Indirect Cost: ¥6,330,000)
Fiscal Year 2014: ¥5,330,000 (Direct Cost: ¥4,100,000、Indirect Cost: ¥1,230,000)
Fiscal Year 2013: ¥5,980,000 (Direct Cost: ¥4,600,000、Indirect Cost: ¥1,380,000)
Fiscal Year 2012: ¥7,020,000 (Direct Cost: ¥5,400,000、Indirect Cost: ¥1,620,000)
Fiscal Year 2011: ¥9,100,000 (Direct Cost: ¥7,000,000、Indirect Cost: ¥2,100,000)
Keywordsマイクロミキサ / マイクロ流体デバイス / 酸化物 / ナノ粒子 / 核発生 / 成長 / 連続製造 / 高温高圧水 / 高圧高温水
Outline of Final Research Achievements

Exact control of nucleation and growth processes is important for producing high-quality metal oxide nanoparticles with desirable properties (particle size, distribution, structure, composition) in the continuous hydrothermal synthesis method. We developed high-temperature and high-pressure microdevices for reducing heterogeneous nucleation in the devices and altitude control of nucleation process. We carried out nanoparticles production from both homogeneous and heterogeneous mixtures of starting materials, clarified the formation mechanisms, and examined the two-stage system for supplying starting solutions to control growth process. On the basis of the results, the design method of desirable nanoparticles was studied.

Report

(6 results)
  • 2015 Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • 2011 Annual Research Report
  • Products Report
  • Research Products

    (18 results)

All 2015 2014 2013 2012 2011 Other

All Int'l Joint Research (1 results) Journal Article (5 results) (of which Peer Reviewed: 4 results) Presentation (6 results) (of which Invited: 3 results) Patent(Industrial Property Rights) (6 results)

  • [Int'l Joint Research] Karlsruhe Institute of Technology(ドイツ)

    • Related Report
      2014 Annual Research Report
  • [Journal Article] Ultrafast hydrothermal synthesis of Pr-doped Ca0.6Sr0.4TiO3 red phosphor nanoparticles using corrosion resistant microfluidic devices with Ti-lined structure under high-temperature and high-pressure condition2014

    • Author(s)
      Kiwamu Sue, Takafumi Sato, Toshihiko Hiaki, Takeshi Ono, Motohiro Ohara, Takeshi Furuya, Yukiya Hakuta, Mitsuko Aoki
    • Journal Title

      Chemical Engineering Journal

      Volume: 239 Pages: 360-363

    • DOI

      10.1016/j.cej.2013.11.035

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Continuous hydrothermal synthesis of Ca1-xSrxTiO3 solid-solution nanoparticles using a T-type micromixer2014

    • Author(s)
      Takeshi Ono, Kiwamu Sue, Daichi Furuta, Mitsuko Aoki, Yukiya Hakuta, Yoshihiro Takebayashi, Satoshi Yoda, Takeshi Furuya, Toshiyuki Sato, Toshihiko Hiaki
    • Journal Title

      The Journal of Supercritical Fluids

      Volume: 85 Pages: 159-164

    • DOI

      10.1016/j.supflu.2013.11.010

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 高品質酸化物ナノ粒子の連続製造を目指したマイクロ流体デバイス開発2013

    • Author(s)
      陶究
    • Journal Title

      化学工学

      Volume: 77 Pages: 275-277

    • Related Report
      2012 Annual Research Report
  • [Journal Article] マイクロミキサーと高温高圧水を利用した金属酸化物ナノ粒子の連続製造法の開発2012

    • Author(s)
      陶究
    • Journal Title

      高圧力の科学と技術

      Volume: 22 Pages: 113-120

    • NAID

      10030642147

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Continuous Hydrothermal Synthesis of Nickel Ferrite Nanoparticles Using a Central Collision-Type Micromixer : Effects of Temperature, Residence Time, Metal Salt Molality, and NaOH Addition on Conversion, Particle Size, and Crystal Phase2011

    • Author(s)
      陶究
    • Journal Title

      Industrial and Engineering Chemistry Research

      Volume: 50 Issue: 16 Pages: 9625-9631

    • DOI

      10.1021/ie200036m

    • Related Report
      2011 Annual Research Report
    • Peer Reviewed
  • [Presentation] 二相旋回流構造を備えたマイクロミキサによる酸化亜鉛ナノ粒子の連続水熱合成2015

    • Author(s)
      陶 究、伯田 幸也、Andreas Koelbl Manfred Kraut、Roland Dittmeyer
    • Organizer
      化学工学会第47回秋季大会
    • Place of Presentation
      北海道大学札幌キャンパス(北海道札幌市)
    • Year and Date
      2015-09-10
    • Related Report
      2014 Annual Research Report
  • [Presentation] Nano Particle Precipitation in Micro Mixers2013

    • Author(s)
      陶究
    • Organizer
      IMVT seminar
    • Place of Presentation
      ドイツ(カールスルーエ)
    • Year and Date
      2013-05-23
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 高温高圧水とマイクロ空間を利用したナノ粒子製造プロセスの開発2011

    • Author(s)
      陶究
    • Organizer
      化学工学会ダイナミックプロセス応用分科会・平成23年度研究討論会
    • Place of Presentation
      静岡県・KKRホテル熱海(招待講演)
    • Year and Date
      2011-11-12
    • Related Report
      2011 Annual Research Report
  • [Presentation] 耐食性マイクロ流体デバイスを用いた高品質酸化物ナノ粒子の連続水熱合成

    • Author(s)
      陶究
    • Organizer
      日本セラミックス協会第25回秋季シンポジウム
    • Place of Presentation
      名古屋大学(愛知県)
    • Related Report
      2012 Annual Research Report
  • [Presentation] マイクロ流体デバイスを用いた高品質酸化物ナノ粒子のオンデマンド製造技術開発

    • Author(s)
      陶究
    • Organizer
      日本セラミックス協会第25回秋季シンポジウム
    • Place of Presentation
      名古屋大学(愛知県)
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] 高品質酸化物ナノ粒子のオンデマンド製造を目指したマイクロ流体デバイス開発

    • Author(s)
      陶究
    • Organizer
      化学工学会超臨界流体部会サマースクール
    • Place of Presentation
      クロス・ウェーブ船橋(千葉県)
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Patent(Industrial Property Rights)] 耐熱耐圧耐食性マイクロ電極2012

    • Inventor(s)
      陶究
    • Industrial Property Rights Holder
      産総研
    • Industrial Property Number
      2012-028274
    • Filing Date
      2012-02-13
    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 耐熱耐圧耐食性電気化学マイクロセル2012

    • Inventor(s)
      陶究
    • Industrial Property Rights Holder
      産総研
    • Industrial Property Number
      2012-028275
    • Filing Date
      2012-02-13
    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 耐熱耐圧耐食性温度測定用マイクロデバイス2012

    • Inventor(s)
      陶究
    • Industrial Property Rights Holder
      産総研
    • Industrial Property Number
      2012-028276
    • Filing Date
      2012-02-13
    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 耐熱耐圧耐食性電気化学マイクロセル2012

    • Inventor(s)
      陶 究, 畑田清隆
    • Industrial Property Rights Holder
      国立研究開発法人産業技術総合研究所
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2012-028275
    • Filing Date
      2012-02-13
    • Acquisition Date
      2016-02-19
    • Related Report
      Products Report
  • [Patent(Industrial Property Rights)] 耐熱耐圧耐食性マイクロ電極の製造方法2012

    • Inventor(s)
      陶 究, 畑田清隆
    • Industrial Property Rights Holder
      国立研究開発法人産業技術総合研究所
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2012-028274
    • Filing Date
      2012-02-13
    • Acquisition Date
      2016-02-19
    • Related Report
      Products Report
  • [Patent(Industrial Property Rights)] 高温高圧流体混合装置2011

    • Inventor(s)
      陶究
    • Industrial Property Rights Holder
      産総研
    • Industrial Property Number
      2011-135348
    • Filing Date
      2011-06-17
    • Related Report
      2011 Annual Research Report

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Published: 2011-04-06   Modified: 2019-07-29  

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