| Project/Area Number |
24656483
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| Research Category |
Grant-in-Aid for Challenging Exploratory Research
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| Allocation Type | Multi-year Fund |
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| Research Field |
Reaction engineering/Process system
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| Research Institution | Sojo University |
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Principal Investigator |
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| Project Period (FY) |
2012
|
| Project Status |
Completed (Fiscal Year 2012)
|
| Budget Amount *help |
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2012: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
|
|---|
| Keywords | マイクロリアクター / 相関移動 / 有機合成 / 液滴 / 相間移動 |
|---|
| Research Abstract |
When potassium hydroxide solution, benzene and dichloromethane including equimolar mixture of benzyltriphenylphosphonium bromide and p-methoxybenzaldehyde was fed through a cross joint into a microreactor, segmented flow consisting water droplet and oil droplets was formed and the Wittig reaction proceeded in the tube. The reaction yield in liquid-liquid-liquid reaction system was higher than that in liquid-liquid one due to the contribution of mass transfer effect.
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