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Development of the measurement method of the internal micro defects in the dental zirconia ceramics

Research Project

Project/Area Number 24659868
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Dental engineering/Regenerative dentistry
Research InstitutionTokyo Medical and Dental University

Principal Investigator

UO Motohiro  東京医科歯科大学, 医歯(薬)学総合研究科, 教授 (20242042)

Co-Investigator(Kenkyū-buntansha) TANAKA Satoshi  長岡技術科学大学, 工学部, 准教授 (20324006)
WADA Takahiro  東京医科歯科大学, 大学院医歯学総合研究科, 助教 (10632317)
Research Collaborator WADA Ken  大学共同利用機関法人, 高エネルギー加速器研究機構・物質構造科学研究所, 特別助教 (10401209)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Fiscal Year 2014: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2013: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywords歯科材料学 / ジルコニア / 微細構造 / 欠陥
Outline of Final Research Achievements

In order to increase the reliability of the zirconia restorations, it is necessary to reveal the relationship between the fracture of zirconia and their internal defect or foreign debris. In this study, the detection method of the internal defect of zirconia in various scales with using the multi probes e.g., X-ray, infrared, and positron. Transmission X-ray image and micro X-ray CT visualized void in sub-milimeter and several ten micrometer scale. Infrared microscope image visualized the micro defects which was assumed as the grain boundary of the zirconia resource particles. Positron annihilation lifetime analysis showed the existence of atomic scale defects. The deference of such defects with the composition and sintering method could not be detected.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (9 results)

All 2015 2014 2013 2012

All Journal Article (4 results) (of which Peer Reviewed: 4 results,  Open Access: 1 results) Presentation (5 results) (of which Invited: 1 results)

  • [Journal Article] Mechanical properties of orthodontic wires made of super engineering plastic2015

    • Author(s)
      Maekawa M., Kanno Z., Wada T., Hongo T., Doi H., Hanawa T., Ono T., Uo M.
    • Journal Title

      Dental Materials Journal

      Volume: 34 Issue: 1 Pages: 114-119

    • DOI

      10.4012/dmj.2014-202

    • NAID

      130004888190

    • ISSN
      0287-4547, 1881-1361
    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of calcium chloride solution immersion on surface hardness of restorative glass ionomer cements2013

    • Author(s)
      Shiozawa M., Takahashi H., Iwasaki N., Uo M.
    • Journal Title

      Dental Materials Journal

      Volume: 32 Issue: 5 Pages: 828-833

    • DOI

      10.4012/dmj.2013-143

    • NAID

      130004519321

    • ISSN
      0287-4547, 1881-1361
    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] 歯科用ジルコニアセラミックスの特徴とその留意点2013

    • Author(s)
      宇尾基弘
    • Journal Title

      日本歯技

      Volume: 1051 Pages: 26-29

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] The effect of enhancing the hydrophobicity of OMMT on the characteristics of PMMA/OMMT nanocomposites2012

    • Author(s)
      Shuichi Yamagata
    • Journal Title

      Applied Surface Science

      Volume: 262 Pages: 56-59

    • DOI

      10.1016/j.apsusc.2012.01.081

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] 高強度プラスチック製矯正ワイヤーの機械的性質2014

    • Author(s)
      前川南,簡野瑞誠,和田敬広,宇尾基弘,小野卓史
    • Organizer
      第73回日本矯正歯科学会大会
    • Place of Presentation
      幕張メッセ(千葉)
    • Year and Date
      2014-10-17 – 2014-10-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] 高強度プラスチック製矯正ワイヤーの機械的性質 第2報 口腔内環境における耐久性についての検討2014

    • Author(s)
      前川南,和田敬広,本郷敏雄,宇尾基弘
    • Organizer
      第64回日本歯科理工学会学術講演会
    • Place of Presentation
      アステールプラザ(広島)
    • Year and Date
      2014-10-04 – 2014-10-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] 希土類蛍光材を用いたコンポジットレジン用高輝度蛍光フィラーの開発2013

    • Author(s)
      宇尾基弘、和田敬広、本郷敏雄
    • Organizer
      第61回日本歯科理工学会学術講演会
    • Place of Presentation
      タワーホール船堀
    • Related Report
      2013 Research-status Report
  • [Presentation] 歯科材料におけるガラス・セラミックスの応用2013

    • Author(s)
      宇尾基弘
    • Organizer
      名古屋工業大学ライフサイエンス分野シンポジウム
    • Place of Presentation
      名古屋
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] YAG:Ce蛍光材の歯科用コンポジットレジンへの応用2012

    • Author(s)
      宇尾基弘, 中島康雄, 和田敬広, 小西智也, 曽我公平
    • Organizer
      第53回ガラスおよびフォトニクス討論会
    • Place of Presentation
      札幌
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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