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Synthesis and search of a new functional diamond using ultra-high pressure and temperature synthesis method.

Research Project

Project/Area Number 24560844
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Structural/Functional materials
Research InstitutionThe University of Tokyo

Principal Investigator

GOTOU Hirotada  東京大学, 物性研究所, 技術専門職員 (50596004)

Co-Investigator(Renkei-kenkyūsha) HAMANE Daisuke  東京大学, 物性研究所, 技術職員 (20579073)
ISOBE Masahiko  マックスプランク物理学研究所(ドイツ), 研究員 (70396919)
Research Collaborator IIZUKA Riko  愛媛大学, 日本学術振興会, 特別研究員 (80632413)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,330,000 (Direct Cost: ¥4,100,000、Indirect Cost: ¥1,230,000)
Fiscal Year 2014: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2013: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Fiscal Year 2012: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywords高温高圧合成 / ダイヤモンド / 不純物 / ドープ / ダイヤモンド合成 / リチウム / 高温高圧 / 装置開発 / 物質合成
Outline of Final Research Achievements

In this study, impurity-doped diamonds were synthesized using high pressure and temperature synthesis method with pressure higher than that employed conventionally. Li- and Mg- doped diamonds were successfully prepared; however, to synthesize Li-doped diamond, Li-GIC (Graphite intercalation compound) is need as a starting material, while the synthesis of the Mg-doped diamond requires the use of a catalyst. In addition, the formation mechanism of Mg-doped diamond was investigated by in-situ X-ray diffraction experiment.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (19 results)

All 2015 2014 2013 2012

All Journal Article (9 results) (of which Peer Reviewed: 9 results,  Open Access: 2 results,  Acknowledgement Compliant: 1 results) Presentation (10 results)

  • [Journal Article] Application of x-ray radiography to study the segregation process of iron from silicate under high pressure and high temperature.2015

    • Author(s)
      H. Gotou, T. Yagi, R. Iizuka and A. Suzuki
    • Journal Title

      High Pressure Research

      Volume: 35 Issue: 2 Pages: 130-138

    • DOI

      10.1080/08957959.2015.1028932

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Phase transitions and hydrogen bonding in deuterated calcium hydroxide: High-pressure and high-temperature neutron diffraction measurements.2014

    • Author(s)
      R. Iizuka, K. Komatsu, H. Kagi, T. Nagai, A. Sano-Furukawa, T. Hattori, H. Gotou and T. Yagi
    • Journal Title

      Journal of Solid State Chemistry

      Volume: 218 Pages: 95-102

    • DOI

      10.1016/j.jssc.2014.06.010

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Pressure-induced oligomerization of benzene at room temperature as a precursory reaction of amorphization2014

    • Author(s)
      Shinozaki, A; Mimura, K; Kagi, H; Komatu, K; Noguchi, N; Gotou, H
    • Journal Title

      JOURNAL OF CHEMICAL PHYSICS

      Volume: 141 Issue: 8 Pages: 0843061-0843061

    • DOI

      10.1063/1.4893870

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Pressure effect on the structure and superconducting transition temperature of filled skutterudites LaT4P12 (T=Fe, Ru)2013

    • Author(s)
      Y. Kawamura, T. Kawaai, J. Hayashi, C. Sekine, H. Goto, J. Cheng, K. Matsubayashi, Y. Uwatoko
    • Journal Title

      J. Phys. Soc. Jpn.

      Volume: 82 Issue: 11 Pages: 114702-114702

    • DOI

      10.7566/jpsj.82.114702

    • NAID

      120005350481

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Crystal structure of the high-pressure phase of calcium hydroxide, portlandite : In situ powder and single-crystal X-ray diffraction study2013

    • Author(s)
      R. lizuka T. Yagi, K. Komatsu, H. Gotou, T. Tsuchiya, K. Kusaba, H. Kagi
    • Journal Title

      American Mineralogist

      Volume: 98 Issue: 8-9 Pages: 1421-1428

    • DOI

      10.2138/am.2013.4386

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Anomalous behavior of cristobalite in heliumunder high pressure2013

    • Author(s)
      T. Sato, H. Takada, T. Yagi, H. Gotou, T. Okada, D. Wakabayashi, N. Funamori
    • Journal Title

      Physics and Chemistry of Minerals

      Volume: 40 Issue: 1 Pages: 3-10

    • DOI

      10.1007/s00269-012-0540-x

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Synthesis, Structure and Electromagnetic Properties of Manganese Hollandite, KxMn8O162012

    • Author(s)
      T. Kuwabara, M. Isobe, H. Gotou, T. Yagi, D. Nishio-Hamane, and Y. Ueda
    • Journal Title

      J. Phys. Soc. Jpn

      Volume: 81 Issue: 10 Pages: 104701-104701

    • DOI

      10.1143/jpsj.81.104701

    • NAID

      210000109733

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Compression behaviors of distorted rutile-type hydrous phases, MOOH (M = Ga, In, Cr) and CrOOD2012

    • Author(s)
      A. Sano-Furukawa, T. Yagi, T. Okada, H. Gotou, T. Kikegawa
    • Journal Title

      Physics and Chemistry of Minerals

      Volume: 39 Issue: 5 Pages: 375-383

    • DOI

      10.1007/s00269-012-0487-y

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] An opposed-anvil-type apparatus with an optical window and a wide-angle aperture for neutron diffraction2012

    • Author(s)
      Riko IIZUKA, Takehiko YAGI, Hirotada GOTOU, Kazuki KOMATSU, Hiroyuki KAGI
    • Journal Title

      HIGH PRESSURE RESEARCH

      Volume: 32 Issue: 3 Pages: 430-441

    • DOI

      10.1080/08957959.2012.722213

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] Pt触媒を用いたダイヤモンド合成の試み2015

    • Author(s)
      後藤 弘匡
    • Organizer
      物構研サイエンスフェスタ
    • Place of Presentation
      つくば国際会議場(茨城県つくば市)
    • Year and Date
      2015-03-17 – 2015-03-18
    • Related Report
      2014 Annual Research Report
  • [Presentation] 中性子実験用の新型ジャケット付きアンビルとそれを用いた6-6式高温高圧実験技術の開発2014

    • Author(s)
      後藤弘匡、八木健彦、飯塚理子
    • Organizer
      第55回高圧討論会
    • Place of Presentation
      徳島大学(徳島県徳島市)
    • Year and Date
      2014-11-22 – 2014-11-24
    • Related Report
      2014 Annual Research Report
  • [Presentation] 中性子線を用いた高温高圧その場観察実験用セルの開発2014

    • Author(s)
      後藤 弘匡
    • Organizer
      東京大学柏キャンパス技術発表会
    • Place of Presentation
      東京大学物性研究所(千葉県柏市)
    • Related Report
      2013 Research-status Report
  • [Presentation] 中性子実験に向けた高温高圧セルの開発2013

    • Author(s)
      飯塚理子、後藤弘匡、八木健彦
    • Organizer
      第54回高圧討論会
    • Place of Presentation
      朱鷺メッセ 新潟コンベンションセンター(新潟県新潟市)
    • Related Report
      2013 Research-status Report
  • [Presentation] Liドープダイヤモンドの高温高圧合成2013

    • Author(s)
      後藤弘匡、八木健彦、安部武志、新名亨、入船徹男
    • Organizer
      第54回高圧討論会
    • Place of Presentation
      朱鷺メッセ 新潟コンベンションセンター(新潟県新潟市)
    • Related Report
      2013 Research-status Report
  • [Presentation] Development of high pessure and high temperature experiment techniques for in-situ X-ray observation using a modified simple opposed anvil apparatus2013

    • Author(s)
      H. GOTO, T. YAGI, A. Shinozaki, and T. Kikegawa
    • Organizer
      51th European High Pressure Reserch Group International Meeting
    • Place of Presentation
      Queen Mary university of London (London, the United Kingdom)
    • Related Report
      2013 Research-status Report
  • [Presentation] 安定した温度測定が可能な対向アンビル型高温高圧発生装置の開発2013

    • Author(s)
      後藤弘匡、八木健彦
    • Organizer
      愛媛大学総合技術研究会
    • Place of Presentation
      松山
    • Related Report
      2012 Research-status Report
  • [Presentation] 試料容積が大きくとれる新しい対向アンビル型装置を用いた高温高圧実験技術の開発2013

    • Author(s)
      後藤弘匡、八木健彦
    • Organizer
      物構研サイエンスフェスタ
    • Place of Presentation
      つくば
    • Related Report
      2012 Research-status Report
  • [Presentation] In-situ X-ray observation of ZnS under high pressure and high temperature2012

    • Author(s)
      Hirotada GOTOU, Takehiko YAGI, Tamami KOIZUMI, Riko IIZUKA, Kazuki KOMATSU
    • Organizer
      50th European High Pressure Research Group Meeting
    • Place of Presentation
      Thessaloniki, GREECE
    • Related Report
      2012 Research-status Report
  • [Presentation] 小型・軽量な新しい対向アンビル型装置を用いたZnSの高温高圧相転移の観察2012

    • Author(s)
      後藤弘匡、八木健彦
    • Organizer
      第53回高圧討論会
    • Place of Presentation
      大阪
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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