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Development of rear earth free oxynitride phosphor and their application for white LED

Research Project

Project/Area Number 24656413
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionHiroshima University

Principal Investigator

OKUYAMA Kikuo  広島大学, 工学(系)研究科(研究院), 特任教授 (00101197)

Co-Investigator(Kenkyū-buntansha) OGI Takashi  広島大学, 大学院工学研究科, 准教授 (30508809)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2014: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2013: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2012: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Keywords発光材料 / 白色LED / 蛍光体 / 微粒子合成 / レアアースフリー / 固相法 / 酸窒化物 / 機能性微粒子 / 粉体工学 / 化学工学 / 高輝度化 / 軟X線吸収分光測定
Outline of Final Research Achievements

In this project, we focused on the development of highly luminescent rare-earth free BCNO phosphor and their application to white LED. As a result, the following results were obtained. (1) A polyethyleneimine provided BCNO phosphors with the high internal quantum efficiency. (2) XAFS spectra indicated the BCNO phosphor consists of B-N, B-O, N-O bond including SP3 carbon (3) A microwave heating can be used to synthesize BCNO nanoparticle phosphors. In addition, light-emitting polymer could be synthesized from a mixture of the prepared BCNO nanoparticles and a polyvinyl alcohol.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (30 results)

All 2015 2014 2013 2012 Other

All Journal Article (11 results) (of which Peer Reviewed: 11 results,  Acknowledgement Compliant: 1 results) Presentation (14 results) (of which Invited: 6 results) Book (3 results) Remarks (2 results)

  • [Journal Article] Transient Nature of Graphene Quantum Dots Formation via a Hydrothermal Reaction2014

    • Author(s)
      T. Ogi, H. Iwasaki, K. Aishima, F. Iskandar, W-N Wang, K Takimiya, and K. Okuyama
    • Journal Title

      RSC Advances

      Volume: 4 Issue: 99 Pages: 55709-55715

    • DOI

      10.1039/c4ra09159k

    • NAID

      120006796552

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Low-energy bead-milling dispersions of rod-type titania nanoparticles and their optical properties2014

    • Author(s)
      T. Tahara, Y. Imajou, A. B. D. Nandiyanto, T. Ogi, T. Iwaki, and K. Okuyama
    • Journal Title

      Advanced Powder Technology

      Volume: 25 Issue: 5 Pages: 1492-1499

    • DOI

      10.1016/j.apt.2014.04.004

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Nanostructuring strategies in functional fine-particle synthesis towards resource and energy saving applications2014

    • Author(s)
      T. Ogi, A.B.D. Nandiyanto, K. Okuyama
    • Journal Title

      Advanced Powder Technology

      Volume: 25 Issue: 1 Pages: 3-17

    • DOI

      10.1016/j.apt.2013.11.005

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Synthesis and photoluminescence of BCNO/SiO2 nanocomposite phosphor materials2014

    • Author(s)
      I. D. Faryuni, B. W. Nuryadin, F. Iskandar, M. Abdullah, Khairurrijal, T. Ogi, K. Okuyama
    • Journal Title

      Journal of Luminescence

      Volume: 148 Pages: 165-168

    • DOI

      10.1016/j.jlumin.2013.12.033

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Photoluminescence Optimization of BCNO Phosphors Synthesized Using Citric Acid as a Carbon Source2014

    • Author(s)
      B. W. Nuryadin, T. P. Pratiwi, F. Iskandar, M. Abdullah, Khairurrijal, T. Ogi, K. Okuyama
    • Journal Title

      Advanced Powder Technology

      Volume: 印刷中 Issue: 3 Pages: 891-895

    • DOI

      10.1016/j.apt.2014.01.003

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Direct White Light Emission from a Rare-Earth-Free Aluminium-Boron-Carbon-Oxynitride Phosphor2014

    • Author(s)
      T. Ogi, H. Iwasaki, A. B. D. Nandiyanto, F. Iskandar, W. N. Wang, K. Okuyama
    • Journal Title

      Journal of Materials Chemistry C

      Volume: 印刷中 Issue: 21 Pages: 4297-4303

    • DOI

      10.1039/c3tc32314e

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Towards better phosphor design: effect of SiO2 nanoparticles on photoluminescence enhancement of YAG2013

    • Author(s)
      T. Ogi, A.B.D. Nandiyantio, K. Okino, F. Iskandar, W-N Wang, E. Tanabe, K. Okuyama
    • Journal Title

      Ce, ECS Journal of Solid State Science and Technology

      Volume: 2 Issue: 5 Pages: R91-R95

    • DOI

      10.1149/2.021305jss

    • Related Report
      2013 Research-status Report 2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] 2軸式ビーズミルによるチタニアナノ粒子の分散,凝集および再分散過程における粒子特性の変化2013

    • Author(s)
      田原 隆志, 院去 貢, 今城 祐二, 荻 崇, 奥山 喜久夫
    • Journal Title

      化学工学論文集

      Volume: 39 Pages: 426-432

    • NAID

      130004463936

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] 酸化チタンの表面改質による無色透明ナノ粒子分散液の作製2013

    • Author(s)
      荻 崇*,木崎原裕, I Made Joni, 岩木貫, 奥山喜久夫
    • Journal Title

      粉体工学会誌

      Volume: 印刷中

    • NAID

      10031178141

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Direct synthesis of spherical YAG : Ce phosphor from precursor solution containing polymer and urea2012

    • Author(s)
      A. B. Nandiyanto
    • Journal Title

      Chem. Eng. J

      Volume: 210 Pages: 461-466

    • DOI

      10.1016/j.cej.2012.09.033

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Influence of Polymer Decomposition Temperature on the Formation of Rare-Earth Free Boron Carbon Oxynitride Phosphors2012

    • Author(s)
      T. Ogi
    • Journal Title

      JOURNAL OF CHEMICAL ENGINEERING OF JAPAN

      Volume: 45 Issue: 12 Pages: 995-1000

    • DOI

      10.1252/jcej.12we138

    • NAID

      130001859693

    • ISSN
      0021-9592, 1881-1299
    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] 水熱合成法によるグラフェン量子ドットの合成と発光特性2015

    • Author(s)
      荻 崇, 相島 佳奈, 奥山 喜久夫
    • Organizer
      化学工学会第80年会
    • Place of Presentation
      芝浦工業大学
    • Year and Date
      2015-03-21
    • Related Report
      2014 Annual Research Report
  • [Presentation] 水熱合成法によるカーボン系発光材料の合成と特性評価2014

    • Author(s)
      相島 佳奈, 荻 崇, 奥山 喜久夫, 岩崎 秀治
    • Organizer
      化学工学会中国四国支部大学院生発表会
    • Place of Presentation
      広島RCC文化センター
    • Year and Date
      2014-12-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] レアアースフリー液状発光材料の合成と発光特性の評価2014

    • Author(s)
      相島 佳奈, 荻 崇, 奥山 喜久夫, 岩崎 秀治
    • Organizer
      第46回化学工学会秋季大会
    • Place of Presentation
      九州大学
    • Year and Date
      2014-09-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] Synthesis of Boron Carbon Oxynitride Phosphor Nanofibers via Electrospining2014

    • Author(s)
      Takashi Ogi,Kana Aishima, Kikuo Okuyama
    • Organizer
      International Aerosol Conference
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2014-08-29
    • Related Report
      2014 Annual Research Report
  • [Presentation] 蛍光体微粒子材料の構造化と発光特性の制御に関する研究2013

    • Author(s)
      荻 崇
    • Organizer
      化学工学会第78年回
    • Place of Presentation
      大阪大学
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] Aerosol Process for Materials Synthesis on the Use of Rare Metal2012

    • Author(s)
      荻 崇
    • Organizer
      NEPTIS21(21th Nisshin Engineering Particle
    • Place of Presentation
      金沢
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] ポリマーを用いたレアアースフリー酸窒化物 蛍光体の合成と蛍光特性2012

    • Author(s)
      沖野浩奨, 荻 崇, 奥山喜久夫
    • Organizer
      化学工学会第44回秋季大会
    • Place of Presentation
      仙台
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] Aerosol Material Processing for Energy and Environmental Application2012

    • Author(s)
      奥山 喜久夫, 荻 崇, Asep Bayu Dani Nandiyanto, Ratna Balgis
    • Organizer
      第一回日中エアロゾルシンポジウム
    • Place of Presentation
      金沢
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] レアアースフリー酸窒化物蛍光体材料の開発と発光特性の制御

    • Author(s)
      荻 崇
    • Organizer
      平成25年度中国地区化学工学懇話会
    • Place of Presentation
      広島
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] エアロゾルプロセスを利用したナノ構造体材料の創製と評価

    • Author(s)
      荻 崇, 奥山 喜久夫
    • Organizer
      第30回エアロゾル科学・技術研究討論会
    • Place of Presentation
      京都大学
    • Related Report
      2013 Research-status Report
  • [Presentation] 窒素含有ポリマーを用いたレアアースフリー酸窒化物蛍光体の合成

    • Author(s)
      荻 崇, Ferry Iskandar, Asep Bayu Dani Nandiyanto, Wei-Ning Wang, 奥山 喜久夫
    • Organizer
      第45回化学工学会秋季大会
    • Place of Presentation
      岡山大学
    • Related Report
      2013 Research-status Report
  • [Presentation] ナノ粒子ハンドリングプロセスの開発に関する研究

    • Author(s)
      荻 崇
    • Organizer
      2013年度 秋期研究発表会
    • Place of Presentation
      大阪南港ATC
    • Related Report
      2013 Research-status Report
  • [Presentation] Synthesis of Nanostructured Fine-Particles for Energy and Resources Saving

    • Author(s)
      K. Okuyama, Ratna Balgis, T. Ogi
    • Organizer
      The 5th Nanoscience and Nanotechnology Symposyum 2013
    • Place of Presentation
      Surabaya, Indonesia
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] 固相法によるレアアースフリー白色蛍光体材料の開発

    • Author(s)
      荻 崇, 奥山 喜久夫
    • Organizer
      化学工学会第79年会
    • Place of Presentation
      岐阜大学
    • Related Report
      2013 Research-status Report
  • [Book] ナノ粒子の創製と製造・処理技術-基礎物性からプロセス設計の実務 トラブル処理まで第1章粉体・ナノ粒子の機能性とその利用, 第2節ナノ粒子の機能性と工学的応用2014

    • Author(s)
      荻 崇、奥山喜久夫
    • Total Pages
      7
    • Publisher
      テクノシステム出版
    • Related Report
      2014 Annual Research Report
  • [Book] 粉体・ナノ粒子の創製と製造・処理技術-基礎物性からプロセス設計の実務 トラブル処理まで第3章粉体層・粒子群の特性, 第4節ナノ粒子の分散・集合状態の制御と利用2014

    • Author(s)
      荻 崇、奥山喜久夫
    • Total Pages
      7
    • Publisher
      テクノシステム出版
    • Related Report
      2014 Annual Research Report
  • [Book] 粉体・ナノ粒子の創製と製造・処理技術-基礎物性からプロセス設計の実務 トラブル処理まで第4章粉体の創製と加工, 第10節用途に応じたナノ粒子材料の構造化と制御2014

    • Author(s)
      荻 崇、奥山喜久夫
    • Total Pages
      11
    • Publisher
      テクノシステム出版
    • Related Report
      2014 Annual Research Report
  • [Remarks] http://home.hiroshima-u.ac.jp/~ogit/index.html/

    • Related Report
      2014 Annual Research Report
  • [Remarks] 熱流体材料工学研究室

    • URL

      http://home.hiroshima-u.ac.jp/aerosol/

    • Related Report
      2012 Research-status Report

URL: 

Published: 2013-05-31   Modified: 2019-07-29  

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