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A simple manufacturing process of nano / micro structures using a freeze drying method

Research Project

Project/Area Number 24651149
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Nanomaterials/Nanobioscience
Research InstitutionFukuoka Industrial Technology Center

Principal Investigator

KIMURA Taro  福岡県工業技術センター, 化学繊維研究所, 専門研究員 (40416491)

Co-Investigator(Kenkyū-buntansha) UCHIYAMA Naoyuki  福岡県工業技術センター, 化学繊維研究所, 研究員 (10502247)
SAITA Shingo  福岡県工業技術センター, 化学繊維研究所, 研究員 (20502248)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2014: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2013: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywords凍結乾燥 / ナノファイバー / 多孔質体 / 多糖 / 水溶性高分子 / アルミナ / ナノ構造
Outline of Final Research Achievements

There are increasing requirements worldwide for nanofiber sheet as support for catalysis, advanced filter, substrate of cell culture, etc. However, the nanofiber of the current state is too expensive to use it as common products, because huge investment in the equipment and precise operation are necessary for production of a nanofiber.
Here we report the fabrication of various nano / micro structures, based on a freeze-drying technique from aqueous polymer solution. By changing the polymer species and the concentration of the solution, particle, nanofiber and microfiber were obtained. Especially PVP, PEO, and SPG could form nanofiber 200 nm in diameter uniformly. Moreover, it was indicated that freeze speed and drying rate has influence with nanostructures. These results are expected as a simple and low-cost production technique of nanofiber.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (7 results)

All 2015 2014 2013

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Acknowledgement Compliant: 1 results) Presentation (5 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] 凍結乾燥法を用いる新規ナノ構造体製造技術2014

    • Author(s)
      木村太郎、内山直行、齋田真吾、岡美早紀
    • Journal Title

      福岡県工業技術センター研究報告

      Volume: 24 Pages: 1-4

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] 凍結乾燥法を利用したナノ/マイクロ構造体の創製2015

    • Author(s)
      木村太郎、内山直行、齋田真吾
    • Organizer
      日本化学会第95春季年会
    • Place of Presentation
      日本大学
    • Year and Date
      2015-03-29
    • Related Report
      2014 Annual Research Report
  • [Presentation] 凍結乾燥法を利用した多糖類ナノファイバーの作製2014

    • Author(s)
      木村太郎、内山直行、齋田真吾、岡美早紀
    • Organizer
      第23回ポリマー材料フォーラム
    • Place of Presentation
      奈良県新公会堂
    • Year and Date
      2014-11-06
    • Related Report
      2014 Annual Research Report
  • [Presentation] 凍結乾燥法を利用した無機ナノファイバーの簡易製造法2014

    • Author(s)
      木村太郎、内山直行、齋田真吾、岡美早紀
    • Organizer
      第63回高分子討論会
    • Place of Presentation
      長崎大学
    • Year and Date
      2014-09-24
    • Related Report
      2014 Annual Research Report
  • [Presentation] 凍結乾燥を利用したナノ構造体の製造2014

    • Author(s)
      木村太郎、内山直行、齋田真吾、岡美早紀
    • Organizer
      第63回高分子学会年次大会
    • Place of Presentation
      名古屋国際会議場
    • Year and Date
      2014-05-28
    • Related Report
      2014 Annual Research Report 2013 Research-status Report
  • [Presentation] 凍結乾燥法を用いる新規ナノ構造体製造技術2013

    • Author(s)
      木村太郎
    • Organizer
      福岡県工業技術センタークラブ先端技術シンポジウム
    • Place of Presentation
      博多サンヒルズホテル
    • Related Report
      2013 Research-status Report
  • [Patent(Industrial Property Rights)] ポリマー繊維構造体及びその製造方法並びに複合繊維構造体2013

    • Inventor(s)
      木村 太郎
    • Industrial Property Rights Holder
      福岡県
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2013-024668
    • Filing Date
      2013-02-12
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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