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Study on the analytical assay system using 1H-NMR-DOSY method for food quality

Research Project

Project/Area Number 24658125
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Food science
Research InstitutionKyushu University

Principal Investigator

TOSHIRO Matsui  九州大学, (連合)農学研究科(研究院), 教授 (20238942)

Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2014: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2013: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2012: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
KeywordsNMR法 / DOSY分析 / 非破壊分析 / 糖定量 / 定量NMR法 / NMR-DOSY法 / 糖分析 / DOSY / 糖質分析 / 食品分析 / グルコース定量 / そのまま分析
Outline of Final Research Achievements

DOSY-1H-NMR method was applied for quantitative food analysis for the first time. The target food components are (d)-glucose and sucrose, and target protons are anomeric C1 proton. Under the optimized DOSY measurement conditions including T1 and 90 pulsed width, both sugars were successfully and separately monitored on the 2D-DOSY spectra with a gradient field of 0.05-0.3 T/m. With the aid of internal standard with the same diffusion behavior in the magnetic field, a good relationship between the ratio of proton signal against that of internal standard and the concentration was obtained. The limit of detection was >0.5 g/L for both sugars. The established DOST-1H-NMR method provided reliable results that their contents in commercially available beverages were in good agreement with those with F-kit method. Taken together, the proposed method would be useful for food analysis as non-destructive assay.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (8 results)

All 2015 2014 2013 2012 Other

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 1 results) Presentation (5 results) (of which Invited: 1 results) Remarks (1 results)

  • [Journal Article] 2.Application of diffusion ordered-1H-nuclear magnetic resonance spectroscopy to quantify sucrose in beverages2015

    • Author(s)
      Ruge Cao, Airi Nonaka, Fusae Komura, Toshiro Matsui
    • Journal Title

      Food Chemistry

      Volume: 171 Pages: 8-12

    • DOI

      10.1016/j.foodchem.2014.08.105

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Qantitative analysis of D-(+)-glucose in fruit juices using diffusion ordered-1H-nuclear magnetic resonance spectroscopy2014

    • Author(s)
      Cao, R., Komura, F., Nonaka, A., Matsui, T
    • Journal Title

      Analytical Sciences

      Volume: 30 Pages: 383-388

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] 食科学と分析化学の接点2014

    • Author(s)
      松井利郎
    • Organizer
      第92回プラズマ分光研究会
    • Place of Presentation
      島津製作所九州支店
    • Year and Date
      2014-10-10
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] 1H-NMR法を用いた飲料中の糖類の非破壊的定量法の構築2014

    • Author(s)
      野中愛理、曹 汝鴿、小村房英,松井利郎
    • Organizer
      第61回日本食品科学工学会
    • Place of Presentation
      中村学園大学
    • Year and Date
      2014-08-28 – 2014-08-30
    • Related Report
      2014 Annual Research Report
  • [Presentation] DOSY-qNMR法の糖類定量への応用2013

    • Author(s)
      野中愛理ほか
    • Organizer
      第50回化学関連支部合同九州大会
    • Place of Presentation
      北九州市国際会議場
    • Related Report
      2013 Research-status Report
  • [Presentation] Application of diffusion ordered-nuclear magnetic resonance spectroscopy to quantify glucose and sucrose in some bevarages2013

    • Author(s)
      Cao, R他
    • Organizer
      Asianalysis XII
    • Place of Presentation
      九州大学
    • Related Report
      2013 Research-status Report
  • [Presentation] Application of diffusion ordered-nucletic resonance spectroscopy to quantify glucose in beverages2012

    • Author(s)
      曹 汝鴿、小村英恵、野中愛理、松井利郎
    • Organizer
      日本食品科学工学会西日本支部大会
    • Place of Presentation
      九州大学
    • Related Report
      2012 Research-status Report
  • [Remarks] 食品分析学ホームページ

    • URL

      http://www.agr.kyushu-u.ac.jp/lab/foodanalysis/

    • Related Report
      2014 Annual Research Report

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Published: 2013-05-31   Modified: 2019-07-29  

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