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One-pot mechanical synthesis of porous composite particles for lithium ion batteries without heat assistance

Research Project

Project/Area Number 24360315
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Metal making engineering
Research InstitutionOsaka University

Principal Investigator

NAITO Makio  大阪大学, 接合科学研究所, 教授 (40346135)

Co-Investigator(Kenkyū-buntansha) ABE Hiroya  大阪大学, 接合科学研究所, 准教授 (50346136)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥18,070,000 (Direct Cost: ¥13,900,000、Indirect Cost: ¥4,170,000)
Fiscal Year 2014: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2013: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Fiscal Year 2012: ¥12,610,000 (Direct Cost: ¥9,700,000、Indirect Cost: ¥2,910,000)
Keywords省エネルギー / セラミックス / リチウムイオン二次電池 / 正極材料 / ナノ粒子 / 複合粒子
Outline of Final Research Achievements

This research aimed at developing the one-pot mechanical process to synthesize cathode nanoparticles and prepare the nanoporous composite cathode particles with the synthesized nanoparticles and carbon nanoparticles for lithium ion batteries. As a result, lithium iron phosphate / carbon nanoporous composite particles were successfully synthesized by the proposed method without any heat assistance and atmosphere control. This method also achieved the synthesis of spinel particles composed of lithium, nickel and manganese. The obtained coin cells made by these composite particles exhibited high discharge capacity and favorable cycle performance.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (10 results)

All 2015 2014 2013 2012

All Journal Article (7 results) (of which Peer Reviewed: 7 results,  Acknowledgement Compliant: 4 results,  Open Access: 1 results) Presentation (3 results)

  • [Journal Article] Facile preparation of core@shell and concentraion-gradient spinel particles for Li-ion battery cathode materials2015

    • Author(s)
      Takahiro Kozawa, Makio Naito
    • Journal Title

      Science and Technology of Advanced Materials

      Volume: 16 Issue: 1 Pages: 015006-015006

    • DOI

      10.1088/1468-6996/16/1/015006

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Facile preparation of porous LiFePO4/C composite granules by mechanical process2015

    • Author(s)
      Takahiro Kozawa, Noriaki Kataoka, Akira Kondo, Eri Nakamura, Hiroya Abe, Makio Naito
    • Journal Title

      Materials Chemistry and Physics

      Volume: 155 Pages: 246-251

    • DOI

      10.1016/j.matchemphys.2015.02.038

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] One-step mechanical processing to prepare LSM/ScSZ composite particles for SOFC cathode2014

    • Author(s)
      Kouhei Hosokawa, Akira Kondo, Masataro Okumiya, Hiroya Abe, Makio Naito
    • Journal Title

      Advanced Powder Technology

      Volume: 25 Issue: 5 Pages: 1430-1434

    • DOI

      10.1016/j.apt.2013.12.006

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] One-step mechanical synthesis of LiFePO4/C composite granule under ambient atmosphere2014

    • Author(s)
      Takahiro Kozawa, Noriaki Kataoka, Akira Kondo, Eri Nakamura, Hiroya Abe, Makio Naito
    • Journal Title

      Ceramics International

      Volume: 40 Issue: 10 Pages: 16127-16131

    • DOI

      10.1016/j.ceramint.2014.07.043

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] 機械的手法によるLa0.8Sr0.2MnO3微粒子の合成2014

    • Author(s)
      細川晃平、近藤光、奥宮正太郎、阿部浩也、内藤牧男
    • Journal Title

      粉体工学会誌

      Volume: 51 Pages: 4-9

    • NAID

      130004545879

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effects of Mechanical Processing Conditions on the Synthesis of Oxide Nano-particles2013

    • Author(s)
      細川晃平、近藤光、奥宮正太郎、阿部浩也、内藤牧男
    • Journal Title

      Journal of the Society of Powder Technology, Japan

      Volume: 50 Issue: 8 Pages: 561-566

    • DOI

      10.4164/sptj.50.561

    • NAID

      10031191002

    • ISSN
      0386-6157, 1883-7239
    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 機械的手法によるランタン・マンガン系複合酸化物粒子合成プロセスの検討2012

    • Author(s)
      近藤光、細川晃平、中村衣利、奥宮正太郎、阿部浩也、内藤牧男
    • Journal Title

      粉体工学会誌

      Volume: 49 Pages: 745-749

    • NAID

      10031123985

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Presentation] 大気雰囲気下でのメカニカル処理によるLiFePO4正極材料の直接合成と電池特性評価2014

    • Author(s)
      小澤隆弘、片岡紀明、近藤光、中村衣利、阿部浩也、内藤牧男
    • Organizer
      第24回無機リン化学討論会
    • Place of Presentation
      高知
    • Year and Date
      2014-09-25 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] 機械的手法による複合酸化物粒子の合成とその応用2014

    • Author(s)
      小澤隆弘、近藤光、中村衣利、阿部浩也、内藤牧男
    • Organizer
      粉体工学会第49回技術討論会
    • Place of Presentation
      東京
    • Year and Date
      2014-06-17 – 2014-06-18
    • Related Report
      2014 Annual Research Report
  • [Presentation] メカニカル法によるLiFePO4/C複合ナノ粒子造粒体のワンステップ合成2014

    • Author(s)
      小澤隆弘、片岡紀明、近藤光、中村衣利、阿部浩也、内藤牧男
    • Organizer
      粉体工学会2014年度春期研究発表会
    • Place of Presentation
      京都
    • Year and Date
      2014-05-29 – 2014-05-30
    • Related Report
      2014 Annual Research Report

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Published: 2012-04-24   Modified: 2019-07-29  

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