• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

Early stage of precipitation in steels studied by In-house small-sangle X-ray and neutron scattering

Research Project

Project/Area Number 24360296
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Structural/Functional materials
Research InstitutionHokkaido University (2013-2014)
National Institute for Materials Science (2012)

Principal Investigator

OHNUMA Masato  北海道大学, 工学(系)研究科(研究院), 教授 (90354208)

Co-Investigator(Kenkyū-buntansha) FURUSAKA Michihiro  北海道大学, 工学研究院, 教授 (60156966)
OHBA Yojiro  京都大学, 原子炉実験所, 助教 (60566793)
PING DeHai  物質材料研究機構, 先進構造材料ユニット, 主幹研究員 (80354207)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥17,550,000 (Direct Cost: ¥13,500,000、Indirect Cost: ¥4,050,000)
Fiscal Year 2014: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2013: ¥7,020,000 (Direct Cost: ¥5,400,000、Indirect Cost: ¥1,620,000)
Fiscal Year 2012: ¥8,840,000 (Direct Cost: ¥6,800,000、Indirect Cost: ¥2,040,000)
Keywords小角散乱法 / 小型中性子源 / ラボ装置 / ナノ析出物 / 量子ビーム複合利用 / 量子ビーム / 強度・靭性 / ナノ構造
Outline of Final Research Achievements

Using both Small-angle X-ray (SAXS) and Neutron scattering (SANS), we confirm the formation of new phase with the diameter of 1nm and the change of their composition with increasing annealing temperatures in high nitrogen martensitic stainless steels . For this study, we have developed new compact SANS installed to the compact pulse neutron source in Hokkaido University. For evaluating the quality of the SANS profiles measured by in-house SANS, we comparing them to those measured by standard SANS which is installed in research reactor HANARO in Korea. The profiles measured by both SANS are perfectly same including absolute intensity level, indicating that the data obtained by in-house SANS are quantitatively correct. Above results of the formation of new phase is analyzed by the data obtained using in-house SANS. The in-house SANS can be powerful tools in the field of materials science.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (26 results)

All 2015 2014 2013 2012 Other

All Journal Article (6 results) (of which Peer Reviewed: 6 results) Presentation (20 results) (of which Invited: 2 results)

  • [Journal Article] Nanoprecipitation in a beta-titanium alloy2015

    • Author(s)
      J.Coakley, V.A. Vorontsov, K.C. Littlell, R.K. Heenan, M. Ohnuma, N.G. Jones, D.Dye
    • Journal Title

      J. of Alloy and Compounds

      Volume: 623 Pages: 146-156

    • DOI

      10.1016/j.jallcom.2014.10.038

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Precipitation in a Nanograined 7475 Aluminium Alloy-Processing, Properties and Nanoanalysis2015

    • Author(s)
      M.Lewandowska, K.wawer, P.Kozikouski, M.Ohnuma, K.J.Kuruzydlowski
    • Journal Title

      Advanced Engineering Materials

      Volume: 16 Pages: 482-485

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Review on omega phase in body-centered cubic metals and alloys2014

    • Author(s)
      Dehai Ping
    • Journal Title

      Acta Metall. Sin.

      Volume: 27 Pages: 1-11

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 中性子小角散乱法とその材料開発へのインパクト2013

    • Author(s)
      大沼正人、佐藤馨
    • Journal Title

      精密工学会誌

      Volume: 79

    • NAID

      130003385037

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Analysis of inclusions in low carbons steel using small-angle X-ray and neutron scattering2012

    • Author(s)
      Y. Oba, Koppoiu, M. Ohnuma. Y. Kinjo, S. Morooka, Y. Tomota, J. Suzuki, D. Yamaguchi, S. Koizumi, M. Sato, T. Shiraga
    • Journal Title

      ISIJ International

      Volume: 52 Pages: 457-463

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 小角散乱法によるナノサイズ不均質の評価2012

    • Author(s)
      大沼正人
    • Journal Title

      表面科学

      Volume: 33 Pages: 278-283

    • NAID

      10030756294

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Presentation] 高窒素マルテンサイト鋼におけるω相析出の可能性2015

    • Author(s)
      大沼正人、石田倫教、古坂道弘、平徳海
    • Organizer
      日本金属学会2015春期講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] ω鉄、鉄の同素体2015

    • Author(s)
      平徳海、大沼正人
    • Organizer
      日本金属学会2015春期講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] 小角散乱および透過電子顕微鏡による高窒素マルテンサイトステンレス鋼の微細構造解析2015

    • Author(s)
      石田倫教、大沼正人、佐藤博隆、古坂道弘、平徳海、阿部太一
    • Organizer
      日本鉄鋼協会2015春期講演大会
    • Place of Presentation
      東京大学駒場キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] 小型加速器パルス中性子源用小角散乱装置におけるデータ補正法2014

    • Author(s)
      石田倫教、大野博久、佐藤博隆、大沼正人、古坂道弘
    • Organizer
      日本中性子科学会2014年会
    • Place of Presentation
      札幌かでる27
    • Year and Date
      2014-12-11
    • Related Report
      2014 Annual Research Report
  • [Presentation] Characterization of Nano-Size Heterogeneities in High Nitrogen Stainless Steels by TEM, In-House SAXS & SANS2014

    • Author(s)
      M.Ohnuma, T.Ishida, M.Furusaka, D.H.Ping, B.S.Seong
    • Organizer
      2014 MRS fall meeting
    • Place of Presentation
      ボストン(アメリカ)
    • Year and Date
      2014-11-30 – 2014-12-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] Concept and Performance of i-ANS combined with small scale neutron facility2014

    • Author(s)
      M.Ohnuma, M.Furusaka, T.Ishida B.S.Seong
    • Organizer
      韓国材料学会(KIM)2014年会
    • Place of Presentation
      Highone resort (韓国)
    • Year and Date
      2014-10-23 – 2014-10-24
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] 京都大学原子炉における中性子小角散乱による鉄鋼材料評価への挑戦2014

    • Author(s)
      大場 洋次郎、杉山 正明
    • Organizer
      日本鉄鋼協会第167回春季講演大会
    • Place of Presentation
      東京工業大学(東京都)
    • Related Report
      2013 Annual Research Report
  • [Presentation] サイズ分布幅が広い析出物に対する小角散乱評価結果と直接観察結果との比較2013

    • Author(s)
      大沼、大場、津崎、片岡、佐藤
    • Organizer
      日本鉄鋼協会 春期講演大会
    • Place of Presentation
      東京電機大学(東京)
    • Year and Date
      2013-03-25
    • Related Report
      2012 Annual Research Report
  • [Presentation] Nanosize heterogeneities in Gum Metal2013

    • Author(s)
      M. Ohnuma, S. Koppoju, Y. Oba, S. Kuramoto, T. Furuta, M. Furusaka, M. Eldrup
    • Organizer
      TMS2012
    • Place of Presentation
      合衆国(サンアントニオ)(招待講演)
    • Year and Date
      2013-03-05
    • Related Report
      2012 Annual Research Report
  • [Presentation] Upgrade of Small-Angle Neutron Scattering Instrument KUR-SANS for Metallic Materials2013

    • Author(s)
      Y. Oba, M. Hino, T. Oda, M. Ohnuma, N. Sato, and M. Sugiyama,
    • Organizer
      The International Union of Materials Research Societies – International Conference in Asia 2013,
    • Place of Presentation
      Bangalore, India
    • Related Report
      2013 Annual Research Report
  • [Presentation] Characterization of Nanostructures in Co-Insulator Nanogranular Films Using Small-Angle Neutron and X-ray Scattering2013

    • Author(s)
      Y. Oba, M. Ohnuma, S. Ohnuma, K. Ohishi, S. Takata, J. Suzuki, and M. Sugiyama
    • Organizer
      The 8th Pacific Rim International Conference on Advanced Materials and Processing
    • Place of Presentation
      Hilton Waikoloa Village , Waikoloa, Hawaii,
    • Related Report
      2013 Annual Research Report
  • [Presentation] Characterization of clusters with diameter less than 2nm2012

    • Author(s)
      M. Ohnuma
    • Organizer
      International symposium on "Recent advance in a nalytical techniques for steelmaking industry
    • Place of Presentation
      科学未来館(東京)(招待講演)
    • Year and Date
      2012-11-29
    • Related Report
      2012 Annual Research Report
  • [Presentation] Study on the Early Stage of Precipitation in Steels by Combined use of SANS and SAXS2012

    • Author(s)
      M. Ohnuma. Y. Oba, P. Kozikowski, S. Koppoju
    • Organizer
      アメリカ結晶協会年会
    • Place of Presentation
      合衆国(ボストン)(招待講演)
    • Year and Date
      2012-07-31
    • Related Report
      2012 Annual Research Report
  • [Presentation] 応力下熱処理を行った試料の熱処理温度記憶効果

    • Author(s)
      大沼正人、橋本龍一
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京工業大学(東京都)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Combined Use of In-House Small-Angle Neutron and X-Ray Scattering for Characterizing Composition of Nano-Size

    • Author(s)
      Masato Ohnuma, Michihiro Furusaka, Hirotaka Sato, Rinkyo Ishida, Hirohisa Ohno
    • Organizer
      Material Research Society 2013 fall meeting
    • Place of Presentation
      the Hynes Convention Center、Boston(USA)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Impact on In-house Small-Angle Neutron Scattering to the Materials Science

    • Author(s)
      Masato Ohnuma
    • Organizer
      UCANS(Union for Compact Accelerator-driven Neutron Sources)-IV
    • Place of Presentation
      Hokkaido University,Sapporo
    • Related Report
      2013 Annual Research Report
  • [Presentation] Nano-size Cluster in Steel - Additional Way to Characterize Nosize

    • Author(s)
      Masato Ohnuma
    • Organizer
      8th Pacific Rim International Congress on Advanced Materials and Processing (PRICM-8)
    • Place of Presentation
      Hilton Waikoloa Village , Waikoloa, Hawaii,
    • Related Report
      2013 Annual Research Report
  • [Presentation] Small and Intermediate-Angle Scattering Instruments for Materials

    • Author(s)
      Michihiro Furusaka
    • Organizer
      8th Pacific Rim International Congress on Advanced Materials and Processing (PRICM-8)
    • Place of Presentation
      Hilton Waikoloa Village , Waikoloa, Hawaii,
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] X線および中性子インハウス小角散乱法による高窒素マルテン

    • Author(s)
      大沼正人、古坂道弘、石田倫教、大野博久、植田茂紀、B.S.Seong
    • Organizer
      日本鉄鋼協会第167回春季講演大会
    • Place of Presentation
      東京工業大学(東京都)
    • Related Report
      2013 Annual Research Report
  • [Presentation] 京大炉中性子小角散乱装置KUR-SANSにおける金属材料研究

    • Author(s)
      大場 洋次郎
    • Organizer
      平成25年度金属組織研究会
    • Place of Presentation
      研究社英語センター(東京都)
    • Related Report
      2013 Annual Research Report

URL: 

Published: 2012-04-24   Modified: 2019-07-29  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi