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Preparation of compositionally graded hollow spherical particles with water-retaining ability for soil improvement

Research Project

Project/Area Number 24560893
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Material processing/treatments
Research InstitutionNihon University

Principal Investigator

TOYAMA Takeshi  日本大学, 理工学部, 准教授 (40318366)

Project Period (FY) 2012-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2014: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2013: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Fiscal Year 2012: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords噴霧乾燥 / アパタイト / 組成傾斜 / マイクロカプセル / 保水材 / 組成傾斜型粒子 / 噴霧乾燥法 / 耐水性 / 土壌改良剤 / 組成傾斜粒子 / 水酸アパタイト / 土壌改質剤
Outline of Final Research Achievements

In the spray-drying method, an aqueous solution containing dissolved materials is sprayed inside a furnace so that the materials undergo instant drying to form a powder. If two materials with different solubility exist in the solution, the particle wall is formed by depositing into low solubility material first, then, high solubility material deposited in the inner side continuously. In the present work, I could prepare the hollow spherical particles with size of 1-5 um. The particles were hydroxyapatite (outer surface)/silica (inner surface) compositionally graded hollow spherical particles. The compressive strength of these particles were maximum 17 MPa. The particles indicates a water resistance, was able to hold the water inside. Moreover, it could be suppressed soil-drying by adding the particles into the soil.

Report

(5 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (16 results)

All 2016 2015 2014 2013 2012 Other

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (11 results) (of which Int'l Joint Research: 2 results,  Invited: 3 results) Remarks (2 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] 噴霧乾燥法による炭酸カルシウム球状中空粒子の作製2014

    • Author(s)
      遠山岳史,川又智也,阿部信彦,服部安彦,小泉公志郎,梅村靖弘
    • Journal Title

      J.Soc.Inorg.Matar.Japan

      Volume: 21 Pages: 226-230

    • NAID

      40020148796

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Presentation] Preparation of compositionally graded hollow spherical particles by spray drying2016

    • Author(s)
      Takeshi Toyama
    • Organizer
      40th International Conference and Expo on Advanced Ceramics and Composites
    • Place of Presentation
      アメリカ,フロリダ
    • Year and Date
      2016-01-24
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Preparation and evaluation of hydroxyapatite/silicate compositionally graded hollow spherical particles by spray-drying2015

    • Author(s)
      Takeshi Toyama
    • Organizer
      The 8th International Symposium on Inorganic Phosphate Materials (ISIPM-8) and The 4th International Symposium on Innovations in Advanced Materials for Electronics & Optics (ISIAMEO-4)
    • Place of Presentation
      モロッコ,アガディール
    • Year and Date
      2015-09-13
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 噴霧乾燥法による組成傾斜型球状粒子の作製2015

    • Author(s)
      遠山岳史
    • Organizer
      第170回フィラー研究会
    • Place of Presentation
      連合会館(東京都千代田区)
    • Year and Date
      2015-04-09
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] 噴霧乾燥法によるⅡ型無水セッコウ軽量フィラーの作製2014

    • Author(s)
      宮内將人,遠山岳史,西宮伸幸
    • Organizer
      4th CSJ化学フェスタ2014
    • Place of Presentation
      東京,船堀
    • Year and Date
      2014-10-14 – 2014-10-16
    • Related Report
      2014 Research-status Report
  • [Presentation] Preparation and mechanical properties of II-gypsum anhydride hollow spherical particles by spray drying2014

    • Author(s)
      M. Miyauchi, T. Toyama, N. Nishimiya
    • Organizer
      3rd International Conference on Composite Materials and Technology Processes(IC-CMTP3)
    • Place of Presentation
      ハンガリー,ミシュコルツ
    • Year and Date
      2014-10-06 – 2014-10-10
    • Related Report
      2014 Research-status Report
  • [Presentation] Preparation of hydroxyapatite/nanofibrous boehmite composite hollow spherical particles by spray drying2014

    • Author(s)
      T. Toyama, T. Kodaira, N. Nagai, F. Mizukami, N. Nishimiya
    • Organizer
      3rd International Conference on Composite Materials and Technology Processes(IC-CMTP3)
    • Place of Presentation
      ハンガリー,ミシュコルツ
    • Year and Date
      2014-10-06 – 2014-10-10
    • Related Report
      2014 Research-status Report
  • [Presentation] 噴霧乾燥法によるβ型半水セッコウ球状中空粒子の作製と機械特性2014

    • Author(s)
      宮内將人,西宮伸幸,遠山岳史
    • Organizer
      無機マテリアル学会第128回学術講演会
    • Place of Presentation
      東京,御茶ノ水
    • Year and Date
      2014-06-05 – 2014-06-06
    • Related Report
      2014 Research-status Report
  • [Presentation] Preparation of compositionally graded hollow spherical particles of calcium carbonate / potassium silicate by spray drying2013

    • Author(s)
      Takeshi Toyama, Nobuhiko Abe, Yasuhiko Hattori, Koushiro Koizumi, Yasuhiro Umemura
    • Organizer
      13th International Conference of the European Ceramic Society
    • Place of Presentation
      フランス,リモージュ
    • Related Report
      2013 Research-status Report
  • [Presentation] Preparation of hollow spherical particles of gypsum by spray drying2013

    • Author(s)
      Takeshi Toyama, Kazuki Shibosawa, Nobuyuki Nishimiya
    • Organizer
      2nd International Symposium on Inorganic and Environmental Materials
    • Place of Presentation
      フランス,レンヌ
    • Related Report
      2013 Research-status Report
  • [Presentation] Preparation of compositionally graded hollow spherical particles of hydroxyapatite/potassium silicate by spray-drying2012

    • Author(s)
      Kazuki Shibosawa, Takeshi Toyama and Nobuyuki Nishimiya
    • Organizer
      2nd International Conference on Competitive Materials and Technology Process
    • Place of Presentation
      ミシュコルツ(ハンガリー)
    • Related Report
      2012 Research-status Report
  • [Presentation] 噴霧乾燥法による水酸アパタイト/ケイ酸カリウム系組成傾斜型球状粒子の作製と機械特性

    • Author(s)
      萎澤和樹,遠山岳史,西宮伸幸
    • Organizer
      第56回日本大学理工学部学術講演会
    • Place of Presentation
      日本大学理工学部(東京都)
    • Related Report
      2012 Research-status Report
  • [Remarks] 組成傾斜型粒子の作製

    • URL

      http://www.chem.cst.nihon-u.ac.jp/~toyama/research01.html

    • Related Report
      2013 Research-status Report
  • [Remarks] 組成傾斜型粒子の作製

    • URL

      http://www.chem.cst.nihon-u.ac.jp/~toyama/research01.html

    • Related Report
      2012 Research-status Report
  • [Patent(Industrial Property Rights)] 微小酸化鉄中空粒子2015

    • Inventor(s)
      遠山岳史
    • Industrial Property Rights Holder
      遠山岳史
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-248625
    • Filing Date
      2015-12-21
    • Related Report
      2015 Annual Research Report
  • [Patent(Industrial Property Rights)] 無機質中空粒子及びその製造方法2012

    • Inventor(s)
      遠山 岳史
    • Industrial Property Rights Holder
      日本大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2012-212108
    • Filing Date
      2012-09-26
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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