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Development of Low Temperature Bonding Technique of Titanium and Zirconium using Hydrogen Diffusion-Induced Phase Transformation

Research Project

Project/Area Number 24560878
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Material processing/treatments
Research InstitutionOsaka University

Principal Investigator

SAIDA Kazuyoshi  大阪大学, 工学(系)研究科(研究院), 教授 (30178470)

Co-Investigator(Kenkyū-buntansha) MORI Hiroaki  大阪大学, 大学院工学研究科, 准教授 (10294026)
OGIWARA Hiroyuki  大阪大学, 大学院工学研究科, 助教 (80455279)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2014: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2013: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywords低温拡散接合 / 水素誘起拡散変態 / チタン / ジルコニウム / 水素化物 / 接合部組織 / 接合強さ / 耐食性 / 拡散接合 / 水素拡散誘起変態 / 引張強さ / 破面解析 / 組織解析 / 接合後熱処理 / 接合継手特性
Outline of Final Research Achievements

A new bonding technique of titanium and zirconium conducted at low temperatures was developed utilizing the hydrogen-induced transformation. Titanium and zirconium hydrides were formed at faying surfaces after hydrogen charge treatment. The β-transus temperature at faying surfaces of titanium and zirconium was reduced to approx. 450-550C with hydrogen-charging. Grain growth across the prior bond interface was observed in the joints bonded at 750-800C after hydrogen-charging for 300-500ks. Tensile strength of titanium joints bonded at 800C attained approx. 70% of the base metal strength (approx. 1.6 times as high as non-charged joints), and corrosion resistance of the joints was comparable to that of the base metal. Furthermore, tensile strength of zirconium joints bonded at 800C was approx. 1.7 times as high as non-charged joints. It follows that the solid-state bondability of titanium and zirconium at low temperatures was improved compared to the conventional diffusion bonding.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (5 results)

All 2015 2014 2013 2012 Other

All Journal Article (2 results) (of which Peer Reviewed: 1 results) Presentation (3 results) (of which Invited: 1 results)

  • [Journal Article] 水素拡散誘起変態を利用したチタンの低温精密接合2015

    • Author(s)
      才田一幸,西本和俊
    • Journal Title

      チタン

      Volume: 63 Pages: 1-10

    • NAID

      40020542722

    • Related Report
      2014 Annual Research Report
  • [Journal Article] Development of Low Temperature Bonding Technique of Titanium and Zirconium using Hydrogen Diffusion-Induced Phase Transformation2012

    • Author(s)
      Kazuyoshi SAIDA, Hiroyuki OGIWARA and Kazutoshi NISHIMOTO
    • Journal Title

      Materials Science Forum

      Volume: Vols. 706-709 Pages: 3010-3015

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] Distortion-Free Diffusion Bonding of Titanium and Zirconium using Hydrogen Diffusion-Induced Phase Transformation2014

    • Author(s)
      Kazuyoshi SAIDA and Kazutoshi NISHIMOTO
    • Organizer
      IIW
    • Place of Presentation
      Seoul (Korea)
    • Year and Date
      2014-07-13 – 2014-07-18
    • Related Report
      2014 Annual Research Report 2013 Research-status Report
  • [Presentation] Research Activities on Advanced Welding & Bonding2013

    • Author(s)
      Kazuyoshi SAIDA
    • Organizer
      ERC Center Seminar
    • Place of Presentation
      Pusan National University, Pusan (Korea)
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] 水素誘起拡散変態を利用したチタンおよびジルコニウムの低温拡散接合法の提案

    • Author(s)
      才田一幸,西本和俊,森 喜久一,安藤彰芳
    • Organizer
      溶接学会界面接合研究委員会
    • Place of Presentation
      東京
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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