Study on prcise temperature measurement of nano-size area

• Project/Area Number: 24656034
• Research Category: Grant-in-Aid for Challenging Exploratory Research
• Allocation Type: Single-year Grants
• Research Field: Thin film/Surface and interfacial physical properties
• Research Institution: Nagoya University
• Principal Investigator: SASAKI KATSUHIRO 名古屋大学, 工学(系)研究科(研究院), 准教授 (00211938)
• Project Period (FY): 2012-04-01 – 2014-03-31
• Project Status: Completed (Fiscal Year 2013)
• Budget Amount: ¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000); Fiscal Year 2013: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000); Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
• Keywords: 電子顕微鏡

Research Abstract

The determination of the temperature at a local area on a specimen in a transmission electron microscope is the repeated questioned problem and that has never been solved in the history of microscopy. I have developed nano-sized needle shape specimen of Au-Si eutectic alloy and attempted to determine the temperature by observing the position of the sold/liquid interface in the specimen. Ion shadow method was applied on the surface of the Au coated Si wafer on which the diamond powders dispersed. Partial melting behavior of the specimen and the move of the sold/liquid interface were observed by using in-situ transmission electron microscopy. The temperature of the specimen has been determined as the move of the solid/liquid interface with the sensitivity of 10ºC/5nm with the reference of the eutectic point of Au-Si system .

Research Products

• [Journal Article] <i>In Situ</i> Observation of Gold Chloride Decomposition in a Confined Nanospace by Transmission Electron Microscopy (2014)
  • Author(s): Keita Kobayashi, Ryo Kitaura, Katsuhiro Sasaki, Kotaro Kuroda, Takeshi Saito and Hisanori Shinohara
  • Journal Title: MATERIALS TRANSACTIONS Volume: 55 Issue: 3 Pages: 461-465
  • DOI: 10.2320/matertrans.MD201308
  • NAID: 130004455274
  • ISSN: 1345-9678, 1347-5320
  • Peer Reviewed
• [Journal Article] (2013)
  • Author(s): Bralee Chayasombat, Yusuke Kimata, Tomoharu Tokunaga, Kotaro Kuroda, and Katsuhiro Sasaki
  • Journal Title: Microsc. Microanal. 19 Volume: S5 Issue: S5 Pages: 119-122
  • DOI: 10.1017/s1431927613012464
  • Peer Reviewed
• [Journal Article] Microstructural analysis of thermal degradation of palladium-coated niobium membrane (2013)
  • Author(s): K.Sasaki, M.Hattori, K.Tsuchimoto, H.Yukawa, S.Arai, T.Tokunaga, Y.Murata, T.Yamamoto
  • Journal Title: J. Alloys and Compounds Volume: 573 Pages: 192-197
  • DOI: 10.1016/j.jallcom.2013.04.037
  • Peer Reviewed
• [Journal Article] (2012)
  • Author(s): K. Sasaki , H. Saka, M. Hattori, S. Arai, N. Tanaka and T. Yamamoto
  • Journal Title: Microsc. Microanal Volume: 18 (Suppl 2) Issue: S2 Pages: 1168-1169
  • DOI: 10.1017/s1431927612007696
• [Journal Article] Oxidation kinetics of single crystal silicon carbide using electron microscopy (2012)
  • Author(s): B. Chayasombat, T. Kato, T. Hirayama, T. Tokunaga, K. Sasaki, and K. Kuroda
  • Journal Title: Journal of the Ceramic Society of Japan Volume: 120 Issue: 1401 Pages: 181-185
  • DOI: 10.2109/jcersj2.120.181
  • NAID: 130004480051
  • ISSN: 1348-6535, 1882-0743
  • Peer Reviewed
• [Journal Article] Characterization of microstructures of thermal oxide scales on silicon carbide using transmission electron microscopy (2012)
  • Author(s): B. Chayasombat, T. Kato, T. Hirayama, T. Tokunaga, K. Sasaki, and K. Kuroda
  • Journal Title: Journal of the Ceramic Society of Japan Volume: 120 Issue: 1398 Pages: 64-68
  • DOI: 10.2109/jcersj2.120.64
  • NAID: 130002067590
  • ISSN: 1348-6535, 1882-0743
  • Peer Reviewed
• [Journal Article] Behavior of Cu Nanoparticles Ink under Reductive Calcination for Fabrication of Cu Conductive Film (2011)
  • Author(s): K. Ida, M. Tomonari, Y. Sugiyama, Y. Chujyo, T. Tokunaga, T. Yonezawa, K. Kuroda, K. Sasaki
  • Journal Title: Thin Solid Films Volume: 520 Issue: 7 Pages: 2789-2793
  • DOI: 10.1016/j.tsf.2011.12.024
  • Peer Reviewed
• [Presentation] (2014)
  • Author(s): 佐々木勝寛, 高橋拓也, 荒井重勇, 徳永智春, 山本剛久
  • Organizer: 顕微鏡学会第70回学術講演会
  • Place of Presentation: 千葉
• [Presentation] (2014)
  • Author(s): 佐々木勝寛, 高橋拓也, 荒井重勇, 山本剛久
  • Organizer: 日本金属学会春期講演大会2014
  • Place of Presentation: 東京
• [Presentation] 共晶ナノニードル透過電子顕微鏡内温度計の試み (2014)
  • Author(s): 佐々木勝寛、高橋拓也、荒井重勇、山本剛久
  • Organizer: 日本金属学会春期講演大会2014
  • Place of Presentation: 東京工業大学
• [Presentation] (2013)
  • Author(s): 佐々木勝寛, 高橋拓也, 荒井重勇, 徳永智春, 山本剛久
  • Organizer: 日本顕微鏡学会第69回学術講演会
  • Place of Presentation: 大阪
• [Presentation] Au-Si共晶合金の融解・凝固過程のTEM内その場観察 (2013)
  • Author(s): 佐々木勝寛、高橋拓也、荒井重勇、山本剛久
  • Organizer: 日本金属学会秋期講演大会2013
  • Place of Presentation: 金沢大学
• [Presentation] ナノサイズ針状Au-Si共晶合金のその場部分融解観察 (2013)
  • Author(s): 佐々木勝寛、高橋拓也、荒井重勇、徳永智春、山本剛久
  • Organizer: 日本顕微鏡学会第69回学術講演会
  • Place of Presentation: 大阪府吹田市
• [Presentation] (2012)
  • Author(s): 高橋拓也, 鈴木隆文, 佐々木勝寛, 徳永智春, 山本剛久
  • Organizer: 日本金属学会2012年秋季講演大会
  • Place of Presentation: 愛媛
• [Presentation] Needle Shape 合金試料による 透過電子顕微鏡内温度計測の試み (2012)
  • Author(s): 高橋 拓也、 鈴木 隆文、 佐々木 勝寛 徳永智春 山本剛久
  • Organizer: 日本金属学会2012 年秋 期 講 演 大 会
  • Place of Presentation: 日本、松山
• [Presentation] In-situ EELS of coexisting solid and liquid in a pure metal and an eutectic alloy in a TEM (2012)
  • Author(s): K. Sasaki , H. Saka, M. Hattori, S. Arai, N. Tanaka and T. Yamamoto
  • Organizer: Microsacopy and Microanalysis 2012
  • Place of Presentation: Phoenix, USA
• [Remarks]
  • URL: http://nanophysics.ap.eng.osaka-u.ac.jp/