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Stability of nanoscale particles in Oxide-Dispersion-Strengthened (ODS) steels under extremely large and multi-directional deformation conditions

Research Project

Project/Area Number 23K13087
Research Category

Grant-in-Aid for Early-Career Scientists

Allocation TypeMulti-year Fund
Review Section Basic Section 14020:Nuclear fusion-related
Research InstitutionNational Institute for Fusion Science

Principal Investigator

申 晶潔  核融合科学研究所, 研究部, 助教 (80824747)

Project Period (FY) 2023-04-01 – 2026-03-31
Project Status Granted (Fiscal Year 2023)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2025: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2024: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2023: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
KeywordsODS steel / Microstructure / Ion irradiation / Irradiation effects / ODS ferritic steel / nanoscale particles / formation mechanisms / thermal stability / large deformation
Outline of Research at the Start

This research is to investigate formation behaviors and the stability of nanoscale oxide particles in the ODS ferritic steel after extremely large plastic deformation to reveal the formation mechanisms of oxide particles, optimize the process parameters and develop the stable oxide particles.

Outline of Annual Research Achievements

The as-fabricated oxide dispersion strengthened (ODS) ferritic steel was recrystallized after large plastic deformation and subsequent heat treatment. The microstructural evolution and hardness changes under single-beam (Fe ions) and dual-beam (Fe and He ions) irradiation up to a peak damage dose of 10.5 displacements per atom (dpa) at elevated temperatures were investigated to clarify the irradiation resistance. Results showed that size and number density of the oxide particles were slightly decreased after ion irradiation. Compared with single-beam irradiation, high density of helium bubbles was observed after dual-beam irradiation. Larger helium bubbles are trapped at the grain boundaries in the as-fabricated specimen, and the size of helium bubbles in the grains is almost the same for both as-fabricated and recrystallized specimens. Nanoindentation hardness was evidently not changed after both single-beam and dual-beam irradiation at 973 K, suggesting that helium bubbles did not significantly induce hardening at this condition.

Current Status of Research Progress
Current Status of Research Progress

3: Progress in research has been slightly delayed.

Reason

In order to make the laboratory-scale ODS steel with a designed chemical composition, adjustment of machine time, such as large glove boxes, hot isostatic pressing etc., is necessary. Also, to control the concentration of the impurities in the fabrication process, specialized parts, high-purity raw materials and atmosphere control should be considered.

Strategy for Future Research Activity

The designed ODS steels are to be made with high-purity raw materials. The coarse Ti-enriched particles are expected to be reduced or controlled by changing the Ti concentration and impurities. Moreover, the behaviors of the oxide particles and Ti-enriched particles during fabrication process will be investigated, and the formation mechanisms and thermal stability after plastic deformation will be elucidated.

Report

(1 results)
  • 2023 Research-status Report
  • Research Products

    (6 results)

All 2024 2023

All Journal Article (1 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 1 results) Presentation (5 results) (of which Int'l Joint Research: 3 results)

  • [Journal Article] Evolution of interfacial microstructure and oxides of CLAM steel by hot compression bonding2024

    • Author(s)
      Bai Yunfei、Wang Jianqiang、Zhu Gaofan、Nagasaka Takuya、Shen Jingjie、Sun Mingyue、Huang Qunying
    • Journal Title

      Materials Characterization

      Volume: 210 Pages: 113848-113848

    • DOI

      10.1016/j.matchar.2024.113848

    • Related Report
      2023 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] Effect of Defect Distribution Gradient on Nano-oxide Behavior in 12Cr-ODS Steels Irradiated with 2.8 MeV Fe2+ Ions2024

    • Author(s)
      Zideng Wang, Jingjie Shen, Huilong Yang, Sho Kano, Hiroaki Abe
    • Organizer
      2024 Spring Meeting of The Japan Institute of Metals and Materials
    • Related Report
      2023 Research-status Report
  • [Presentation] Study of ion irradiation effects on oxide dispersion strengthened (ODS) ferritic steel2023

    • Author(s)
      Jingjie Shen, Kiyohiro Yabuuchi
    • Organizer
      The 14th International Symposium of Advanced Energy Science
    • Related Report
      2023 Research-status Report
    • Int'l Joint Research
  • [Presentation] Ion irradiation effects of 12Cr ODS steel after a novel recrystallization process2023

    • Author(s)
      Jingjie Shen, Takeo Muroga, Kiyohiro Yabuuchi, Sho Kano, Hiroaki Abe
    • Organizer
      2023 Fall Meeting of Atomic Energy Society of Japan
    • Related Report
      2023 Research-status Report
  • [Presentation] Ion irradiation effects on as-fabricated and recrystallized 12Cr ODS steel at 973 K2023

    • Author(s)
      Jingjie Shen, Kiyohiro Yabuuchi, Huilong Yang, Sho Kano, Hiroaki Abe
    • Organizer
      21st International Conference on Fusion Reactor Materials (ICFRM21)
    • Related Report
      2023 Research-status Report
    • Int'l Joint Research
  • [Presentation] Effects of Oxides on the Microstructure and Properties of ODS-CLAM Steel2023

    • Author(s)
      Gaofan Zhu, Qunying Huang, Yunfei Bai, Jingjie Shen
    • Organizer
      21st International Conference on Fusion Reactor Materials (ICFRM21)
    • Related Report
      2023 Research-status Report
    • Int'l Joint Research

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Published: 2023-04-13   Modified: 2024-12-25  

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