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Crystal growth of high performance giant magnetostriction alloys by using micro-pulling down method

Research Project

Project/Area Number 24560905
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Metal making engineering
Research InstitutionTohoku University

Principal Investigator

OIKAWA Katsunari  東北大学, 工学(系)研究科(研究院), 教授 (70356608)

Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2014: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2013: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2012: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords超磁歪 / 単結晶 / ミクロ組織 / 偏析 / 磁歪材料 / 結晶方位
Outline of Final Research Achievements

Fe2(Dy0.73Tb0.27) alloys have been received great attention as vibration-powered generator materials. In this study, the fiber shape single crystals of Fe2(Dy0.73Tb0.27) alloys were prepared by the micro-pulling-down method. Optimum conditions for the crystal growth, the solidification behavior and physical properties of them were investigated. As the results, the single crystal wires approximately 2 mm in diameter could be grown by 30mm/h pulling-down-rate using CaO crucible under Ar+6%H2 atomspherre. The effective distribution coefficient of them approximately is unit, suggesting that the macroscopic segregation is very small. The saturation magnetostriction increases with increasing the annealing temperature although the crystals annealed higher than 1173 K were broken. In addition, Zr additions increase the saturation magnetization. The sample annealed at 1173 K showed the maximum saturation magnetization about 1900ppm.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (2 results)

All 2014 2013

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Acknowledgement Compliant: 1 results) Presentation (1 results) (of which Invited: 1 results)

  • [Journal Article] Effect of Zr addition on Magnetostriction of Tb-Dy-Fe Alloys Prepared by Micro-Pulling-Down Method2014

    • Author(s)
      Katsunari Oikawa, Testu Shoji and Koichi Anzai
    • Journal Title

      Materials Science Forum

      Volume: 783-786 Pages: 2497-2502

    • DOI

      10.4028/www.scientific.net/msf.783-786.2497

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Effect of Zr addition on magnetostriction of Tb-Dy-Fe Alloys Prepared by Micro-Pulling-Down Method2013

    • Author(s)
      K. Oikawa, T. Shoji, K. Anzai
    • Organizer
      THERMEC 2013, International conference on Processing and Manufacturing of Adavanced Materials
    • Place of Presentation
      USA, Las Vegas
    • Related Report
      2013 Research-status Report
    • Invited

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Published: 2013-05-31   Modified: 2019-07-29  

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