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New challenge of grain boundary engineering for development of ferritic/martensitic heat-resistant steels with superior environmental durability

Research Project

Project/Area Number 24246125
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Metal making engineering
Research InstitutionKumamoto University

Principal Investigator

Tsurekawa Sadahiro  熊本大学, 自然科学研究科, 教授 (40227484)

Co-Investigator(Kenkyū-buntansha) WATANABE Seiichi  北海道大学, 大学院工学研究院, 教授 (60241353)
SIBAYAMA Tamaki  北海道大学, 大学院工学研究院, 教授 (10241564)
MORIZONO Yasuhiro  熊本大学, 大学院自然科学研究科, 准教授 (70274694)
Research Collaborator YAMAMURO Takateru  熊本大学, 工学部, 技術専門職員 (30747407)
Project Period (FY) 2012-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥46,150,000 (Direct Cost: ¥35,500,000、Indirect Cost: ¥10,650,000)
Fiscal Year 2015: ¥8,320,000 (Direct Cost: ¥6,400,000、Indirect Cost: ¥1,920,000)
Fiscal Year 2014: ¥6,630,000 (Direct Cost: ¥5,100,000、Indirect Cost: ¥1,530,000)
Fiscal Year 2013: ¥14,560,000 (Direct Cost: ¥11,200,000、Indirect Cost: ¥3,360,000)
Fiscal Year 2012: ¥16,640,000 (Direct Cost: ¥12,800,000、Indirect Cost: ¥3,840,000)
Keywords粒界工学 / 粒界性格分布 / フェライト系耐熱鋼 / ラスマルテンサイト / 高温クリープ / 高温水蒸気酸化 / 液体金属脆化 / マイクロピラー試験 / パルスレーザー / EBSD / 表面改質 / 溶接熱影響部 / in-situ EBSD / 高温変形 / 微細組織 / 地球温暖化ガス排出削減 / 水蒸気酸化 / 組織制御 / マルテンサイト
Outline of Final Research Achievements

Grain boundary engineering (GBE) was applied to 9-12Cr heat-resistant ferritic steels with lath-martensite for achieving enhanced environmental durability. We could observably increase the fraction of coincidence site lattice (CSL) boundaries along the prior austenitic boundaries in martensite through a new processing route with a combination of thermomechanical treatment and martensitic transformation. In addition, the GBE could introduce a high density of subblock structure in martensite, which resulted in a homogeneous distribution of fine M23C6 precipitates in tempered martensite. These GBEed ferricitc steels showed superior resistances against high temperature creep, steam oxidation and liquid metal corrosion.

Report

(5 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (97 results)

All 2016 2015 2014 2013 2012 Other

All Int'l Joint Research (3 results) Journal Article (26 results) (of which Peer Reviewed: 26 results,  Open Access: 5 results,  Acknowledgement Compliant: 3 results) Presentation (61 results) (of which Int'l Joint Research: 1 results,  Invited: 13 results) Book (2 results) Remarks (4 results) Patent(Industrial Property Rights) (1 results)

  • [Int'l Joint Research] チェコ科学アカデミー物理研究所(チェコ)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] アーヘン工科大学(ドイツ)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] ルール大学(ドイツ)

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Grain Boundary Engineering of 10% Cr Ferritic-Martensitic Steel SUH32015

    • Author(s)
      K. Hirayama, Y. Yoshii, Y. Morizono, S. Tsurekawa, Y. Hidaka
    • Journal Title

      ISIJ International

      Volume: 55 Issue: 9 Pages: 1973-1979

    • DOI

      10.2355/isijinternational.ISIJINT-2015-057

    • NAID

      130005100505

    • ISSN
      0915-1559, 1347-5460
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Novel long-period stacking-ordered structure of martensite in zirconium–cobalt–palladium alloys2015

    • Author(s)
      M. Matsuda, F. Tanaka, S. Tsurekawa, K. Takashima, M. Mitsuhara, M. Nishida
    • Journal Title

      Philosophical Magazine Letters

      Volume: 95 Issue: 1 Pages: 21-29

    • DOI

      10.1080/09500839.2014.995739

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Reduction and carbonitriding of anodic titanium oxide film by using a mixture of iron and carbon powders2015

    • Author(s)
      M. Yoshimoto, S. Agawa, Y. Morizono and S. Tsurekawa
    • Journal Title

      Journal of the Ceramic Society of Japan

      Volume: 123 Issue: 1441 Pages: 903-907

    • DOI

      10.2109/jcersj2.123.903

    • NAID

      130005096379

    • ISSN
      1348-6535, 1882-0743
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Aluminizing of High-carbon Steel by Explosive Welding and Subsequent Heat Treatment2015

    • Author(s)
      Y. Morizono, T. Yamaguchi, S. Tsurekawa
    • Journal Title

      ISIJ International

      Volume: 55 Issue: 1 Pages: 272-277

    • DOI

      10.2355/isijinternational.55.272

    • NAID

      130004734507

    • ISSN
      0915-1559, 1347-5460
    • Related Report
      2015 Annual Research Report 2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Crystallography and morphology of antiphase boundary-like structure induced by martensitic transformation in Ti-Pd-Fe alloy2014

    • Author(s)
      M. Matsuda, S. Nishimura, K. Tsurekawa, K. Takashima, M. Mitsuhara, M. Nishida
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 618 Pages: 572-532

    • DOI

      10.1016/j.jallcom.2014.08.258

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] 鉄粉を利用した新しい表面改質技術2014

    • Author(s)
      森園靖浩,連川貞弘,山室賢輝
    • Journal Title

      耐火物

      Volume: 66 Pages: 542-546

    • NAID

      40020255008

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Local plastic deformation in the vicinity of grain boundaries in Fe-3 mass% Si alloy bicrystals and tricrystal2014

    • Author(s)
      S. Tsurekawa, Y. Chihara, K. Tashima, S. Ii, P. Lejcek
    • Journal Title

      Journal of Materials Science

      Volume: 印刷中 Issue: 14 Pages: 4698-4704

    • DOI

      10.1007/s10853-014-8150-2

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ductility enhancement in Co-Fe-Ni alloys by microstructural control2014

    • Author(s)
      M. Matsuda, K. Yamashita, S. Tsurekawa, K. Takashima, M. Nishida
    • Journal Title

      Intermetsllics

      Volume: 52 Pages: 124-130

    • DOI

      10.1016/j.intermet.2014.04.004

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] In situ observations of crack propagation and role of grain boundary microstructure in nickel embrittled by sulfur2014

    • Author(s)
      S. Kobayashi, T. Maruyama, S. Saito, S. Tsurekawa, T. Watanabe
    • Journal Title

      Journal of Materials Science

      Volume: 49 Issue: 11 Pages: 4007-4017

    • DOI

      10.1007/s10853-014-8056-z

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Transmission electron microscopy/electron energy loss spectroscopy measurements and ab initio calculation of local magnetic moments at nickel grain boundaries2014

    • Author(s)
      K. Hirayama, S. Ii, S. Tsurekawa
    • Journal Title

      Science and Technology of Advanced Materials

      Volume: 15 Issue: 1 Pages: 015005-015005

    • DOI

      10.1088/1468-6996/15/1/015005

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Differential Scanning Calorimetry of the α/γ Transformation in Fe–Co Alloys under a Magnetic Field2013

    • Author(s)
      W. Maruno, Y. Morizono, S. Tsurekawa
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 54 Issue: 9 Pages: 1823-1828

    • DOI

      10.2320/matertrans.M2013174

    • NAID

      10031194678

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Surface Hardening of Titanium by Using a Simplified Carbon and Nitrogen Diffusion Technique with Steel and Carbon Powders2013

    • Author(s)
      Y. Morizono, Y. Kawano, S. Tsurekawa, T. Yamamuro
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 54 Issue: 8 Pages: 1454-1459

    • DOI

      10.2320/matertrans.M2012409

    • NAID

      10031189504

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of Nanostructured Tungsten Based Materials Resistant to Recrystallization and/or Radiation Induced Embrittlement2013

    • Author(s)
      H. Kurishita
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 54 Issue: 4 Pages: 456-465

    • DOI

      10.2320/matertrans.MG201209

    • NAID

      10031162810

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2013 Annual Research Report 2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Reply to “Comment on direct measurement of local magnetic moments at grain boundaries in iron” by Stoger-Pollach2013

    • Author(s)
      K. Hirayama, S. Ii, S. Tsurekawa
    • Journal Title

      Scripta Materialia

      Volume: 69 Issue: 11-12 Pages: 823-825

    • DOI

      10.1016/j.scriptamat.2013.08.003

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of post-GBE strain-sensitisation on corrosion resistance of grain boundary engineered 304 austenitic stainless steel2013

    • Author(s)
      G. Yamada
    • Journal Title

      Philosophical Magazine

      Volume: 93 Issue: 10-12 Pages: 1443-1453

    • DOI

      10.1080/14786435.2012.762467

    • Related Report
      2013 Annual Research Report 2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Growth of bridging carbon nanofibers in cracks formed by heat-treating iron oxide thin sheets in acetylene gas2013

    • Author(s)
      T. Hikata, S. Okubo, Y. Higashi, T. Matsuba, R. Utsunomiya, S. Tsurekawa, K. Murakami, J. Fujita
    • Journal Title

      AIP Advances

      Volume: 3 Issue: 4 Pages: 042127-042127

    • DOI

      10.1063/1.4802966

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Potential barrier at grain boundaries in polycrystalline silicon: influence of grain-boundary character and copper/iron contamination2013

    • Author(s)
      S. Tsurekawa, H. Takahashi, Y. Nishibe, T. Watanabe
    • Journal Title

      Philosophical Magazine

      Volume: 93 Issue: 10-12 Pages: 1413-1424

    • DOI

      10.1080/14786435.2012.753482

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Direct measurement of local magnetic moments at grain boundaries in iron2013

    • Author(s)
      S. Ii
    • Journal Title

      Scripta Materialia

      Volume: 68 Issue: 5 Pages: 253-256

    • DOI

      10.1016/j.scriptamat.2012.10.028

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Surface Cracking on Σ3, Σ 9 CSL and Random Grain Boundaries in Helium Implanted 316L Austenitic Stainless Steel2013

    • Author(s)
      N. Sakaguchi
    • Journal Title

      Journal of Nuclear Materials

      Volume: 432 Issue: 1-3 Pages: 23-27

    • DOI

      10.1016/j.jnucmat.2012.08.019

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Radiation-induced segregation and corrosion behavior on Σ3 coincidence site lattice and random grain boundaries in proton-irradiated type-316L austenitic stainless steel2013

    • Author(s)
      Norihito Sakaguchi
    • Journal Title

      Journal of Materials Science

      Volume: 434 Issue: 1-3 Pages: 65-71

    • DOI

      10.1016/j.jnucmat.2012.11.036

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Corrosion-erosion test of SS316L grain boundary engineering material (GBEM) in lead bismuth flowing loop2012

    • Author(s)
      Shigeru Saito
    • Journal Title

      Journal of Materials Science

      Volume: 431 Issue: 1-3 Pages: 91-96

    • DOI

      10.1016/j.jnucmat.2011.11.040

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Controlling grain boundary character distribution of high-temperature B2 phase in Ti-Ni-Fe alloy2012

    • Author(s)
      S. Ii
    • Journal Title

      Intermetallics

      Volume: 31 Pages: 65-71

    • DOI

      10.1016/j.intermet.2012.06.009

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Grain boundary engineering based on fractal analysis for control of segregation-induced intergranular brittle fracture in polycrystalline nickel2012

    • Author(s)
      S. Kobayashi
    • Journal Title

      Acta Materialia

      Volume: 60 Issue: 17 Pages: 6200-6212

    • DOI

      10.1016/j.actamat.2012.07.065

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ステンレス鋼に対する簡易浸炭処理法2012

    • Author(s)
      森園靖浩
    • Journal Title

      鉄と鋼

      Volume: 98 Pages: 476-481

    • NAID

      130002127331

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Anodizing of aluminum in sulfuric acid and oxalic acid solutions with percarboxylic acid-based additive2012

    • Author(s)
      M. Yoshimoto
    • Journal Title

      Journal of the Ceramic Society of Japan

      Volume: 120 Issue: 1403 Pages: 276-279

    • DOI

      10.2109/jcersj2.120.276

    • NAID

      130004480079

    • ISSN
      1348-6535, 1882-0743
    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Grain boundary plane reorientation : model experiments on bi-and tricrystals2012

    • Author(s)
      Pavel Lejcek
    • Journal Title

      Journal of Materials Science

      Volume: 47 Issue: 13 Pages: 5106-5113

    • DOI

      10.1007/s10853-012-6384-4

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Presentation] 液体Pb-Bi腐食された粒界制御フェライト系耐熱鋼T91のマイクロピラー圧縮試験2016

    • Author(s)
      楓杏子,多久島睦子,Ales Jager,連川貞弘,山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      九州大学春日キャンパス
    • Year and Date
      2016-06-11
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高強度鋼SCM435の水素脆化挙動に及ぼす粒界制御熱処理の影響2016

    • Author(s)
      伊藤宏輝,連川貞弘,森園靖浩,山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      九州大学春日キャンパス
    • Year and Date
      2016-06-11
    • Related Report
      2015 Annual Research Report
  • [Presentation] Aluminide Coating on Nickel by Explosive Welding and Subsequent Heat Treatment2015

    • Author(s)
      Y. Morizono, T. Koyanagi, S. Tsurekawa
    • Organizer
      International Workshop on Explosion, Shock-wave and High-velocity Phenomena 2015 (ESHP 2015)
    • Place of Presentation
      熊本大学黒髪南キャンパス
    • Year and Date
      2015-09-28
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 鉄粉利用によるフェライト系ステンレス鋼の表面改質2015

    • Author(s)
      森園靖浩, 松田尚久, 連川貞弘, 大西昌澄
    • Organizer
      日本鉄鋼協会第170回秋季講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] パルスレーザー・電子ビーム複合照射によるステンレス鋼の微細組織変化と照射誘起偏析2015

    • Author(s)
      中島啓介,柴山環樹,石岡準也,谷津茂男,大久保賢二,谷岡隆志,渡辺精一
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 爆発圧着とその後の熱処理によって作製したMoアルミナイド被膜の微細組織2015

    • Author(s)
      吉永聖矢, 森園靖浩, 連川貞弘, 山室賢輝
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 鉄粉パック法によるクロムめっき皮膜の改質効果2015

    • Author(s)
      山東知陽, 森園靖浩, 連川貞弘, 山室賢輝
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] ニッケル粒界の局所力学挙動に及ぼす硫黄の粒界偏析の影響2015

    • Author(s)
      高田駿士,連川貞弘,森園靖浩
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] ニッケルの粒界金造における局所力学特性に及ぼす硫黄偏析の影響2015

    • Author(s)
      高田駿士,連川貞弘,森園靖浩
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      北九州国際会議場
    • Year and Date
      2015-06-06
    • Related Report
      2015 Annual Research Report
  • [Presentation] クロムめっき鋼板に対する炭素・窒素拡散浸透処理2015

    • Author(s)
      山東知陽, 森園靖浩, 連川貞弘, 山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      北九州国際会議場
    • Year and Date
      2015-06-06
    • Related Report
      2015 Annual Research Report
  • [Presentation] アルミナイド被覆鋼の表面構成相に及ぼす鋼中炭素濃度の影響2015

    • Author(s)
      福倉槙哉,森園靖浩,連川貞弘,山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      北九州国際会議場
    • Year and Date
      2015-06-06
    • Related Report
      2015 Annual Research Report
  • [Presentation] フェライト系耐熱鋼T91の高温引張り変形にともなう微細組織変化2015

    • Author(s)
      石井涼太,山口将史,森園靖浩,連川貞弘,山室賢輝
    • Organizer
      日本鉄鋼協会第169回春季講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] TEM-EELS法を用いたFeCo合金の粒界局所磁気モーメント評価2015

    • Author(s)
      河口 寿,平山恭介,連川貞弘,森園靖浩
    • Organizer
      日本金属学会2015年春期講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] 硫黄添加多結晶ニッケルにおける粒成長挙動の特異性2015

    • Author(s)
      山崎 温,森園靖浩,連川貞弘
    • Organizer
      日本金属学会2015年春期講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] 粒界近傍における局所力学挙動からHallーPetch則を考える2015

    • Author(s)
      連川貞弘
    • Organizer
      日本金属学会グリーンエネルギー材料のマルチスケール創製研究会
    • Place of Presentation
      松江しんじ湖温泉
    • Year and Date
      2015-01-11 – 2015-01-13
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] TEM/EELS法および第一原理計算を用いた強磁性材料の粒界局所磁気モーメント評価2015

    • Author(s)
      平山恭介,連川貞弘
    • Organizer
      日本金属学会グリーンエネルギー材料のマルチスケール創製研究会
    • Place of Presentation
      松江しんじ湖温泉
    • Year and Date
      2015-01-11 – 2015-01-13
    • Related Report
      2014 Annual Research Report
  • [Presentation] Grain boundary magnetism in ferromagnetic metals2014

    • Author(s)
      S. Tsurekawa, K. Hirayama, S. Ii
    • Organizer
      7th CNRS-JSPS France-Japan Joint Seminar on New Developments for Energy, Materials and Environment
    • Place of Presentation
      Pornichet, France
    • Year and Date
      2014-10-28 – 2014-10-30
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] The Behaviors of Lattice Point Defects in FCC crystalline under Nano Second Pulsed Laser and/or Electron Irradiation2014

    • Author(s)
      A. Jinno, Y. Zhanbing, K. Nakajima,T. Shibayama, S. Yatsu and S. Watanab
    • Organizer
      10th Japanese-Polish Joint Seminar on Micro and Nano Analysis
    • Place of Presentation
      北海道大学鈴木記念ホール
    • Year and Date
      2014-10-25
    • Related Report
      2014 Annual Research Report
  • [Presentation] 塑性変形に対する粒界の役割~Hall-Petch則を考える2014

    • Author(s)
      連川貞弘
    • Organizer
      日本金属学会/日本鉄鋼協会 九州支部 秋季講演会
    • Place of Presentation
      熊本大学工学部
    • Year and Date
      2014-10-17
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] ニッケル粒界の局所磁気モーメントに及ぼす粒界偏析の影響の実権的・理論的評価2014

    • Author(s)
      平山恭介,連川貞弘,井誠一郎,M. Sob
    • Organizer
      日本金属学会2014年秋期講演大会
    • Place of Presentation
      名古屋大学東山キャンパス
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] グラファイト中への鉄粉添加によって起る鋼の浸炭現象2014

    • Author(s)
      岩田大輝,森園靖浩,連川貞弘,山室賢輝
    • Organizer
      日本金属学会2014年秋期講演大会
    • Place of Presentation
      名古屋大学東山キャンパス
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] 二相ステンレス鋼の磁場中熱処理における再結晶組織2014

    • Author(s)
      藤井啓道,佐野康太郎,佐藤裕,粉川博之,連川貞弘
    • Organizer
      日本鉄鋼協会第168回秋季講演大会
    • Place of Presentation
      名古屋大学東山キャンパス
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] Towards development of high-efficiency polycrystalline solar cells using grain boundary engineering2014

    • Author(s)
      S. Tsurekawa
    • Organizer
      Yellow Sea Rim Workshop on Explosion, Combustion and Other Energetic Phenomena for Various Environmental Issues
    • Place of Presentation
      Kumamoto, Japan
    • Year and Date
      2014-09-17 – 2014-09-19
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Nanoindentation study of incipient plasticity in the vicinity of grain boundaries in Fe-3mass% Si alloy bicrystals and tricrystal2014

    • Author(s)
      S. Tsurekawa, Y. Chihara, K. Tashima, S. Ii, P. Lejcek
    • Organizer
      13th International Symposium on Physics of Materials (ISPMA 13)
    • Place of Presentation
      Prague, Czech Republic
    • Year and Date
      2014-08-31 – 2014-09-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] ニッケルの粒成長に及ぼす硫黄の効果2014

    • Author(s)
      山崎温,森園靖浩,連川貞弘
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2014-06-07
    • Related Report
      2014 Annual Research Report
  • [Presentation] 鋼中への炭素の拡散浸透現象に対する鉄粉利用の効果2014

    • Author(s)
      岩田大輝,森園靖浩,連川貞弘,山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2014-06-07
    • Related Report
      2014 Annual Research Report
  • [Presentation] TEM-EELSを用いたコバルト粒界の局所磁気モーメント2014

    • Author(s)
      河口寿,平山恭介,森園靖浩,連川貞弘
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2014-06-07
    • Related Report
      2014 Annual Research Report
  • [Presentation] Magnetization at the grain boundaries in ferromagnetic metals: Theory and experiment2014

    • Author(s)
      M. Sob, M. Vsianska, H. Vemolova, K. Hirayama, S. Ii, S. Tsurekawa
    • Organizer
      Atomic structure of nanosystems from first-principles simulations and microscopy experiments
    • Place of Presentation
      Helsinki, Finland
    • Year and Date
      2014-06-03 – 2014-06-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] 鉄鋼材料における粒界工学2014

    • Author(s)
      連川貞弘
    • Organizer
      日本鉄鋼協会第167回春季講演大会・鉄鋼材料の結晶界面物性とその制御フォーラム「鉄鋼材料における結晶界面研究の現状理解」
    • Place of Presentation
      東京工業大学 大岡山キャンパス
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 鉄粉を利用した新しい炭素・窒素拡散浸透技術2014

    • Author(s)
      森園靖浩
    • Organizer
      日本金属学会・第1回グリーンエネルギー材料のマルチスケール創製研究会
    • Place of Presentation
      上天草市 ホテル松竜園 海星
    • Related Report
      2013 Annual Research Report
  • [Presentation] Potential barrier at grain boundaries in polycrystalline silicon and cadmium telluride for solar cells2013

    • Author(s)
      S. Tsurekawa, H. Takahashi, Y. Nishibe, S. Ods
    • Organizer
      International Symposum on EcoTopia Science
    • Place of Presentation
      Nagoya, Japan
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 高Crフェライト系耐熱鋼T91におけるα'→γ相変態挙動のSEM/EBSDその場観察2013

    • Author(s)
      中園亮,吹野達也,連川貞弘,森園靖浩
    • Organizer
      第55回日本顕微鏡学会九州支部総会・学術講演会
    • Place of Presentation
      九州大学伊都キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] State-of-the-art grain boundary engineering towards development of new materials2013

    • Author(s)
      S. Tsurekawa, T. Watanabe
    • Organizer
      International Conference on PROCESSING & MANUFACTURING OF ADVANCED MATERIALS (THERMEC'2013)
    • Place of Presentation
      Rio Hotel, Las Vegas, USA
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Quantitative analyses by transmission electron microscopy and those application to the grain boundary phenomena2013

    • Author(s)
      S. Ii, S. Tsurekawa, K. Tsuchiya
    • Organizer
      International Conference on PROCESSING & MANUFACTURING OF ADVANCED MATERIALS (THERMEC'2013)
    • Place of Presentation
      Rio Hotel, Las Vegas, USA
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Development of ductile B2-type Fe-Co based alloys with micro structural control2013

    • Author(s)
      M. Matsuda, R. Sago, S. Ii, S. Tsurekawa, K. Takashima, M. Nishida
    • Organizer
      International Conference on PROCESSING & MANUFACTURING OF ADVANCED MATERIALS (THERMEC'2013)
    • Place of Presentation
      Rio Hotel, Las Vegas, USA
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 粒界制御したフェライト系耐熱鋼T91の高温変形挙動2013

    • Author(s)
      山口将司,連川貞弘,森園靖浩
    • Organizer
      日本鉄鋼協会第166回秋季講演大会
    • Place of Presentation
      金沢大学角間キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] 粒界制御したフェライト系耐熱鋼T91のHAZ部における組織安定性2013

    • Author(s)
      中園亮,連川貞弘,森園靖浩
    • Organizer
      日本鉄鋼協会第166回秋季講演大会
    • Place of Presentation
      金沢大学角間キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] 炭素や窒素を拡散浸透させたフェライト系ステンレス鋼の微細組織2013

    • Author(s)
      松田尚久,森園靖浩,連川貞弘,山室賢輝
    • Organizer
      日本鉄鋼協会第166回秋季講演大会
    • Place of Presentation
      金沢大学角間キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] 粒界制御フェライト系耐熱鋼SUS410の鉛ビスマス液体金属腐食試験2013

    • Author(s)
      多久島睦子,吉井陽之輔,連川貞弘,森園靖浩,渡辺精一,柴山環樹
    • Organizer
      日本金属学会秋期(第153回)講演大会
    • Place of Presentation
      金沢大学角間キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] 鉄粒界の局所磁気モーメントに及ぼす侵入型元素の粒界偏析の影響2013

    • Author(s)
      平山恭介,森園靖浩,連川貞弘,井誠一郎
    • Organizer
      日本金属学会秋期(第153回)講演大会
    • Place of Presentation
      金沢大学角間キャンパス
    • Related Report
      2013 Annual Research Report
  • [Presentation] Grain Boundary Engineering for High Cr Ferritic Steels2013

    • Author(s)
      S. Tsurekawa, Y. Kinoshita, Y. Yoshii, Y. Morizono, V. Yardley, S. Watanabe
    • Organizer
      The 8th Pacific Rim International Congress on Advanced Materials and Processing (PRICM 8)
    • Place of Presentation
      Waikoloa, Hawaii, USA
    • Related Report
      2013 Annual Research Report
  • [Presentation] The Hall-Petch relation depending on grain boundary character distribution2013

    • Author(s)
      S. Tsurkawa
    • Organizer
      International Symposium on Strength of Fine Grained Materials - 60 years of Hall-Petch -
    • Place of Presentation
      Tokyo, Japan
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Local Plastic Deformation in the vicinity of Grain Boundaries and Hall-Petch Relation in Nickel2013

    • Author(s)
      S. Tsurekawa, K. Tashima, S. Ii
    • Organizer
      International Conference on Intergranular and Interphase Boundaries in Materials (iib 2013)
    • Place of Presentation
      Athena Pallas Village, Halkidiki, Greece
    • Related Report
      2013 Annual Research Report
  • [Presentation] In-situ Observations of Crack Propagation and Roles of Grain Boundary Microstructure in Nickel Embrittled by Sulfur2013

    • Author(s)
      S. Kobayashi, T. Maruyama, S. Saito,S. Tsurekawa, T. Watanabe
    • Organizer
      International Conference on Intergranular and Interphase Boundaries in Materials (iib 2013)
    • Place of Presentation
      Athena Pallas Village, Halkidiki, Greece
    • Related Report
      2013 Annual Research Report
  • [Presentation] 室温クリープ変形されたチタン多結晶の粒界近傍におけるひずみ緩和の観察2013

    • Author(s)
      柿坂祐貴,連川貞弘,森園靖浩,山室賢輝
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部平成25年度合同学術講演大会
    • Place of Presentation
      熊本県民交流会館パレア
    • Related Report
      2013 Annual Research Report
  • [Presentation] SUS316Lステンレス鋼溶射皮膜に対する簡易炭窒化処理2013

    • Author(s)
      上野美里,松田尚久,森園靖浩,連川貞弘,野口正広
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部平成25年度合同学術講演大会
    • Place of Presentation
      熊本県民交流会館パレア
    • Related Report
      2013 Annual Research Report
  • [Presentation] 粒界制御フェライト系耐熱構の開発2013

    • Author(s)
      連川貞弘
    • Organizer
      日本金属学会2013年春期講演大会
    • Place of Presentation
      東京理科大学
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] 強磁性材料の粒界局所磁気モーメント2013

    • Author(s)
      平山恭介
    • Organizer
      日本金属学会2013年春期講演大会
    • Place of Presentation
      東京理科大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 鉄鋼材料における粒界工学2013

    • Author(s)
      連川貞弘
    • Organizer
      日本鉄鋼協会 材料の組織と特性部会 自主フォーラム「鉄鋼材料の結晶界面物性とその制御」
    • Place of Presentation
      エッサム神田ホール
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Nano-inswntation study of local plastic deformation in the vicinity of grain boundary2012

    • Author(s)
      K. Tashima
    • Organizer
      2012 MRS Fall Meeting
    • Place of Presentation
      Hynes Convention Center, Boston, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] Measurement of the local magnetic moments at the grain boundaries in nickel via TEM/EELS technique2012

    • Author(s)
      K. Hirayama
    • Organizer
      2012 MRS Fall Meeting
    • Place of Presentation
      Hynes Convention Center, Boston, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] 太陽電池用多結晶SiおよびCdTe粒界におけるポテンシャル障壁2012

    • Author(s)
      連川貞弘
    • Organizer
      日本金属学会セミナー「材料科学的アプローチによる太陽電池研究の最前線」
    • Place of Presentation
      エッサム神田ホール
    • Related Report
      2012 Annual Research Report
    • Invited
  • [Presentation] Enhancement of the local magnetic moments at grain boundaries in ferromagnetic metals2012

    • Author(s)
      S. Tsurekawa
    • Organizer
      Materials Science and Engineering
    • Place of Presentation
      Darmstadt, Germany
    • Related Report
      2012 Annual Research Report
  • [Presentation] TEM/EELS法を用いたニッケル粒界の局所磁気モーメント評価2012

    • Author(s)
      平山恭介
    • Organizer
      日本金属学会2012年秋期講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 粒界工学手法に基づく高対応粒界頻度組織形成過程のEBSDその場観察2012

    • Author(s)
      畑瀬裕基
    • Organizer
      日本金属学会2012年秋期講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] Hall-Petchの関係に及ぼす粒界性格分布の影響2012

    • Author(s)
      田島恭平
    • Organizer
      日本金属学会2012年秋期講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 磁場作用下におけるFe-Co合金のα/γ相変態挙動の示差走査熱量分析2012

    • Author(s)
      丸野航
    • Organizer
      日本金属学会2012年秋期講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] フェライト系耐熱鋼SUH3の粒界微細組織制御2012

    • Author(s)
      吉井陽之輔
    • Organizer
      日本鉄鋼協会第164回秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 高炭素鋼線の組織に及ぼすブルーイング温度の影響2012

    • Author(s)
      西田世紀
    • Organizer
      日本鉄鋼協会第164回秋季講演大会
    • Place of Presentation
      愛媛大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] フェライト系耐熱鋼T91の高温変形にともなう微細組織変化2012

    • Author(s)
      山口将史
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      北九州国際会議場
    • Related Report
      2012 Annual Research Report
  • [Presentation] 粒界制御したフェライト系耐熱鋼T91の溶接熱影響部における微細組織変化2012

    • Author(s)
      中園亮
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部合同学術講演大会
    • Place of Presentation
      北九州国際会議場
    • Related Report
      2012 Annual Research Report
  • [Book] 「新版 鉄鋼材料と合金元素」第3章 回復,再結晶と粒成長に及ぼす合金元素の効果2015

    • Author(s)
      連川貞弘,池田賢一,中島英治
    • Total Pages
      10
    • Publisher
      日本鉄鋼協会
    • Related Report
      2015 Annual Research Report
  • [Book] 材料科学的アプローチによる太陽電池研究の最前線2012

    • Author(s)
      連川貞弘
    • Total Pages
      9
    • Publisher
      日本金属学会
    • Related Report
      2012 Annual Research Report
  • [Remarks] 熊本大学大学院自然科学研究科産業創造工学専攻 材料組織・界面制御学研究室HP

    • URL

      http://www.msre.kumamoto-u.ac.jp/~mice/

    • Related Report
      2015 Annual Research Report
  • [Remarks] 熊本大学大学院自然科学研究科産業創造工学専攻マテリアル工学講座 材料組織・界面制御学研究室HP

    • URL

      http://www.msre.kumamoto-u.ac.jp/~mice/

    • Related Report
      2014 Annual Research Report
  • [Remarks] 熊本大学大学院自然科学研究科産業創造工学専攻 材料組織・界面制御学研究室HP

    • URL

      http://www.msre.kumamoto-u.ac.jp/~mice/

    • Related Report
      2013 Annual Research Report
  • [Remarks] 材料組織・界面制御学研究室HP

    • URL

      http://www.msre.kumamoto-u.ac.jp/~mice/

    • Related Report
      2012 Annual Research Report
  • [Patent(Industrial Property Rights)] カーボンナノ構造体の製造装置およびカーボンナノ構造体の製造方法2012

    • Inventor(s)
      日方威
    • Industrial Property Rights Holder
      日方威
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2012-198377
    • Filing Date
      2012-09-10
    • Related Report
      2012 Annual Research Report

URL: 

Published: 2013-05-15   Modified: 2019-07-29  

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