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Development of biocompatible stainless steel and beta-type Ti alloy with high-nitrogen surface layer made by solution nitriding

Research Project

Project/Area Number 24560093
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionGifu University

Principal Investigator

YOSHIHIKO Uematsu  岐阜大学, 工学部, 教授 (80273580)

Co-Investigator(Renkei-kenkyūsha) KAKIUCHI Toshifumi  岐阜大学, 工学部, 准教授 (20452039)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2014: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2013: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2012: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Keywords疲労 / 腐食疲労 / 窒素固溶 / 表面硬化 / 窒化物析出
Outline of Final Research Achievements

Biocompatible stainless steel and beta-type Ti alloy with high-nitrogen surface layer were fabricated by solution-nitriding method. Type 304 stainless steel and beta-type Ti alloy were solution nitrided at high temperature. Solution nitriding resulted in the formation of surface-hardened layer, which was beneficial for wear resistance. In Type 304, fatigue strengths in laboratory air were highly improved by solution nitriding due to the surface-hardened layer. However, precipitation of chromium nitrides (CrN) occurred during solution nitriding, resulting in the formation of Cr-depicted zone along grain boundary. Consequently, corrosion fatigue strengths in 3%NaCl solution decreased compared with un-treated material. Solution-nitrided beta-type Ti alloy exhibited lower fatigue strengths in laboratory air than un-treated material due to the sever grain growth during solution nitriding.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (10 results)

All 2015 2014 2013 2012

All Journal Article (4 results) (of which Peer Reviewed: 3 results,  Open Access: 3 results) Presentation (6 results)

  • [Journal Article] Fatigue behavior of bulk β-type titanium alloy Ti-15Mo-5Zr-3Al annealed in high temperature nitrogen gas2015

    • Author(s)
      Masayuki Akita, Yoshihiko Uematsu, Toshifumi Kakiuchi, Masaki Nakajima, Yu Bai, Kazuhiro Tamada
    • Journal Title

      Materials Science and Engineering: A

      Volume: 627 Pages: 351-359

    • DOI

      10.1016/j.msea.2015.01.022

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Improvement of fatigue properties in type 304 stainless steel by annealing treatment in nitrogen gas2014

    • Author(s)
      Yu Bai, Masayuki Akita, Yoshihiko Uematsu, Toshifumi Kakiuchi, Yuki Nakamura, Masaki Nakajima
    • Journal Title

      Materials Science and Engineering: A

      Volume: 607 Pages: 578-588

    • DOI

      10.1016/j.msea.2014.04.047

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of solution treatment after nitriding on fatigue properties in type 304 stainless steel2014

    • Author(s)
      Masaki Nakajima, Yuki Nakamura, Kentaro Suzuki, Yu Bai, Yoshihiko Uematsu
    • Journal Title

      International Journal of Fatigue

      Volume: 68 Pages: 103-110

    • DOI

      10.1016/j.ijfatigue.2014.05.013

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Fatigue Properties of Solution-treated Type 304 Stainless Steel after Nitriding2013

    • Author(s)
      Yuki Nakamura, Masaki Nakajima, Toshihiro Shimizu, Kentaro Suzuki, Yu Bai and Yoshihiko Uematsu
    • Journal Title

      Key Engineering Materials

      Volume: 525-526 Pages: 217-220

    • DOI

      10.4028/www.scientific.net/kem.525-526.217

    • Related Report
      2012 Research-status Report
  • [Presentation] 固相窒素吸収処理を施したSUS304の疲労挙動に及ぼす鋭敏化の影響2014

    • Author(s)
      秋田正之
    • Organizer
      日本機械学会 平成26年度材料力学部門講演会(M&M2014)
    • Place of Presentation
      福島大学
    • Year and Date
      2014-07-19 – 2014-07-21
    • Related Report
      2014 Annual Research Report
  • [Presentation] Improvement of Fatigue Properties by Solution Treatment in Nitrided Type 304 Stainless Stee2014

    • Author(s)
      Kentaro Suzuki
    • Organizer
      20th European Conference on Fracture (ECF20, Fracture at all scales)
    • Place of Presentation
      Trondheim, Norway
    • Year and Date
      2014-06-30 – 2014-07-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] β型チタン合金Ti-15Mo-5Zr-3Alの疲労強度に及ぼす窒素中焼鈍処理の影響2013

    • Author(s)
      秋田正之
    • Organizer
      日本機械学会 2013年度 年次大会
    • Place of Presentation
      岡山大学
    • Related Report
      2013 Research-status Report
  • [Presentation] 窒素中焼鈍を施したSUS304の疲労挙動に及ぼす再溶体化処理の影響2013

    • Author(s)
      磯野健太
    • Organizer
      日本機械学会 平成25年度材料力学部門講演会(M&M2013)
    • Place of Presentation
      岐阜大学
    • Related Report
      2013 Research-status Report
  • [Presentation] β型チタン合金Ti-15Mo-5Zr-3Alの疲労強度に及ぼす窒素中焼鈍処理および再溶体化の影響2013

    • Author(s)
      玉田和寛
    • Organizer
      日本機械学会 東海支部第62期総会講演会
    • Place of Presentation
      三重
    • Related Report
      2012 Research-status Report
  • [Presentation] 窒素中焼鈍処理を施したステンレス鋼SUS304の大気中および塩水中における疲労挙動2012

    • Author(s)
      秋田正之
    • Organizer
      日本材料学会 第31回疲労シンポジウム
    • Place of Presentation
      東京
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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