Development of precise electrical measurement method in TEM
| Project/Area Number |
23760626
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| Research Category |
Grant-in-Aid for Young Scientists (B)
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| Allocation Type | Multi-year Fund |
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| Research Field |
Physical properties of metals
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| Research Institution | National Institute for Materials Science |
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Principal Investigator |
KAWAMOTO Naoyuki 独立行政法人物質・材料研究機構, ナノチューブユニット, MANA研究員 (70570753)
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| Project Period (FY) |
2011-04-28 – 2015-03-31
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| Project Status |
Completed (Fiscal Year 2014)
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| Budget Amount *help |
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2013: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2012: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2011: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
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| Keywords | 透過電子顕微鏡法 / 微小電気計測 / 局所温度計測 / 熱電対 / ゼーベック効果 / ナノ電気計測 / ナノ温度計測 / 透過電子顕微鏡 / その場観察 / 帯電効果 / 微細加工 / 電気計測 / 温度計測 / ナノチューブ / 電気抵抗 |
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| Outline of Final Research Achievements |
By introducing two nanoscale probes inside a transmission electron microscope (TEM), we promoted to improve an electrical measurement method in TEM for evaluating of electrical and thermal properties. For example, to improve a space resolution and precision of an electrical resistivity measurement, we developed a new sharpened CNT probe welded to a top of W probe and a TEM specimen for supplying a constant current by using an electron lithography and a focused ion beam system (FIB). Moreover, we also developed a local temperature measurement method in TEM as a fundamental technique for thermal resistivity measurement in TEM by assembling a nanoscale thermocouple. By using the developed thermocouple, direct measurement of a temperature increase of specimen on heating by electron beam irradiation and measurement of phonon conduction in a heat radiation composite material could be successfully demonstrated.
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Report
(5 results)
Research Products
(15 results)
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[Presentation] Mechanical Properties of 1-D Materials as Revealed by In Situ Transmission Electron Microscopy and Molecular Dynamics Simulations2012
Author(s)
T. Daiming, C.-L. Ren, M. Yamaguchi, M. Wang, X. Wei, N. Kawamoto, C. Zhi, C. Liu, Y. Bando, M. Mitome, N. Fukata, D. Golberg
Organizer
10th China-Japan-Korea Joint Symposium on Carbon Materials
Place of Presentation
Guangzhou、China
Related Report
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