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Fabrication of high performance pure titanium material via direct consolidation of TiH2 powder with additions of TiO2

Research Project

Project/Area Number 24560099
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionOsaka University

Principal Investigator

UMEDA JUNKO  大阪大学, 接合科学研究所, 助教 (50345162)

Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,330,000 (Direct Cost: ¥4,100,000、Indirect Cost: ¥1,230,000)
Fiscal Year 2014: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2013: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywordsレアメタルフリー / 高強靭性チタン / 酸化チタン / 酸素固溶強化 / 水素化チタン / 純チタン / 放電プラズマ焼結
Outline of Final Research Achievements

Mixtures of titanium hydride (TiH2) powders and titanium dioxide (TiO2) particles were employed as starting materials. The mixtures were consolidated by using SPS process and hot extrusion. XRD analysis showed the additive TiO2 particles were thermally decomposed and were completely dissolved into Ti matrix during SPS process at 1073K for 1.8 ks. The lattice constant in c-axis increased proportional to TiO2 contents, while no remarkable changes were detected in the a-axis. Tensile testing showed that UTS and 0.2%YS increased in proportion to TiO2 content, but elongation decreased slightly with increased TiO2 content. In particular, extruded TiH2 powder material with 1.5 wt.% TiO2 particles produced 1158 MPa UTS, 946 MPa 0.2%YS and 24% elongation. Comparison to pure Ti with no additive TiO2 particle, extruded TiH2 powder material showed the decrease of ductility while improving tensile strength. These results were showed to be superior to those of the conventional Ti-6Al-4V alloy.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (3 results)

All 2014 2012 Other

All Journal Article (1 results) Presentation (2 results)

  • [Journal Article] Oxygen Solid Solution Strengthened Pure Titanium Powder Materials2012

    • Author(s)
      Bin Sun, Shufeng Li, Hisashi Imai, Junko Umeda, Katsuyoshi Kondoh
    • Journal Title

      Transaction of JWRI

      Volume: 41 Pages: 59-64

    • NAID

      120004921927

    • Related Report
      2012 Research-status Report
  • [Presentation] 水素・酸素同時添加によって高強靭化した純チタン粉末押出材の組織構造と力学特性2014

    • Author(s)
      三本嵩哲,梅田純子,近藤勝義
    • Organizer
      平成26年度塑性加工春季講演会
    • Place of Presentation
      つくば
    • Year and Date
      2014-06-06 – 2014-06-08
    • Related Report
      2014 Annual Research Report
  • [Presentation] チタン粉末押出材の力学特性に及ぼす焼結条件の影響

    • Author(s)
      孫斌,李樹豊,今井久志,梅田純子,近藤勝義
    • Organizer
      スマートプロセス学会平成24年春季総合学術講演会
    • Place of Presentation
      大阪大学(大阪府)
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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